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21 articles for “GC/MS”
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Comparative Study of Bioactive Phytochemicals from Hexane Extract of Two Amaranthaceae Leafy Vegetables by GC-MS Method
Abstract: Amaranthus tricolor Linn and Amaranthus viridis Linn, belonging to the Amaranthaceae family, are popularly consumed leafy vegetables in India and many other countries globally. The bioactive components of Hexane extract from these two plants have been analysed using gas chromatography-mass spectrometry (GC–MS) technique. According to analysis, both species contain a total of nineteen important chemicals. Of these, ten were found in A. tricolour L. and nine in A. viridis L. …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 7–17 Read article
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Bioactive Compounds in Ethanolic Extract of Strychnos innocua Root Using Gas Chromatography and Mass Spectrometry (GC-MS)
Abstract: Medicinal plants are of great relevance with endless pharmaceutical and therapeutic properties. They are source of wide array of secondary metabolites or bioactive compounds/phytochemicals (phenols, alkaloids, flavonoids, terpenoids, tannins, steroids and saponins) which can discharge numerous biological functions (antimicrobial, antioxidant, antiviral, antifungal, anti-fibrotic, immune-modulatory, cytotoxic, antipyretic, antitumor, antihelminthic, antiprotozoal, antibacterial, and so on). The use of gas chromatography and mass spectrometry analysis in identifying the bioactive compounds in the ethanolic …
Published in International Journal of Biochemistry and Biomolecule Research · Vol. 1, Issue 1, 2023 · pp. 9–14 Read article
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Recent Advancements and Comprehensive Review on Hyphenated Techniques
Abstract: Hyphenated techniques represent a powerful class of analytical methods that combine two or more established techniques – typically a separation method with a spectroscopic detection technique – to achieve enhanced analytical performance. First introduced by Hirschfeld in 1980, the term “hyphenation” refers to the online coupling of such methods, enabling more precise, sensitive, and comprehensive analysis of complex samples. These techniques exploit the strengths of individual methods while overcoming their …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 16, Issue 3, 2025 · pp. 37–50 Read article
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Formation, Analysis and Characterization of Wood Pyrolysed Oil
Abstract: Pyrolysis of wood is the possible path for converting biomass to higher valuable products such as bio-oil, bio-char and bio-gas. Bio-oil or liquid bio-fuels have higher heating values, so it can store and transport more conveniently the by-products bio-char and bio-gas, which can be used to provide heat required in the process. This work is focused on the formation, analysis and characterization of bio-oil which was obtained from the mixed …
Published in Emerging Trends in Chemical Engineering · Vol. 3, Issue 2, 2016 · pp. 36–41 Read article
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Predicting Rate Equation for the Synthesis of Octadec-9-Enoic Acid Methyl Esters by the Methanolysis of Pongamia Pinnata Triglycerides Using Sono Reactor
Abstract: In the present work, octadec-9-enoic acid methyl esters are synthesized from pongamia pinnata oil using methanolysis in sono reactor. The rate equation is predicted for the methanolysis reaction. The produced methyl esters from pongamia pinnata oil confirmed to ASTM D6751 standards. Fourier Transform Infrared Analysis and Gas Chromatography Mass Spectrometry were used to characterise the methyl esters. The rate is dependent greatly on methanol concentration, and then on catalyst concentration …
Published in Journal of Polymer & Composites · Vol. 9, Issue 3, 2021 · pp. 45–55 Read article
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Characterization Of Senna Occidentalis (Link.) Seed Extract
Abstract: Senna occidentalis (L.) Link commonly known as "coffee senna" or majamfari/rai dore in Hausa is a plant with a long history of traditional and medicinal uses against diseases such as inflammation, pains, and diabetes. This study presents characterization of the bioactive compounds of the seed extracts. Physicochemical analysis of seed powder was carried out following standard procedures. Qualitative phyto-chemical contents were determined for the presence and absence of major metabolites. …
Published in Research & Reviews : Journal of Botany · Vol. 13, Issue 3, 2024 · pp. 13–22 Read article
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A non-hydrotreated feedstock’s polyaromatic cracking under FCC industrial operating conditions using an equilibrium catalyst
Abstract: Catalytic cracking of non-hydrotreated atmospheric residue’s main polyaromatic hydrocarbon (PAHs) in the presence of an equilibrium catalyst was investigated under industrial operating conditions. During the fluid catalytic cracking process, the catalyst that presented the key factor in hydrocarbon cracking (aromatic by hydrogen transfer reaction) quickly deactivated and compromised the process’s performance due to its acid surfaces and pores covered by the polyaromatic species. A deep study of the catalyst behavior …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 1, 2025 · pp. 10–26 Read article
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A Systematic Review of Impurity Profiling and Stability Studies in Pharmaceutical Drug Substances
Abstract: Ensuring the safety, efficacy, and quality of pharmaceutical goods is essential in the Indian pharmaceutical market, which is a global centre for generic drugs. Stability studies and impurity profiling are two fundamental activities that ensure this quality during the whole lifespan of a medicine. The effect of environmental variables such as temperature, humidity, and light on the quality of a drug substance over time is demonstrated by stability studies. The …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 16, Issue 3, 2025 · pp. 81–88 Read article
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Comparative Evaluation of Hibiscus Cannabinus and Solanum Trilobatum Extracts as Inhibitors for C- Steel Corrosion protection in Acidic Medium
Abstract: This study analyzed the efficacy of various inhibitors in safeguarding carbon steel against corrosion in hydrochloric acid. The compounds that were subjected to testing included Acalypha indica root extract (AIRE), Hibiscus cannabinus (HC), and Solanum trilobatum (ST) leaf extracts. The investigation focused on the inhibitory efficacy through the application of gravimetric and electrochemical impedance methods. GC-MS and FTIR were employed to investigate the features of the inhibitors and co-inhibitors. Tafel …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 555–565 Read article
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Production of n-Butanol from Biomass by Two Step Fermentation Process Using Staphylococcus Sciuri
Abstract: This study explores the sustainable production of n-butanol from wheat husk through a two-step bioconversion process. Wheat husk, an abundant agricultural residue, was first fermented into butyric acid using Bacillus subtilis. The resultant butyric acid was then converted into n-butanol using Staphylococcus sciuri. The process leverages biological fermentation to create value-added chemicals from lignocellulosic biomass, offering an eco-friendly alternative to petrochemical methods. Two steps fermentation process were carried to increase …
Published in International Journal of Biochemistry and Biomolecule Research · Vol. 2, Issue 2, 2024 · pp. 18–31 Read article
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Monitoring the Effectiveness of Water-Based Plants for the Inhibition of Metal
Abstract: The temperature performance profile of the plant extracts shows that inhibition efficiency increased with increasing temperature of the system until at about 323K at 9.00hrs immersion time where a decline in inhibition efficiency occurred implying the opposite at higher temperatures and longer immersion time. Corrosion rate parameters changed with rise in temperature and exposure – immersion time. Plots of rates of corrosion against the volume(s) of the test inhibitor(s) in …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 13, Issue 1, 2026 · pp. 37–47 Read article
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SYNTHESIS, CHARACTERIZATION AND BIOMEDICAL APPLICATIONS OF A SILVER NANOPARTICLE-COATED CHITOSAN–FUCOIDAN POLYMER NANOCOMPOSITE LOADED WITH PERSEA AMERICANA LEAF EXTRACT
Abstract: Consuming a natural composite of Persea americana (Avocado) leaf extract and a chitosan and fucoidan form a biodegradable biopolymer matrix–polymer nanocomposite with biomedical applications, this study explored a potential therapeutic method. GC-MS and UV spectroscopy were used to describe the aqueous leaf extract, which was verified by phytochemical screening to contain flavonoids, tannins, phenols, terpenoids, and alkaloids. The chitosan–fucoidan biodegradable polymer matrix served as a biocompatible stabilizing and encapsulating carrier …
Published in Journal of Polymer & Composites · Vol. 14, Issue 5, 2026 Read article
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Sulfated Zirconia Catalyzed Biodiesel Production from Acid Oil Containing High Free Fatty Acids
Abstract: Biodiesel fuel has shown great promise as an alternative to petro-diesel fuel. Biodiesel production is widely conducted through esterification and transesterification reaction, catalyzed by homogeneous or heterogeneous catalysts. In the present endeavour, sulphated zirconia has been prepared using microwave method and characterized by using XRD, FT-IR, BET surface area, SEM and acidity measurement. The utility of synthesized catalyst is demonstrated in catalytic biodiesel production from acid oil feed stock. The …
Published in Journal of Catalyst & Catalysis · Vol. 4, Issue 2, 2017 · pp. 35–45 Read article
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Synthesis of Biodiesel from Biowaste/Vegetable Oil by Using Heterogeneous Nano-Catalyst
Abstract: This paper presents preparation of heterogeneous nanocatalyst (NaOH/ZnO-Li2CO3) for biodiesel synthesis from biowaste/vegetable oil by transesterification. Transesterification is an important reaction that produces fatty acid methyl esters which are excellent substitutes for diesel fuel. Biodiesel production by using nanocatalyst is one of important approaches in the biofuel research. The optimization of transesterification reaction is affected by the catalyst type, reaction temperature, reaction time, methanol to biowaste/oil ratio. The analysis of …
Published in Journal of Catalyst & Catalysis · Vol. 4, Issue 1, 2017 · pp. 11–23 Read article
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Thermodynamic, Kinetic and Mechanistic Investigations of Ruthenium(III) Catalyzed Methylparaben Oxidation by Diperiodatocuprate(III) in Aqueous Alkaline Medium
Abstract: The kinetics of ruthenium(III) catalyzed degradative oxidation of methylparaben by the copper complex, diperiodatocuprate(III) in alkaline medium is studied at 25ºC and at a ionic strength of 8.0 × 10−2 mol dm−3. In the presence of catalyst ruthenium(III), the reaction between methylparaben and diperiodatocuprate(III) in aqueous alkaline medium exhibits 1:1 stoichiometry. The oxidation products were identified by UV-visible, GC-MS and IR spectroscopy. The reaction exhibited unit order in case of …
Published in Journal of Catalyst & Catalysis · Vol. 2, Issue 1, 2015 · pp. 4–17 Read article
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Mechanistic and Catalytic Behavior of Os(VIII) for the Chlorpheniramine Maleate and Bromamine-B Redox System: A Kinetics Based Approach
Abstract: Chlorpheniramine maleate (CPM) is an important antihistamine agent. To the best of our knowledge there is no report in the literature about the oxidation of CPM with halogen + 1 oxidant from the stand point of its kinetics and mechanistic chemistry. Hence, a systematic kinetics and mechanistic study on the oxidation of CPM with bromamine-B (BAB) in the presence of NaOH and Os(VIII) catalyst has been carried out at 303 …
Published in Journal of Catalyst & Catalysis · Vol. 2, Issue 1, 2015 · pp. 18–31 Read article
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Semiconductor Devices for Assessing Freshness of Food Products
Abstract: Freshness of food is one of the major deterministic factors that govern human health and wellbeing. Consumption of stale food can have minor to serious health implications. In general assessment of the quality of food relies upon human sensory evaluations. However, the perceived intensity of sensory attributes can vary significantly. To replace this confusion, scientists develop portable and inexpensive sensors with notable accuracy. In particular, dairy products, seafood and meat …
Published in Journal of Semiconductor Devices and Circuits · Vol. 7, Issue 3, 2020 · pp. 5–10 Read article
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Chemical Composition and Toxicity Profile of the Essential Oils of Bosqueia angolensis Ficalho and Berlinia grandiflora (Vahl) Hutch & Dalziel
Abstract: The chemical composition of the essential oils obtained from the leaves and stem bark of Bosqueia angolensis (Moraceae) and Berlinia grandiflora (Fabaceae) using hydrodistillation were analysed using Gas Chromatography–Mass Spectrometry (GC-MS) techniques. The percentage yields of the essential oils are: B. angolensis leaves (0.53%), B. angolensis stem bark (0.49%), B. grandiflora leaves (0.45%) and B. grandiflora stem bark (0.51%). A total of 10 and four compounds representing 84.3% and 96.1% …
Published in Research and Reviews: A Journal of Toxicology · Vol. 8, Issue 2, 2018 · pp. 15–20 Read article
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Chemical Profile and Toxicity of Fresh and Dry leaves of the Essential Oils of Vetiveria zizanioides (L.) Nash. From Southwest Nigeria
Abstract: The fresh and dry leaves of Vetiveria zizanioides (L.) Nash (Gramineae) plant was collected, air dried and authenticated at the University of Ibadan Herbarium with voucher number: UIH-23237. The plant's dried, fresh leaves were hydro distilled in a Clevenger device to extract the essential oils. The oils were characterized by Gas Chromatography-Mass Spectrometry (GC – MS) while the toxicity of the essential oils was tested using brine shrimps’ lethality assay. …
Published in Recent Trends in Cosmetics · Vol. 1, Issue 1, 2024 · pp. 44–49 Read article
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Advances in Analytical Chemistry Research Methodology: Trends and Applications
Abstract: Analytical chemistry is critical to scientific study because it allows for the accurate identification, measurement, and characterization of chemical compounds. Recent advances in methodology have improved accuracy, sensitivity, and efficiency, with techniques such as High-Performance Liquid Chromatography (HPLC), Gas Chromatography (GC), Mass Spectrometry (MS), and Nuclear Magnetic Resonance (NMR) spectroscopy transforming analytical procedures. The combination of Artificial Intelligence (AI) and Machine Learning (ML) has enhanced data processing, pattern recognition, and …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 2, 2025 · pp. 10–18 Read article