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277 articles for “Spectroscopic methods.”
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Recent Advances in Crystal Defect Engineering of Semiconductor Photocatalysts for Sustainable Environmental and Energy Applications
Abstract: Semiconductor photocatalysis has emerged as one of the most promising green technologies for addressing environmental pollution and global energy challenges through solar energy utilization. Nevertheless, the practical application of conventional semiconductor photocatalysts is often limited by their narrow visible-light absorption, rapid recombination of photogenerated electron–hole pairs, insufficient active sites, and poor charge-transfer efficiency. Defect engineering has recently attracted significant attention as an effective strategy to overcome these limitations by deliberately …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 4, Issue 2, 2026 Read article
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Effect of the Annealing Temperature on CdS Nanoparticles Synthesized by Chemical Precipitation Technique and also Characterized for its Potential Technological Applications
Abstract: Cadmium Sulfide (CdS) nano particles are synthesized by chemical precipitation method. Cadmium Chloride and Thiourea are used as the precursor materials. Ammonia water & distilled water are used as solvent. The samples are annealed at 100°C, 300°C and 500°C for 1 hour. Transmission electron microscopy (TEM), Energy–dispersive X-ray spectroscopy (EDAX), and X-ray diffraction pattern (XRD) are used to study the morphologies, distribution, and crystallinity of the CdS nanoparticles and to …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 23, Issue 3, 2021 · pp. 20–28 Read article
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Detection and Killing of Food Poisoning Salmonella Typhimurium in Cheese by Using Monoclonal Antibody and Nanoparticles Complex
Abstract: Present studies were conducted to test the ability of gold nanoparticles (GNPs) to detect and kill the bacterial contaminated food samples like cheese. The GNPs were prepared in two methods, sample A was purple 72 to 78.3 nm, while sample B was wine-red and the size was 51.5 to 58 nm. The results obtained suggest that the GNPs were synthesized with different particle size. UV-VIS spectroscopy and zeta potential tests …
Published in Research & Reviews : Journal of Food Science & Technology · Vol. 5, Issue 1, 2016 · pp. 1–10 Read article
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Development and Characterization of a Solid Dispersion of an Anti-Diabetic Drug Using Pectin as a Natural Polymer
Abstract: Aim: The current study sought to improve the solubility and oral bioavailability of gliclazide by creating solid dispersions and oral dispersible tablets (ODTs) with enhanced physicochemical characteristics and maintained antidiabetic action. Methods: Preformulation studies were conducted to evaluate the physicochemical properties of gliclazide, including physical appearance, melting point, solubility, and partition coefficient. Solid dispersions were prepared using hydrophilic carriers-pectin and PVP K30, and subsequently characterized by Fourier Transform Infrared Spectroscopy …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 17, Issue 2, 2026 · pp. 01–12 Read article
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Preparation, Characterization and Electrical Conductivity of Chitosan-C 30B/MWCNT Nanocomposite Films
Abstract: In this research programme organoclay clay Cloisite 30B (C 30B) and Multi walled carbon nanotubes (MWCNTs) were successfully blended with the biopolymer Chitosan (CS). The polymer nanocomposites were characterised by various techniques like Fourier Transmission Infrared spectroscopy (FTIR), X-ray Diffraction (XRD) and Scanning Electron Microscope (SEM). From the results it was found that intercalation or nearly exfoliation has been occurred between the polymer and the clay. Electrical conductivity was also …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 18, Issue 3, 2016 · pp. 1–4 Read article
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Comparative Study of Structural and Ionic Properties of Doped Zirconia Electrolytes for Solid Oxide Fuel Cells
Abstract: The current study looks at yttria and scandia doped zirconia electrolytes for application in solid oxide fuel cells. Samples with (i) 10 mol% yttria, (ii) 5 mol% yttria and 5 mol% scandia, and (iii) 10 mol% scandia in zirconia host lattice were prepared by mixed oxide method and were sintered by conventional heating at 1400°C for six hours. The samples were then analysed by X-ray diffraction (XRD) and scanning electron …
Published in Research & Reviews : Journal of Physics · Vol. 7, Issue 2, 2018 · pp. 1–7 Read article
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Recent Advances in Crystalline Materials
Abstract: Crystalline materials are solids in which atoms, ions, or molecules are arranged in a highly ordered, repeating three-dimensional lattice. This well-defined structure gives rise to unique physical, chemical, electrical, optical, thermal, and mechanical properties, making crystalline materials essential for numerous scientific and industrial applications. Advances in materials science, crystal engineering, and nanotechnology have enabled precise control over crystal size, morphology, composition, and defect structures through innovative synthesis techniques. These developments …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 2, 2026 · pp. 14–21 Read article
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Formulation and Evaluation of Transdermal Drug Delivery of Piroxicam
Abstract: The aim of the present study was to formulate transdermal films loaded with Piroxicam (PX). Transdermal films were prepared by using sodium alginate (SA) and xanthan gum (XG) as biopolymers by varying the blend ratios viz., 10:0, 8:2, 6:4, 4:6 and 2:8 (w/w %) through solution casting method. The drug loaded membranes were evaluated for thickness, tensile behaviours, and content uniformity. In-vitro diffusion was determined by Franz diffusion cell. Piroxicam …
Published in Trends in Drug Delivery · Vol. 1, Issue 2, 2014 · pp. 8–13 Read article
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Novel Poly (Methyl Cellulose-G-Acrylamide)/Sodium Alginate Based Zeolite 4A Filled Mixed Matrix Membranes for The Separation of Water-Isopropyl Alcohol Mixtures by Pervaporation
Abstract: The Filled blend matrix membranes of (Methyl Cellulose-g-Acryl amide)/Sodium Alginate {(MC-g-AAm)/NaAlg} prepared via solution casting method by in situ incorporation with 4A zeolite particles in 5, 10 and 15 mass % with respect to the weight of (MC-g-AAm)/NaAlg membrane. Several analytical tools such as scanning electron microscope (SEM), atomic force microscope (AFM), Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and thermo-gravimetric analysis (TGA) were …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 131–152 Read article
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A review of the reported technologies to segregate municipal solid waste into dry and wet waste based on their moisture content
Abstract: This paper deals with the various techniques used to segregate municipal solid waste based on its size and types. We study various research works and ongoing industry practices and finally summarize a general process that is being used to segregate municipal solid waste. This paper also addresses the major problem related to segregating waste as wet and dry and the existing technologies that are being used in industries to segregate …
Published in Journal of Geotechnical Engineering · Vol. 9, Issue 3, 2022 · pp. 27–36 Read article
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Techniques for Characterization of Anticancer Drug Loaded Polymeric Nanoparticles: A Review
Abstract: Normal 0 false false false EN-US X-NONE X-NONE Polymeric nanoparticles have been used for targeted drug delivery against different diseases during last decades. Particularly in cancer, targeted polymeric nanoparticles can be used to deliver anticancer drugs to cancer cells with reduced cytotoxicity and greater efficacy. Various natural polymers like chitosan, albumin, gelatin and synthetic such as Polylactides (PLA), Poly (Lactide co-Glycolides) (PLGA) have been researched as carrier of anticancer drugs. …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 2, 2015 · pp. 32–43 Read article
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Phytochemical Screening and Trace Element Analysis of Cryptomeria japonica
Abstract: The present study was aimed to investigate the preliminary phytochemical screening of the bark of Cryptomeria japonica belonging to family Cupressaceae. The bark of the plant were subjected to successive soxhlet extraction by continuous hot percolation method using organic solvents of increasing polarity such as ethanol. Both the extracts were subjected to qualitative phytochemical screening and it showed the presence of active constituents such as alkaloid, flavonoid, phenol and carbohydrates. …
Published in Research and Reviews : A Journal of Biotechnology · Vol. 4, Issue 2, 2014 · pp. 17–20 Read article
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A Mini-Review on Spectral (UV Visible, FT-IR, 1H NMR, GC-MS) Analysis of Various Shaded Dried Leaves Extracts
Abstract: To collect the different types of leaves in various places, wash collected leaves with distilled water and dried these leaves in various processes like under shade dry for 15 days, place oven (45 oC) for 1 hour. Grind well using the above-dried leaves, so these leaves are changed to powder form. Utilize these shaded dried leaves powder, to prepare extract with solvents like methanol, ethanol, hexane, carbon tetrachloride, petroleum ether, …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 13, Issue 1, 2022 · pp. 1–8 Read article
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Composite Fabrication by Stir-Cast for Al C355.0 With Particulates Hematite Reinforcements at Different Weight Percentages in Copper Chills with and Without Water Circulation for Mechanical and Fatigue Performance
Abstract: This study investigates the fabrication of aluminum matrix composites using the stir casting method to analyze the mechanical characterization and fatigue behavior of Al C355.0 composites reinforced with varying weight percentages of hematite particulates. The hematite content was systematically adjusted from 0 wt. % to 12 wt. % in 3 wt. % increments, with the presence of constituent elements confirmed through Energy Dispersive Spectroscopy (EDS). The incorporation of hematite reinforcement …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 324–336 Read article
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Fabrication and Comparative Study of Synthetic and Eggshell Waste Derived Hydroxyapatite-Based Composites for Biomedical Applications
Abstract: Hydroxyapatite is widely used as a bioceramic material in orthopedic and dental field because of its exceptional biocompatibility and bioactivity. Hydroxyapatite (HAp) doped with several mineral ions has been frequently reported to further enhance its bioactive nature. Several studies indicate that biological waste materials can serve as calcium sources for hydroxyapatite synthesis, with eggshells being one such promising source. In the present work, two types of hydroxyapatite were synthesized: pure …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 33–46 Read article
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Silver Nanoparticles Biosynthesis Using Grape Extract and Its Application in Photocatalytic Dye Degradation
Abstract: AbstractGrapes are known for its antioxidant properties. Aqueous grape extract is used in the current study as a reducing and stabilising agent in the production of silver nanoparticles. Silver nanoparticles were synthesized in single step method, at room temperature, under magnetic stirring without application of external energy. Silver nanoparticles are substantial for its application in numerous areas such as medicine, agriculture, food, chemical sector etc. Synthesis and optimization of silver …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 13, Issue 3, 2022 · pp. 1–8 Read article
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A Review on Synthesis and Characterisation of Nanoclusters
Abstract: Nanoclusters are materials with size less than 2 nm. Because of their small size and high surface area, they have properties which can be used for various applications like bio-sensing, catalysis, fuel cells etc. The synthesis techniques are carried out in such a way that the size-selection of nanoclusters take place. The synthesis methods discussed in this review include both top-down and bottom-up techniques. The different characterization techniques taken into …
Published in Emerging Trends in Chemical Engineering · Vol. 8, Issue 1, 2021 · pp. 1–19 Read article
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Antifungal Activity of Zero-valent Iron Nanoparticles Synthesized by Green Protocols Using Camellia sinensis Extract against Pathogenic Aspergillus Species
Abstract: Zero-valent iron nanoparticles with potential antifungal activity were synthesized following a green protocol using Camellia sinensis leaves extract. FeSO4.7H2O was reduced to black metallic iron by Camellia sinensis leaves extract. The green synthetic procedure without using any hazardous chemical reagents is hopeful which reduces the possibility of chemical pollution. The synthesized nanoparticles were characterized by UV/visible and fluorescence spectroscopies. The surface morphology, size, shape and particle distribution were studied using …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 8, Issue 3, 2017 · pp. 40–45 Read article
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Synthesis and Characterization of a Naphthalene-Derived Schiff Base for Fe³⁺ Sensing Applications
Abstract: The development of chemosensors for metal ions has gained significant attention due to their crucial role in industrial, environmental, and biological applications. Metal ion detection is essential for monitoring environmental pollution, industrial processes, and biological systems where metal homeostasis plays a vital role. In this study, we focus on the synthesis, characterization, and application of a novel naphthalene-based Schiff base ligand, derived from the condensation reaction between 1,8-diaminonaphthalene and 3-nitrobenzaldehyde. …
Published in International Journal of Cheminformatics · Vol. 2, Issue 2, 2024 · pp. 1–8 Read article
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Exploring the Dual Functionality of Polypyrrole/Cobalt Sulphide Nanocomposite in Photocatalysis and Gas Sensing
Abstract: Cobalt sulphide nanomaterial was synthesized using the co-precipitation method, and chemical polymerization of polypyrrole (ppy) was performed in the presence of the synthesized cobalt sulphide nanomaterial for the preparation of nanocomposite. The synthesized ppy/cobalt sulphide nanocomposite was characterized by transmission electron microscopy (TEM), selected area electron diffraction (SAED), X-ray powder diffraction (XRD), Fourier transformation infrared spectroscopy, and UV-visible spectroscopy. The TEM micrograph revealed that the generated cobalt sulphide nanoparticles were …
Published in Journal of Polymer & Composites · Vol. 11, Issue 3, 2023 · pp. 72–85 Read article