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116 articles for “IR spectroscopy”
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Photonic Diagnostics: Harnessing Optical Sensing for Non-Invasive Assessment of Coronary Obstruction
Abstract: Cardiovascular diseases (CVDs) remain the leading cause of mortality globally, with coronary artery blockages primarily atherosclerosis representing a critical challenge. The gold standard for diagnosing coronary artery disease remains invasive coronary angiography, a procedure that, while precise, carries inherent patient risks, high costs, and logistical burdens. Optical sensors, leveraging the principles of light-tissue interaction, offer real-time, high-resolution insights into vascular health, paving the way for early detection of arterial stenoses …
Published in International Journal of Optical Innovations & Research · Vol. 4, Issue 1, 2026 · pp. 25–30 Read article
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A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
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Sustainable Innovations in Green Nanotechnology for Nanoparticle Synthesis
Abstract: Green nanotechnology is an emerging field that focuses on the environmentally friendly production of nanoparticles through biological and sustainable processes. This approach has diverse applications across industries such as pharmaceuticals, energy, electronics, and bioengineering. Compared to conventional methods, biologically driven nanoparticle synthesis, particularly utilizing green chemistry principles, offers a safer, eco- friendly, non-toxic, and cost-effective alternative. Metal nanoparticles are commonly synthesized through top-down and bottom-up strategies using physical, chemical, and …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 1, 2025 · pp. 31–37 Read article
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A Sol-Gel Approach for the Fabrication of Zinc Oxide Nanoparticles and Their Nanocomposite with Urea Formaldehyde (UF)
Abstract: In the performed work, zinc oxide nanoparticles were synthesized via the sol-gel method using zinc sulphate as the precursor material. Urea-formaldehyde (UF) resin was employed as a polymer matrix to encapsulate the produced ZnO through an acid-catalyzed polymerization process. This encapsulation aimed to improve the dispersion stability and surface reactivity of ZnO within the polymeric medium. The synthesized materials were subjected to comprehensive characterization using Fourier Transform Infrared Spectroscopy (FT-IR), …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 21–27 Read article
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Synthesis, Characterization of New Imidazolidin-4-One Containing Azo Compound Derived from Acetylacetone as Antibacterial and Antioxidant Agents
Abstract: In the present study, new derivatives of imidazolidine-4-one was prepared. Which involved reactions to diazonium salt of o-methoxy aniline with acetylacetone in the presence of sodium hydroxide, and isolating the azo compound as a brown precipitate. The azo diketone reacts efficiently with aromatic amine derivatives to produce Schiff bases as a light yellow and dark brown precipitates, and from this Schiff bases three derivatives of imidazolidine-4-one was prepared by reacting …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 94–114 Read article
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Design, Synthesis, and in vitro Evaluation of Novel Benz/Imidazole-2-acetonitrile Derivatives as Antibacterial and Antifungal Agents
Abstract: Benzimidazole is a pharmaceutically important compound. In this research, we were able to prepare several heterocyclic derivatives from it by first preparing a new azo derivative ZH through a reaction of 3-aminoacetophenone with benzimidazole-2-acetonitrile. This azo derivative was then introduced via a condensation reaction with aromatic amine derivatives, resulting in the preparation of two Schiff base derivatives Z1 and Z2. From these bases, six and seven membered heterocyclic derivatives were …
Published in Emerging Trends in Chemical Engineering · Vol. 13, Issue 2, 2026 · pp. 53–87 Read article
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To explore the effect of polyethylene glycol additive on mechanical and gas permeation properties of polyvinyl alcohol membranes
Abstract: Polyvinyl alcohol (PVA) membranes were prepared by solution casting and blended with Polyethylene glycol (PEG) in de-ionized water which led to the formation of porous and flexible membranes. Extensive experimentation were performed, in order to find out that at what composition of PEG pores will be generated in the PVA membranes. The PVA polymer is a hard and crystalline thermoplastic so high concentrations of PEG were used, i.e. 40 wt%, …
Published in Journal of Polymer & Composites · Vol. 7, Issue 1, 2019 · pp. 27–33 Read article
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Fabrication, Interfacial Characterization, and Superparamagnetic Properties of Fe₃O₄@γ-Fe₂O₃ Core/Shell Nanoparticle-Reinforced Chitosan Biopolymer Composites
Abstract: Magnetite/maghemite core/shell nanoparticles were prepared by alkaline co-precipitation of Fe(II) and Fe(III) precursors followed by controlled thermal oxidation at 350 °C and subsequently incorporated into chitosan at 1, 3, and 5 wt% loadings by solution casting. The resulting films were evaluated by X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), high-resolution transmission electron microscopy (HR-TEM), vibrating-sample magnetometry (VSM), thermogravimetric analysis (TGA), and tensile testing. XRD showed the characteristic cubic spinel reflections …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article
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Preparation and Characterization of Microwave-assisted Candesartan Cilexetil Solid Dispersions
Abstract: The aim of the present study was to enhance the solubility & dissolution rate of a poorly soluble, BCS class II drug candesartan cilexetil (CC), using its solid dispersions (SDs) with polyethylene glycol (PEG) 6000 & hydroxypropyl methylcellulose (HPMC) E5. Solid dispersions were prepared by melting, solvent evaporation & microwave method. The dispersions were evaluated for various in vitro parameters such as solubility study, dissolution study, fourier transform infrared spectroscopy …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 4, Issue 3, 2013 · pp. 9–19 Read article
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Biosynthesis, Characterization and Antibacterial Studies of Silver Nanoparticles from Tamil Nadu Major Crop Anacardium occidentale
Abstract: Recent studies have shown that Silver Nanoparticles have physical, optical and catalytic properties. Present work involves the eco-friendly and reproducible synthesis of Silver Nanoparticles from the Anacardium occidentale leaves extract. The synthesized silver Nanoparticle from 1 mM AgNO3 solution through the leaf extract were characterizing was monitored using Ultraviolet-visible (UV-vis) spectrophotometer, Scanning electron microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray powder diffraction (XRD) and Fourier transform infra-red spectroscopy (FT-IR).Scanning …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 20, Issue 3, 2018 · pp. 13–22 Read article
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Synthesis of Silver Nanoparticles from Pseuderanthemum malabaricum and Evaluation of Anticancer Activity
Abstract: The present study was focused on eco-friendly and green approach synthesis of silver nanoparticles using plant extracts of P. malabaricum. The morphological and physical properties of synthesized silver nanoparticles were analyzed using various spectroscopic and microscopic studies such as UV visible spectroscopy, FT-IR, XRD, SEM with EDAX, DLS, Zeta potential and Particle size analyzer. After structural characterization, the synthesized silver nanoparticles were subjected to anti-cancer activity studies against cervical cancer …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 2, 2019 · pp. 31–40 Read article
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Hydrothermal synthesis of ZnS for efficient photodegradation of Malachite green
Abstract: In this work, ZnS nanoparticles were prepared by hydrothermal method. Various characterization techniques such as X-ray diffraction (XRD), UV-visible optical spectroscopy and FT-IR spectra were used to study the structural, composition and optical properties of synthesized nanoparticles. The XRD pattern showed that the prepared ZnS nanoparticles have a cubic zinc blende structure. The band gap is calculated from absorption spectra with the help of Taucplot and is found to be …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 10, Issue 1, 2020 · pp. 11–15 Read article
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Comparative Study of Extraction and Characterization of Chitosan by Chemical and Biological Method from the Crab Shell Waste and Analyzing its Anticancer Activity
Abstract: Crab shell waste causes environmental pollution, So it is in need to process the waste into useful chitosan The crab shell waste act as an alternative for chitosan production The chitosan molecule appears to be a suitable polymeric complex for many biomedical applications. Chitosan is an amino polysaccharide and a versatile, natural polysaccharide. The specific objective of this study is to compare chitosan from the exoskeleton of freshwater crab obtained …
Published in Research and Reviews : Journal of Veterinary Science and Technology · Vol. 8, Issue 1, 2019 · pp. 22–32 Read article
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Synthesis and Spectral Characterization of Complexes Tin(II) With 4-Nitrophenol
Abstract: Tin(II)4-nitrophenoxide complexes with the formulas SnCl(OC₆H₄NO₂-4) and Sn(OC₆H₄NO₂-4)₂ were prepared through the reaction of stannous chloride (SnCl₂) with 4-nitrophenol (HOC₆H₄NO₂-4) in 1:1 and 1:2 molar ratios, respectively. The reaction was performed in tetrahydrofuran (THF) with diethylamine serving as the base. The resulting compounds were characterized through elemental analysis, determination of molecular weight, molar conductance measurements, and spectroscopic methods including IR and ¹H NMR spectroscopy. Current investigations are directed toward assessing …
Published in International Journal of Advance in Molecular Engineering · Vol. 4, Issue 1, 2026 · pp. 22–26 Read article
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Design, Synthesis, and Evaluation of Novel Quinazoline Derivatives as Anti-Inflammatory Agents
Abstract: Novel quinazoline derivatives are well-known heterocyclic scaffolds that are renowned for having a wide range of biological functions. A new quinazoline derivative was synthesized from anthranilic acid through a multi-step sequence involving amide formation, cyclization, and aromatic group substitution. The structure of the methoxy- and chloro-substituted final compound was confirmed by IR and 1H NMR spectroscopy. Evaluation of synthesized molecules anti-inflammatory activity using paw edema caused by carrageenan paradigm in …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 13, Issue 1, 2026 · pp. 01–09 Read article
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Swift heavy Ion Irradiation Effects on Structural and Spectroscopic Properties of Nanocomposites of Polypyrrole Nanotubes and Silver Nanoparticles
Abstract: Polypyrrole nanotubes-silver nanoparticle nanocomposites (PPy-NTs:Ag-NPs) have been synthesized by in-situ reduction of silver nitrate (AgNO3) to suppress the agglomeration of Ag-NPs. The synthesized nanocomposite has been irradiated with 100 MeV Si9+ ion beam. The structural and spectroscopic properties of the nanocomposites after irradiation have been studied by SEM, XRD, Raman and UV-vis spectroscopy. Decrease in size of the nanotubes has been observed from SEM micrographs due to swift heavy ion …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 8, Issue 2, 2018 · pp. 1–6 Read article
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Nanostructure-Induced Thermoelectric Enhancement in Bi₂Te₃ Nanorods Design, Analysis, and Performance Evaluation
Abstract: Thermoelectric materials capable of efficient energy conversion near room temperature are critical for waste heat recovery applications. In this work, solution-grown Bi₂Te₃ nanorods were synthesized via a trioctylphosphine-assisted thermal decomposition route, and the influence of surfactant-induced nanostructuring on their thermoelectric properties was systematically investigated. Structural analysis using X-ray diffraction and Rietveld refinement confirmed the formation of rhombohedral Bi₂Te₃ with the emergence of Bi₂Te₃–BiTe nanocomposites at higher surfactant concentrations. Electron microscopy …
Published in International Journal of Energy and Thermal Applications · Vol. 4, Issue 1, 2026 · pp. 34–44 Read article
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Identification of Some Imported Lubricating Oil Additives Used in Libya and Synthesis of the Most Consumed Ones from the Local Raw Materials
Abstract: This paper presents the identified six additives imported under trade names used in the lubricating oil blending factory of A-Zawia-Libya. Their structures have been completely confirmed by examining their physical properties and using modern analytical techniques such as nuclear magnetic resonance spectroscopy (NMR), infra-red (IR), atomic absorption (AAS) and gas chromatography (GC). The synthesis of most important and more consumed additives in lubricating oils in Libyan oil industry from local …
Published in Journal of Catalyst & Catalysis · Vol. 3, Issue 3, 2016 · pp. 10–17 Read article
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Nanostructure-Induced Thermoelectric Enhancement in Bi2Te3 Nanorod Design, Analysis, and Performance Evaluation
Abstract: Thermoelectric materials capable of efficient energy conversion near room temperature are critical for waste heat recovery applications. In this work, solution-grown Bi2Te3 nanorods were synthesized via a trioctylphosphine-assisted thermal decomposition route, and the influence of surfactant-induced nanostructuring on their thermoelectric properties was systematically investigated. Structural analysis using X-ray diffraction and Rietveld refinement confirmed the formation of rhombohedral Bi2Te3 with the emergence of Bi2Te3–BiTe nanocomposites at higher surfactant concentrations. Electron microscopy …
Published in Research & Reviews : Journal of Physics · Vol. 15, Issue 2, 2026 · pp. 26–37 Read article
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Synthesis, Characterization of MoS2 Nanosheets, Amorphous Carbon Nanotube (ACNT) and ACNT-MoS2 Nanohybrids: A Comparative Research Analysis
Abstract: The superior properties of graphene and its applications in several fields like sensor, electronics, etc have inspired the researchers to concentrate on other 2D material and their hybrids. Among them, MoS2 nanosheets has gain research interest due to its amazing electronic, optical and physical properties. Due to all these properties, MoS2 nanosheets are used in numerous applications such as catalysis, photo emitting diode, double layer capacitors, lithium-ion batteries, etc. Here, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 3, 2019 · pp. 27–36 Read article