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1970 articles for “3-acetyl-7-bromo-2H-chromen-2-one” (ranking capped at the first 2,000 matches — narrow the search to see the rest)
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An Efficient Synthesis of Some Novel Benzo Coumarin Derivatives Under Solvent Conditions from 2-acetyl-benzo[f]chromen-3-one
Abstract: The synthesis of the target compounds began with the preparation of 2-[3-dimethylamino[acryloyl-3H-benzo[f]chromen-3-one. This intermediate was obtained through the reaction of 2-acetylbenzo[f]coumarin-3-one with N,N-dimethylformamide dimethyl acetal [DMFDMA[ under reflux conditions in xylene. The enaminone thus formed was subsequently reacted with 6-aminothiouracil in acetic acid, leading to the formation of 2-thioxo-2,3-dihydro-1H-pyrido[2,3-d]pyrimidin-4-one. This compound served as a pivotal intermediate for the synthesis of a series of pyridotriazolopyrimidinones. These derivatives were synthesized by reacting …
Published in International Journal of Cheminformatics · Vol. 2, Issue 2, 2024 · pp. 33–46 Read article
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The thermodynamic studies of 6-(4-chlorophenyl)-1, 2, 3, 4-tetrahydro-2,4-dioxopyrimidine-5-carbonitrile in 60% DMSO in the temperature range 298 to 313 K
Abstract: Densities and viscosities of 6-(4-chlorophenyl)-1, 2, 3, 4-tetrahydro-2,4-dioxopyrimidine-5-carbonitrile have been measured at different concentration in 60% dimethyl sulphoxide (DMSO) in the temperature range 298 to 313 K. The John-Dole equation was used to determine the viscosity. Gibb’s free energy (∆G), entropy change (∆S) and enthalpy change (∆H) were evaluated from relative viscosity . The negative sign of ∆G and ∆H and positive sign of ∆S indicates the spontaneity of reaction …
Published in Journal of Polymer & Composites · Vol. 8, Issue 2, 2020 · pp. 78–81 Read article
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Theoretical Study of Substituent Effects on Electronic Properties and Polarizability for (2, 5, 24, 27-Tetrahalogen Pentacene) Molecule
Abstract: DFT and semi empirical methods have been carried out studying (2, 5, 24, 27 tetrahalogen pentacen) molecules using the B3LYP functional and the 6-311G (d, p) basis set and AM1 model. Total energy, electronic properties such as; ionization potential, electron affinity, energy gap, dipole moment, polarizability and electronic potential. The calculated ionization potential (6.126 eV) and electron affinity (1.417 eV) of this molecule is in a good agreement with experimental …
Published in Emerging Trends in Chemical Engineering · Vol. 3, Issue 1, 2016 · pp. 1–8 Read article
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Report on Indian Nuclear Programs from the 20th Century of 2nd Millennium to the 21st Century of 3rd Millennium
Abstract: In this report, the fundamental models of nuclear physics and nuclear chemistry are briefly mentioned by author. Outline of the establishment and research-directions of Bhabha Atomic Research Centre (BARC) is briefly described. Strategies regarding the Indian nuclear power plants are briefly described. Also, the Pokhran-Test-1 and Pokhran-Test-2 are briefly described to manifest the outline of Indian nuclear programs implemented in the Indian territory. In this 21st century of 3rd millennium, …
Published in Journal of Nuclear Engineering & Technology · Vol. 7, Issue 2, 2017 · pp. 4–11 Read article
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From 2D to 3D: An Evidence Based Review of 3D Printing in Dentistry
Abstract: Additive manufacturing, the technology popularly known as “3D printing” is the process of making any 3 dimensional solid objects from a digital model. This technology has revolutionized the process of manufacturing and has enumerable applications in automotive, aerospace and defense industries. Recently it has found application in medicine and dentistry where customized prosthesis is desired for every patient. 3D printing is valuable aid in orthognathic surgery, implantology, prosthetics and even …
Published in Research and Reviews: A Journal of Dentistry · Vol. 8, Issue 3, 2017 · pp. 1–6 Read article
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Negative Pressure Wound Therapy and Intermittent Irrigation with Systemic Antibiotic Suppression followed by One-stage Revision in Delayed Periprosthetic Hip Infection Cases: Reinfection Rate
Abstract: Background: Success rate of one-stage revision remains controversial in patients with delayed periprosthetic joint infection after primary cementless hip arthroplasty. We evaluated the reinfection-free efficacy of negative-pressure wound therapy (NPWT) and intermittent pulsatile irrigation (IPR) using chlorhexidine/povidone iodide combined with systemic antibiotic suppression (SAS) followed by one-stage exchange procedure with NPWT in those patients. Materials and Method: Reinfection rate was assessed in randomly selected forty-two cases (group A) with NPWT-IPR-SAS …
Published in Research and Reviews : Journal of Surgery · Vol. 11, Issue 2, 2022 · pp. 7–15 Read article
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Chemical Synthesis, Spectral Characterization and Electrical Conductivity Behavior of Poly(2-Methoxyaniline-Co-2-Chloroaniline) and its CuO Nanocomposite and Polypropylene Glycol Blend
Abstract: AbstractCopolymerization of 2-chloro aniline and 2-methoxy aniline was achieved chemically by oxidative polymerization technique using ammonium persulphate as the oxidizing agent in acidic medium in the presence of sodium lauryl sulphate, an anionic surfactant. Copolymerization was also carried out in the absence of the surfactant to study the effect of surfactant on the thermal stability and electrical conductivity. The copolymer composite with CuO nano particles and blend with poly propylene …
Published in Journal of Polymer & Composites · Vol. 6, Issue 3, 2018 · pp. 1–13 Read article
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Investigation of Residual Stress, and corrosion behavior of AA6082/Al 2 O 3 /C/ Si 3 N 4 Composite Material
Abstract: The main objective of the current study was to create AA6082/ Al2O3/C/Si3N4 Composite Material by the use of stir casting. The properties of the AA6082/ Al2O3/C/ Si3N4 Composite Material shown a significant improvement, with a micro-hardness rise of 13.5% and a residual stress decrease of 60%. As the testing parameters were increased, the residual stress of the AA6082/ Al2O3/C/ Si3N4 Composite Material rapidly decreased from -65MPa to -15MPa. An electromagnetic …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1104–1109 Read article
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Synthesis and Study of Photoluminescence properties of Sm3+ activated 7TiO2 + 3Al2O3 + (60-x)B2 O3 +xY+ 5LiCO3 +25SrCO3 Borate Glass for SSL Applications
Abstract: Melt quenching was used to successfully create the raddish orange light-emitting Sm3+activated 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 (X=0.001, 0.002, 0.005, 0.01 and 0.02, Y=Sm3+) borate glass. XRD examination confirmed the phase of the prepared Un-doped and Doped 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 glass. Its PL characteristics under ultraviolet (UV) light (302-468 nm) were later studied. At 602 nm, the excitation was detected, and at 402 nm, the emission. …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 55–60 Read article
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Caries-Preventive Effects of Self-Applied Subacidic 0.5% NaF-HF Gel via Toothbrushing in 7–8-Year-Old Schoolchildren: A Randomized Controlled Clinical Trial
Abstract: To assess the caries-preventive effectiveness of self-applied subacidic 0.5% sodium fluoride–hydrofluoric acid (NaF-HF) gel used during toothbrushing in children aged 7–8 years Objective: To assess the caries-preventive effectiveness of self-applied subacidic 0.5% sodium fluoride–hydrofluoric acid (NaF-HF) gel used during toothbrushing in children aged 7–8 years. Methods: This 1-year, multi-arm, double-blind, placebo-controlled, parallel-group randomized study evaluated the caries-preventive efficacy of self-applied 0.5% NaF-HF gel among primary schoolchildren. A total of 1200 …
Published in Research and Reviews: A Journal of Dentistry · Vol. 17, Issue 1, 2026 · pp. 14–19 Read article
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Lithium Induces Lower Specific Activity and Expression of Acetylcholinesterase in Old Aged Rats Brain and Liver for the Regulation of Acetyl Choline Cellular Signaling
Abstract: Acetylcholinesterase (AChE) acts on acetylcholine (ACh) to terminate its actions on the synaptic cleft by cleaving Ach to choline and acetate. This directly correlates with memory dysfunction and loss of cognitive functions in Alzheimer’s disease (AD) patients which was a continuous decline of the cholinergic neurotransmission in cortical and other regions of human brain. Specific activity and expression for AChEwere determined in LiCl2 treated young and old male wistar rat's …
Published in Research and Reviews: A Journal of Neuroscience · Vol. 8, Issue 2, 2018 · pp. 1–12 Read article
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Synthesis, spectroscopic, crystal structure, Hirshfeld surface, computational, and biological investigations on Isophorone derivatives: 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one
Abstract: FT-IR, 1H NMR, and 13C NMR spectroscopy were among the spectroscopic methods used to synthesize and analyze 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one, a new isophorone derivative. Single-crystal X-ray diffraction (SCXRD) was used to determine the crystal structure, which showed that the molecule crystallizes in a monoclinic system (space group P121/c1) with packing configurations and intermolecular interactions. To learn more about the non-covalent interactions influencing the crystal packing, Hirshfeld surface analysis was used. In order …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 2, 2025 · pp. 51–69 Read article
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25 Gbps Downstream, 3 Gbps Upstream, 20 Km Reach PON Using Duobinary Modulation Based on Reflective-ONU Utilizing R-SOA for Remodulation
Abstract: AbstractThe paper demonstrates 3 Gbps upstream transmission, 25 Gbps of downstream transmission of a single channel PON over 20 Km utilizing the wavelength reuse scheme using R-SOA in the ONU. NRZ and duobinary modulation scheme is considered and compared and the duobinary modulation scheme is selected for its better performance.Keywords: Reflective semiconductor optical amplifier, Passive Optical Network (PON), duobinary modulation, fiber to the x (FTTx)
Published in Trends in Opto-electro & Optical Communication · Vol. 4, Issue 3, 2014 · pp. 1–7 Read article
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A Comparative Study of the Structure–Property Relationships in CAD/CAM Milled vs. 3D-Printed High-Performance Polymers: Impact of Molecular Orientation on Abrasive-Wear Resistance
Abstract: Background: The transition from subtractive to additive manufacturing in prosthetic dentistry has introduced significant variations in the macromolecular architecture of high-performance polymers. While CAD/CAM milling utilizes high-density, industrially polymerized blocks, 3D printing (Additive Manufacturing) relies on layer-by-layer deposition, which may induce anisotropic molecular orientation. This retrospective study investigates how these distinct manufacturing “thermal histories” influence the long-term abrasive-wear resistance of PEEK and PEKK restorations. Materials and Methods: Data were retrospectively …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 133–140 Read article
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Synthesis of new heterocyclic compounds containing nitrogen, sulphur and study their biological activity
Abstract: Several substituted pyridines with brominated coumarin and with other substituents were achieved by condensing brominated coumarin IV with 4-methoxybenzaldehyde in basic solution forming α,β-unsaturated ketone II. Hantzsch reaction of this ketone with β-ketoester to provide precursor substituted pyridines. The Hantzsch reaction product was subjected to different reactions. The other targeted heterocyclic compound was obtained by reaction of α,β-unsaturated ketone II with hydrazine carbothioamide to give substituted pyrazole with brominated coumarin, …
Published in Emerging Trends in Chemical Engineering · Vol. 8, Issue 3, 2021 · pp. 8–16 Read article
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Effect of 2D-EBG Structure on Monopole Antenna Radiation and Analysis of Its Characteristics
Abstract: In this paper, we present a two dimensional electromagnetic (2D-EBG) square shaped mushroom structure placed between two monopole antennas. Two artificial properties of this 2D-EBG structure such as PMC and Band Reject Region are investigated here. The radiation characteristics of a monopole antenna over this, 2D-EBG structure is tested by considering two cases. In the first case monopole antenna is made to operate within band rejection region where as in …
Published in Journal of Microwave Engineering and Technologies · Vol. 2, Issue 2, 2015 · pp. 1–4 Read article
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Design of Booth Encoded Multi-Modulus {2n-1, 2n, 2n+1} RNS Multiplier
Abstract: Multiplication, a very important arithmetic operation, is finding a great use these days in various applications (especially DSP, multimedia and image processing). Due to advances in technology and increasing needs for high-speed calculations, it has become really necessary and important to design a fast efficient multiplier. A productive method to speed up the multiplication is reduction in the Partial Product (PP) array. In this paper, the design of 8, 16 …
Published in Journal of VLSI Design Tools and Technology · Vol. 6, Issue 3, 2016 · pp. 7–14 Read article
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A Study on Role of Pharmacist in Providing Advanced Patient Counseling in Medication Usage in General Medicine Department of an ESI Hospital
Abstract: Aim: The present study aims at the implementation of pharmacist services in providing advanced patient counselling in medication usage in the general medicine department of an ESI hospital. Objectives: The key objectives of the study include Improving Patient safety initiatives, improving Patient health related outcomes, reducing work burden of Physicians and nurses, providing knowledge on medication usage. Methodology: (1) Study Design: It is a Prospective and observational study. (2) Study …
Published in Research and Reviews: A Journal of Medicine · Vol. 9, Issue 1, 2019 · pp. 1–8 Read article
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Synthesis and Characterization of VO 2+ doped SrMg 2 (PO 4 ) 2 Nanopowder by Solid State Reaction technique suitable for White LED material
Abstract: VO2+ doped SrMg2(PO4)2 nanopowder was synthesized by using solid state reaction (SSR) technique. Various experimental techniques have been performed on prepared sample. XRD analysis has revealed that prepared nanopowder is in monoclinic phase. The average crystallite size, micro strain and dislocation density evaluated and make an analogy with W-H plot method. SEM micrographs shows that agglomerated stone like structure and EDS spectrum shows elemental compositions of synthesized sample. FTIR spectrum …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 95–110 Read article
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Ceria and Modified Ceria: A Reusable Catalyst for the Green Synthesis of 2,3-diphenyl Quinoxaline at Room Temperature
Abstract: Simple, highly versatile and efficient synthesis of 2,3-diphenylquinoxalines is achieved from benzil and o-phenylene diamine using ceria and modified ceria as the catalyst. Modification of ceria is done using different weight percentage of zirconia. The catalysts are characterized by XRD, FT-IR, BET surface area, TGA and EDX-SEM. The advantages of this method are short reaction times, milder conditions and easy work-up. The product could be separated from the heterogeneous catalyst …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 3, 2014 · pp. 1–11 Read article