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408 articles for “Synthesis”
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Optimization of Reaction Parameters for Biodiesel (Methyl Ester) Synthesis Using Surface Response Methodology
Abstract: The Polyoxo vanadate catalytic trans-esterification of waste cooking oil (WCO) was carried out by optimizing four reaction parameters which include: catalyst loading, methanol/oil ratio, temperature, and reaction time. These optimized parameters are 0.5 g, 0.8 g, and 1.2 g catalyst loading, 3:1, 6:1 and 9:1 methanol/oil ratio, 45°C, 60°C and 65°C reaction temperature, 45 min, 60 min and 90 min reaction time. The regression equation in the uncoded units of …
Published in OmniScience: A Multi-disciplinary Journal · Vol. 14, Issue 3, 2024 · pp. 20–28 Read article
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Synthesis of Biofuel from Castor Oil Using Novel Catalysts
Abstract: An essential step in improving biofuels, especially those made from biomass, is hydrodeoxygenation (HDO). HDO's primary goal is to eliminate oxygen atoms from the biofuel feedstock in the form of water, which enhances the fuel's energy density, stability, and compatibility with current fuel.This study uses a large surface area catalyst to investigate the hydrodeoxygenation (HDOx) activity of non-edible oils. In addition to other supports including H-USY and MCM-41, large surface …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 226–237 Read article
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Recent Advances in Transition Metal Complexes with Phenyl Acetic Acid and Pseudo Halogen: Synthesis, Characterization and Applications
Abstract: A well established strategy is to introduce a biologically relevant organic molecule in coordination sphere of transition metal complexes to increase the selectivity and biocompatibility. Phenylacetic acid (PAA), an organic molecule with a phenyl functional group and a carboxylic acid functional group, is a phenylalanine that is generated from the naturally occurring auxin, which is extensively present in plants. The most promising outcomes in the battle against cancer and microbes …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 68–78 Read article
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Synthesis and Study of Photoluminescence properties of Sm3+ activated 7TiO2 + 3Al2O3 + (60-x)B2 O3 +xY+ 5LiCO3 +25SrCO3 Borate Glass for SSL Applications
Abstract: Melt quenching was used to successfully create the raddish orange light-emitting Sm3+activated 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 (X=0.001, 0.002, 0.005, 0.01 and 0.02, Y=Sm3+) borate glass. XRD examination confirmed the phase of the prepared Un-doped and Doped 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 glass. Its PL characteristics under ultraviolet (UV) light (302-468 nm) were later studied. At 602 nm, the excitation was detected, and at 402 nm, the emission. …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 55–60 Read article
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Synthesis and Applications of Copper- Doped Pyridine Precipitate
Abstract: A metal organic nonlinear optical single crystal, copper doped pyridine material, was created at room temperature using the slow evaporation solution growth technique (SEST). The developed material's crystalline nature was revealed by a powder X-ray diffraction (XRD) analysis. Single crystal XRD study shows that the material synthesized possesses monoclinic system of cell parameters, a = 11.44 Å, b = 7.92 Å, C = 11.74 Å and alpha and gamma is …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 1, 2025 · pp. 51–60 Read article
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Synthesis, spectroscopic, crystal structure, Hirshfeld surface, computational, and biological investigations on Isophorone derivatives: 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one
Abstract: FT-IR, 1H NMR, and 13C NMR spectroscopy were among the spectroscopic methods used to synthesize and analyze 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one, a new isophorone derivative. Single-crystal X-ray diffraction (SCXRD) was used to determine the crystal structure, which showed that the molecule crystallizes in a monoclinic system (space group P121/c1) with packing configurations and intermolecular interactions. To learn more about the non-covalent interactions influencing the crystal packing, Hirshfeld surface analysis was used. In order …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 2, 2025 · pp. 51–69 Read article
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Synthesis and Characterization of Sustainable, Low-Cost, Biomass-Derived Carbon Films from Hevea Brasiliensis (Rubber) Wood for Environmentally Friendly Gas Sensors with Enhanced Selectivity and Sensitivity to Polar Vapors and Hazardous Gases
Abstract: Hevea brasiliensis (rubber) wood sawdust was utilized to fabricate carbon gas sensors for detecting 1000 ppm of ethanol, methanol, acetone, carbon dioxide, and ammonia gases. The carbon particles were prepared by phosphoric acid impregnation followed by thermal activation and then fabricated into films on conductive and non-conductive substrates using the doctor blade method. X-ray diffraction (XRD) analysis revealed distinct graphitic features with peaks at the (002) and (100) planes, indicating …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 1, 2025 · pp. 22–36 Read article
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Green Synthesis and Evaluation of Electronic and Optical Properties of CdS/CdTe Quantum Dots
Abstract: The CdS/CdTe quantum dots (QDs), with altered concentrations of CdS, were synthesized using straightforward precursors through an environmentally friendly green method. The synthesized quantum dots were characterization by UV–visible absorption spectroscopy, Photoluminescence (PL), and Fourier Transform Infrared Spectroscopy (FTIR) to understand their electronic and structural properties. The average particle size is nearly consistent with the values derived from Brus's formula. The UV–visible spectra show a blueshift compared with pure sample, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 185–194 Read article
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Synthesis, Spectral Characterization and Computational Studies of Hydrazine Derivative
Abstract: (E)-1-(2,3-dimethoxy benzylidene)hydrazine (2,3-DMBH) is synthesized by condensation reaction. FT-IR, ¹H NMR, ¹³C NMR spectra were recorded for this compound. The synthesized compounds were evaluated as potential drug candidates through ADME analysis and Lipinski’s rule verification. Molecular docking studies against six proteins using AUTO DOCK software showed promising results. Among them, 2,3-DMBH exhibited strong binding affinities, particularly with 3ERT (-5.44 kcal/mol), followed by 5F90, 7E9B, and 3EWD. These findings suggest that …
Published in Emerging Trends in Chemical Engineering · Vol. 12, Issue 2, 2025 · pp. 1–17 Read article
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Synthesis and Characterization of Forsterite Incorporated HDPE Composites for Microwave Substrate Application
Abstract: High Density Polyethylene (HDPE) combined with dispersed forsterite (Mg₂SiO₄) powder was utilized to fabricate polymer matrix composites (PMCs) aimed at high-frequency microwave substrate applications. Forsterite powders were synthesized using the mixed oxide method, and their phase purity was confirmed by X-ray diffraction (XRD) analysis. The dispersion and morphology of the ceramic filler within the HDPE matrix were examined through Scanning Electron Microscopy (SEM), ensuring a homogeneous distribution essential for optimal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 109–120 Read article
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Cobalt-Iron Sulfide and Cobalt Sulfide of Cobalt –III Dithiocarbamate Complexes Synthesis and Efficacy for Photocatalytic Dilapidation of Tints
Abstract: Dithio Carbamate compounds comprising pyrrole moiety which is a hetero cyclic fragrant Carbon- based composite for identifying of anions of Cobalt-III, Methyl Ferro Cenyl Sulfoxide and Nickel-II complexes were used as only basis originators on behalf of working out of Sulfide & Iron Sulfide of Cobalt atoms. Infrared spectral notes on nanoparticles endorse the occurrence of coating agent – Tri- ethylenetetramine. The exploration of nano particles by photo reagents to …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 2, Issue 1, 2024 · pp. 01–06 Read article
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Synthesis, Characterization, Biological evaluation, and in silico study of aniline derivatives
Abstract: In many hospitals worldwide, bacterial infections brought on by resistant strains are wreaking havoc, particularly in patients who are already impaired by age, disease, and other conditions. Due to the bacterial resistance, it is required to search for newer antibacterial drugs or molecules. In the current study, we aimed to develop aniline derivatives, followed by their anti-bacterial and in silico studies. Out of all the synthesized derivatives, compound 4d was …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 16, Issue 2, 2025 · pp. 25–32 Read article
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Advanced Polymer-Based Packaging Composite with Metal Oxide Nanofillers: Synthesis, Characterization, and Applications
Abstract: The development of high-performance polymeric composites for food packaging applications has gained significant attention in recent years due to increasing concerns about food safety, durability, and environmental impact. The increasing demand for active packaging materials that not only protect food but also extend shelf life has led to extensive research into polymer-based antimicrobial composites. Traditional packaging materials, including plastics, ceramics, and metals, often lack bioactive properties and can contribute to …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 56–63 Read article
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Synthesis of Thermal Resistant and Transparent Al2O3 Reinforced Epoxy-Based Composite Coatings
Abstract: This study explores the influence of thermal treatment on the structural, optical, and surface wettability characteristics of epoxy-based composite coatings reinforced with 3 wt.% aluminum oxide (Al₂O₃) nanoparticles. The coatings were synthesized via a dip-coating method on carbon fiber substrates and subjected to controlled thermal treatments at 300 °C, 400 °C, and 500 °C to assess their thermal resilience. X-ray diffraction (XRD) analysis confirmed the structural integrity of the composite …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 178–183 Read article
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Synthesis of Activated Carbon from Corn Cob and Factors Affecting its Adsorption and Desorption Efficiency of Cationic Brilliant Green Dye
Abstract: Extreme dye pollutants released from textile, leather, and pulp industries are becoming a major concern to the water. These pollutants are highly toxic to living things. The major objective of this study was to prepare low-cost and efficient activated carbon from corncob (CCAC) adsorbent through the H2SO4 activation method and characterize its suitability for removing brilliant green dye (BGD) from aqueous solution. The adsorption and desorption efficiency of the prepared …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 27–44 Read article
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Brain Tumor Detection by Aggregating Deep Learning and GAN Models for Faster MRI image Synthesis
Abstract: Brain tumors comprise a global health challenge that, in order to be treated and organized, need early and accurate diagnosis. Usually conducted through medical imaging, brain tumor detection techniques have problems of accuracy, efficiency, and confidentiality. Issues of limited datasets, strict privacy laws that provide restrictions on data sharing, and the necessity for specialized expertise on medical image analysis relegates modern methodologies to vulgar charades. For patient prognosis, treatment planning, …
Published in International Journal of Brain Sciences · Vol. 2, Issue 2, 2025 · pp. 45–53 Read article
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Facile Synthesis and Characterization of Cd²⁺ Doped NiAl₂O₄ Nanoparticles for Advanced Polymer Composite Integration
Abstract: Ni1-xCdxAl2O4, where 0 ≤ x ≤ 0.5, was successfully synthesized using the chemical co-precipitation technique, a scalable and cost-effective route suitable for composite material applications. X-ray diffraction (XRD) analysis revealed a crystalline cubic spinel structure for the resulting nanoparticles, with determined crystallite sizes ranging from 36 to 12 nm for NiAl2O4 and Cd-doped NiAl2O4. The respective band gaps for the materials were found to be 3.51 and 4.18 eV. Infrared …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 59–72 Read article
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Synthesis, Characterization, Antibacterial Evaluation and Study of Organic Separation Behavior for Five Membered Ring for Pyridine Derivatives
Abstract: Imidazoles can be prepared by condensation between amines and various aldehydes and ketones. Imidazole derivatives are important compounds due to their broad biological activity and pharmacological properties, such as antifungal, antioxidant, cytotoxic, anti-inflammatory, analgesic, anti-YFV (yellow fever virus), anti-tuberculosis, and antimicrobial activity. In recent years, many studies have been conducted on the preparation of biological imidazole derivatives, especially derivatives linked to heterogeneous rings containing nitrogen or any other donor atom. …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 16, Issue 3, 2025 · pp. 106–121 Read article
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Design, Synthesis, and Evaluation of Novel Quinazoline Derivatives as Anti-Inflammatory Agents
Abstract: Novel quinazoline derivatives are well-known heterocyclic scaffolds that are renowned for having a wide range of biological functions. A new quinazoline derivative was synthesized from anthranilic acid through a multi-step sequence involving amide formation, cyclization, and aromatic group substitution. The structure of the methoxy- and chloro-substituted final compound was confirmed by IR and 1H NMR spectroscopy. Evaluation of synthesized molecules anti-inflammatory activity using paw edema caused by carrageenan paradigm in …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 13, Issue 1, 2026 · pp. 01–09 Read article
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Azepines, Chemistry, Synthesis and Reactions
Abstract: Azepines, which consist of a seven-membered cyclic compound featuring six carbon atoms, an additional nitrogen atom, and no double bonds between carbons, form a diverse group within organic chemistry. The fully hydrated form of this compound is called azepam (C6H13N). Compounds and their variants play crucial roles in pharmaceutical research due to their biologic attributes like cancer-fighting, bacteria-killing, fungus-busting, virus-suppressing, and inflammation-reducing capabilities. Various organic molecules found within nature draw …
Published in International Journal of Minerals · Vol. 2, Issue 2, 2025 · pp. 35–45 Read article