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240 articles for “and XRD”
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EFFECT OF CALCINATION CONDITION AND COOLING METHOD ON REACTIVITY OF LIME SLUDGE
Abstract: In this Experimental Study, Raw Lime sludge from the Paper industry was characterized by XRD and TGA techniques. Lime Sludge was calcined for a temperature range of 550–7500C for 2 h and cooled by air cooling. The effect of calcination temperature on the reactivity of resultant Sludge was investigated by various indirect and direct methods of pozzolanic activity assessment such as the Strength Activity Test(SAI), Lime reactivity test, XRD, TGA, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 10, 2023 · pp. 36–48 Read article
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Influence of Agitation and Static Cultivation on Physicochemical Characteristics of Bacterial Cellulose Produced by Gluconacetobacterliquefaciens MTCC 3135
Abstract: Bacterial cellulose (BC) a with applications spanning biomedical, food, paper, electronics, and diverse industrial processes. Its unique properties include high purity, biocompatibility, and flexibility. BC is a versatile natural biopolymeric material, secreted by certain acetic acid bacteria. BC has numerous benefits over plant cellulose due to distinctive features, e.g., higher polymerization degree and purity, superior crystalline structure, water retention, biocompatibility, and biodegradability, which make BC a valuable material in creating …
Published in Research and Reviews : A Journal of Biotechnology · Vol. 14, Issue 2, 2024 · pp. 1–11 Read article
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Synthesis and Functional Group Analysis of Solution Processed Zinc Oxide Thin Film Grown on Polyethylene Terephthalate
Abstract: Flexible electronics field is growing every day. Existing technology is facing issues like brittleness, toxicity, inadequacy. Fabrication cost increases in processing of such materials. In this work, zinc oxide nanoparticles synthesized by solution processing technique were used to grow 120nm thick thin film (TF) on Polyethylene terephthalate (PET). This method reduces the processing cost and Zinc Oxide (ZnO) is cheaper and abundant in comparison to other semiconductors option. Material was …
Published in Journal of Polymer & Composites · Vol. 12, Issue 3, 2024 · pp. 56–66 Read article
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Tb3+ activated Boro Phosphate Glass: Synthesis and Photoluminescence (PL) Characteristics
Abstract: The (40B2O3+ 3Al2O3+(10-x) P2O5 + xTb + 7ZnO+5LiCO3+ 10H6NO4P+25SrCO3) boro phosphate glass was successfully synthesized via melt quenching method. The structural confirmation is supported with X-ray diffraction (XRD) data and surface morphology was defined by scanning electron microscope (SEM). The (40B2O3+ 3Al2O3+(10-x) P2O5 + xTb+ 7ZnO+5LiCO3+ 10H6NO4P+25SrCO3) boro phosphate glass has been investigated for its Photoluminescence (PL) under UV excitation. At 544 nm, the excitation was observed, and at 222 …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 43–47 Read article
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SYNTHESIS AND CHARACTERIZATION OF Mn2+ DOPED LiPbX3(X = Cl, Br, I)
Abstract: In this paper the structural, electronic and optical properties of Mn doped Pb based cubic perovskites LiPbX3(X= Cl, Br and I) were studied by wet chemical method (sol gel method). For Mn doped LiPbX3(X= Cl, Br and I) NCs, MnCl2 and PbBr2 were added in molar feed ratio 1.35 mole% and nan crystal were examine with the help of TEM and their structure were confirmed by X-ray diffraction (XRD). Additionally, …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 48–54 Read article
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Eu3+/Gd3+ doubly doped ions in SrCO3-Al2O3-B2O3-SiO2 glasses for optical and White light applications
Abstract: The present work deals with the optical analysis of SrCO3-Al2O3-B2O3-SiO2 glass materials doubly doped with Eu3+/Gd3+ ion were prepared by melt quenching technique. These are studied by XRD, physical properties, FITIR, optical absorption and luminescence spectroscopy. The XRD measurements are conducted to verify the amorphous form of prepared material and structural modifications can be explained by the FTIR spectra. The thermal stability of the glass matrix is measured by the …
Published in Journal of Semiconductor Devices and Circuits · Vol. 11, Issue 2, 2024 Read article
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Characterization Of Senna Occidentalis (Link.) Seed Extract
Abstract: Senna occidentalis (L.) Link commonly known as "coffee senna" or majamfari/rai dore in Hausa is a plant with a long history of traditional and medicinal uses against diseases such as inflammation, pains, and diabetes. This study presents characterization of the bioactive compounds of the seed extracts. Physicochemical analysis of seed powder was carried out following standard procedures. Qualitative phyto-chemical contents were determined for the presence and absence of major metabolites. …
Published in Research & Reviews : Journal of Botany · Vol. 13, Issue 3, 2024 · pp. 13–22 Read article
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Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article
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Synthesis of Lawsonia Inermis (Henna) Carbon Supported AgO Nanocomposite, Characterizations and Photocatalytic Activity Studies
Abstract: Synthesis of Carbon supported AgO nanocomposite is reported for first time. Henna carbon was successfully synthesized from henna leaf. Bare AgO and C-AgO nanocomposites are effectively made using precipitation method. The synthesised composites structural, morphological, and optical properties are assessed using FT-IR, XRD, FE-SEM, UV-DRS, and PL techniques. FT-IR analysis proved that specific functional groups of synthesized materials. The uniform distribution of the composites is revealed in the FE-SEM. XRD …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 749–760 Read article
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Synthesis and Study of Photoluminescence properties of Sm3+ activated 7TiO2 + 3Al2O3 + (60-x)B2 O3 +xY+ 5LiCO3 +25SrCO3 Borate Glass for SSL Applications
Abstract: Melt quenching was used to successfully create the raddish orange light-emitting Sm3+activated 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 (X=0.001, 0.002, 0.005, 0.01 and 0.02, Y=Sm3+) borate glass. XRD examination confirmed the phase of the prepared Un-doped and Doped 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 glass. Its PL characteristics under ultraviolet (UV) light (302-468 nm) were later studied. At 602 nm, the excitation was detected, and at 402 nm, the emission. …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 55–60 Read article
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Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article
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Substitution of La3+ in Cu0.5Co0.5 LaxFe2-x O4 (x=0.02, 0.06) spinel ferrites improves the structural and dielectric Properties
Abstract: Nanosized Spinel ferrites with composition Cu0.5Co0.5 LaxFe2-x O4 (x=0.2, 0.6) synthesized by Sol-Gel auto Combustion method. The prepared sample was calcinated at 8000c for 4 hours. The substitution of La3+ effects the structural parameters, which is characterized by X-ray diffraction (XRD). The X-rd analysis shows that the crystallite size is 34.609 nm for 0.02 and 38.994 nm for 0.06 was calculated by using Debye-Scherrer’s formula. dislocation density shows at value …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 45–48 Read article
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Solid acidity of MoO3 synthesized by solution combustion method and acetalization of formaldehyde using it
Abstract: MoO 3 nanoparticles were synthesized via solution combustion approach. Ammonium nitrate was used as oxidant and ammonium molybdate as fuel in combustion reaction. XRD, FTIR and Raman spectroscopy results showed that MoO 3 nanoparticles were successfully synthesized by the solution combustion reaction. The SEM analysis showed that synthesized MoO 3 nanoparticles have rod-like shape with width and thickness of 50-200nm and length of 0.2-1μm, respectively. The XRD pattern and morphology …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 3, 2025 · pp. 01–09 Read article
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Evaluate The Engineering Properties of Low Load-Carrying Capacity of Expansive Soil by Using Magnesium Chloride and Dry Leaf Ash Powder
Abstract: The swell-shrink behavior of expansive soils poses numerous challenges with the substructure and distress in infrastructures such as buildings, pavements, breast walls, etc. The behavior of expanding soil has been carefully examined by geotechnical engineers, who have then put adequate management techniques into place. Present investigation intends to investigate potential benefits of dry leaf ash (DLA) powder and magnesium chloride (MgCl2) to enhance geological characteristics of soil, particularly addressing problems …
Published in Journal of Geotechnical Engineering · Vol. 12, Issue 1, 2025 · pp. 33–45 Read article
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A Sol-Gel Approach for the Fabrication of Zinc Oxide Nanoparticles and Their Nanocomposite with Urea Formaldehyde (UF)
Abstract: In the performed work, zinc oxide nanoparticles were synthesized via the sol-gel method using zinc sulphate as the precursor material. Urea-formaldehyde (UF) resin was employed as a polymer matrix to encapsulate the produced ZnO through an acid-catalyzed polymerization process. This encapsulation aimed to improve the dispersion stability and surface reactivity of ZnO within the polymeric medium. The synthesized materials were subjected to comprehensive characterization using Fourier Transform Infrared Spectroscopy (FT-IR), …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 21–27 Read article
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Growth, Structural and Optical characteristics of Citric Acid Doped Copper Sulphate Single Crystals Polymer Composites Photonic Applications
Abstract: The organic material Citric Acid doped Copper Sulphate single crystals (CACS) was synthesized and single crystal was grown by slow evaporation method. The incorporation of citric acid, an organic compound, introduces polymer-like functional behavior into the crystal matrix, forming an organic-inorganic hybrid composite with enhanced optical and structural characteristics. Single crystal XRD confirmed the triclinic system with unit cell parameters: a = 5.96 Å, b = 6.11 Å, c = …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 482–488 Read article
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Optimization of Direct Ink Writing Process Parameters for Liquid Silicone Rubber/TiO2 Composite Ink
Abstract: The purpose of this research is to develop and optimize the Liquid Silicone Rubber (LSR)/Titanium Dioxide (TiO₂) composite inks in Direct Ink Writing (DIW)-based 3D printing systems. The primary research objective was to use enhancement of mechanical, rheological, and dielectric characteristics of LSR using TiO₂ reinforcement but still retain extrusion stability and dimensional consistency. TiO₂ content (0, 5, 10, and 15 wt%) and catalyst and glycerol ratios were regulated and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 240–259 Read article
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Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 45–59 Read article
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Turning the Properties of Wastes Paper-Derived Cellulose Nanocrystals for Enhanced Erythromycin Adsorption
Abstract: This study explores the modification, characterization, and adsorption performance of waste paper-derived cellulose nanocrystals (CNCs) for the removal of erythromycin from aqueous solutions. CNCs were modified using organic acid, inorganic acid, and base treatments, and their structural changes were evaluated using FTIR, XRD, and BET analysis. FTIR confirmed the introduction of carboxyl and hydroxyl groups in acid-treated CNCs and deprotonation effects in base-treated CNCs. XRD analysis revealed that organic acid …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 1–24 Read article