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79 articles for “XRD technique”
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Zn Doped CuO Nanoparticles for Increasing the Longevity of The Agricultural Products †
Abstract: Nanotechnology is an enabling technology at the service of mankind. Indeed, enhancing the long-term storage of agricultural products (post-harvest during transportation and storage) in general and apples and tomatoes, in particular, is a challenge. Zn-doped CuO is a proven nanomaterial with special ability to kill plant pathogens as well as a variety of microorganisms (bacteria, virus, and fungus). Much of the review is focused on the landmark papers published by …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 1, 2024 · pp. 14–29 Read article
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Characterization Techniques for Thin Film Coatings Based on SiO₂, TiO₂, and ZrO₂
Abstract: Thin film coatings made from silicon dioxide (SiO₂), titanium dioxide (TiO₂) and zirconium dioxide (ZrO₂) have attracted great interest owing to their excellent optical, electrical, mechanical and chemical properties. These oxide thin films are widely used in microelectronics, solar cells, sensors, biomedical devices, photocatalysis, anti-reflective coatings and protective layers. The structural, morphological, compositional, optical and mechanical properties of these coatings are closely related to their performance and reliability. Therefore, thorough …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 Read article
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Oxidation Behaviour of Plasma Sprayed Carbon Nanotubes-Alumina Coated ASME-SA213-T291 Boiler Tube Steel
Abstract: In this research work, oxidation behaviour of Carbon Nanotubes reinforced Al2O3 coated ASME-SA213-T91 boiler tube steel specimens were investigated at 900°C temperature in air. The different CNTs-Alumina composite coatings were deposited using plasma spray technique and NiCr was used as bond coat before applying CNTs-Al2O3 coatings. The hot corrosion studies were conducted on all coated specimens in air at 900°C under cyclic conditions. The thermogravimetric technique was used to establish …
Published in Journal of Materials & Metallurgical Engineering · Vol. 7, Issue 3, 2017 · pp. 1–15 Read article
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Tailoring The Electrochemical Interface of Graphene–Gd₂O₃ Nanocomposites for Advanced Energy Storage
Abstract: Graphene–Gd₂O₃ nanocomposites were synthesized by incorporating varying concentrations of reduced graphene oxide (rGO) into Gd₂O₃ using a straightforward room-temperature solution method. The composites were analyzed using various distinct characterization techniques, including X-ray diffraction (XRD), Fourier-transform infrared (FTIR) spectroscopy, Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). Electrochemical measurements, particularly cyclic voltammetry (CV), demonstrated that the incorporation of graphene significantly enhanced the electrochemical performance …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 369–388 Read article
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Structure–Optical Property Correlation of Co-Doped TiO₂ and ZnO Nanofillers for Advanced Functional Composite Applications
Abstract: This study investigates the enhancement of the structural and optical properties of titanium dioxide (TiO₂) and zinc oxide (ZnO) nanoparticles through cobalt (Co) doping. Pristine TiO₂ and ZnO are widely studied metal oxides; however, their large band gaps and limited visible-light absorption restrict their performance in optoelectronic, photocatalytic, and environmental applications. Co doping is employed as an effective strategy to overcome these limitations by inducing band-gap narrowing, creating defect-related electronic …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1374–1394 Read article
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Synthesis and Experimental Evaluation of Graft Polymer Nanocomposite in Water Based Drilling Fluid System for Reactive Unconventional Reservoirs
Abstract: AbstractThis experimental work discusses the evaluation of polyacrylamide-grafted-gum arabic/carboxymethyl cellulose nanocomposite as a drilling mud additive for the drilling of reactive shale formations which may lead to wellbore instability. The synthesized nanocomposite was synthesized with free polymerization technique and it was characterized by XRD, FTIR, and FESEM. Then, it was preceded in the development of the WBDMS. Its effect on the rheological and filtration control properties of the formulated mud …
Published in Journal of Polymer & Composites · Vol. 5, Issue 2, 2017 · pp. 34–41 Read article
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Thermal degradation analysis of banana fiber by Coats & Redfern methodThermal Degradation Analysis of Banana Fiber by Coats and Redfern Method
Abstract: Nowadays, natural fiber is more advantageous than synthetic fiber. Natural fibers are used as reinforcement material with combination of polymer matrix. These are of different types like banana fiber, bamboo fiber, sisal, hemp, and jute, etc. Banana fiber is one of them which is most common and easily available fiber in global scenario. It is biodegradable, renewable, and lower in cost. This fiber is higher in cellulosic content. Out of …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 28–32 Read article
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Crystalline Materials: From Crystal Growth and Defect Engineering to Advanced Functional Applications
Abstract: Crystalline materials form the foundation of numerous modern technologies owing to their highly ordered atomic structures and exceptional physical, chemical, electrical, optical, and mechanical properties. Their periodic crystal lattices provide superior structural stability and enable precise control of electronic, thermal, and optical behavior, making them indispensable in microelectronics, photonics, energy storage, catalysis, aerospace, environmental remediation, and biomedical engineering. Rapid advances in crystal growth techniques, nanotechnology, and computational materials science have …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 2, 2026 · pp. 23–31 Read article
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Growth, XRD, FTIR and Second Order NLO studies of Undoped and Zinc Sulphate doped L-Histidine Single Crystals
Abstract: AbstractSingle crystals of pure (undoped) L-histidine and Zinc sulphate doped L-histidine have been synthesized and grown by slow evaporation method using water as the solvent. These grown crystals are characterized by FTIR, XRD and SHG. From Fourier transform infrared (FTIR) spectral analysis, the various functional groups present in the sample have been confirmed. The X-ray diffraction (XRD) study ensures that the grown crystal crystallizes in the orthorhombic system and the …
Published in Trends in Opto-electro & Optical Communication · Vol. 8, Issue 3, 2018 · pp. 31–36 Read article
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Synthesis of Lawsonia Inermis (Henna) Carbon Supported AgO Nanocomposite, Characterizations and Photocatalytic Activity Studies
Abstract: Synthesis of Carbon supported AgO nanocomposite is reported for first time. Henna carbon was successfully synthesized from henna leaf. Bare AgO and C-AgO nanocomposites are effectively made using precipitation method. The synthesised composites structural, morphological, and optical properties are assessed using FT-IR, XRD, FE-SEM, UV-DRS, and PL techniques. FT-IR analysis proved that specific functional groups of synthesized materials. The uniform distribution of the composites is revealed in the FE-SEM. XRD …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 749–760 Read article
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Synthesis and Characterization of VO 2+ doped SrMg 2 (PO 4 ) 2 Nanopowder by Solid State Reaction technique suitable for White LED material
Abstract: VO2+ doped SrMg2(PO4)2 nanopowder was synthesized by using solid state reaction (SSR) technique. Various experimental techniques have been performed on prepared sample. XRD analysis has revealed that prepared nanopowder is in monoclinic phase. The average crystallite size, micro strain and dislocation density evaluated and make an analogy with W-H plot method. SEM micrographs shows that agglomerated stone like structure and EDS spectrum shows elemental compositions of synthesized sample. FTIR spectrum …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 95–110 Read article
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Synthesis And Application of Nano Zinc Oxide in Fabrication of Rubber Composites
Abstract: Nano zinc oxide (ZnO) has garnered significant attention in recent years due to its unique properties and potential applications in various fields. This paper discusses the synthesis of nano ZnO by precipitation method and characterizes them with various techniques such as X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and Fourier Transform Infra-Red (FTIR) Spectroscopy and explores its application in the preparation of rubber composites. These synthesized particles were measured to …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 1–10 Read article
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Vapour Phase Hydrogenation of Levulinic Acid Over Carbon Coated HZSM-5 Supported Ni Catalysts
Abstract: Carbon coated HZSM-5 supported Ni catalyst shown to be a promising catalyst in the hydrogenation of levulinic acid to yield γ- valerolactone. Physicochemical characterizations were undertaken using N2 physisorption, H2-chemisorption, X-ray diffraction (XRD), CHNS and temperature programmed reduction (TPR) techniques. The CHNS studies reveal about 3 wt% carbon was coated by the passage of cyclohexene at 600 °C for 3 h. The carbon coated HZSM-5 supported Ni catalyst shown lower …
Published in Journal of Catalyst & Catalysis · Vol. 2, Issue 2, 2015 · pp. 33–38 Read article
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An Efficient Synthesis of Annulated Novel Dihydropyridine Derivatives using Zeolite H-BEA and Zeolite BEA-SO3H
Abstract: Modified zeolite (zeolite BEA-SO3H) was synthesized with intent to improve the surface area and Si/Al ratio by loading chlorosulphonic acid onto zeolite H-BEA. Parent and modified zeolite were characterized by variety of characterization techniques such as, ICP, FT-IR, XRD, TGA, NH3-TPD,BET surface area, etc. The catalytic applications of parent and modified zeolite H-BEA were demonstrated through the synthesis of novel quinoline and benzoquinoline substituted dihydropyridines (DHPs) via one pot Hantzsch …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 2, 2014 · pp. 1–12 Read article
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Correlation Between XRD Analysis and Mechanical Characterization Using Lens Manufactured Specimens Based on IoT Sensors
Abstract: The advent of the Internet of Things (IoT) has enabled the seamless integration of sensors into the manufacturing process, facilitating the collection of real-time data for analysis and optimization. The correlation between X-ray diffraction (XRD) analysis and mechanical characterization is investigated using specimens manufactured through the Laser Engineered Net Shaping (LENS) technique. The study focuses on three different materials: brass, SS202, and SS304. XRD analysis is employed to determine the …
Published in Journal of Polymer & Composites · Vol. 12, Issue 2, 2024 · pp. 41–58 Read article
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Electrochemical Exfoliation of Graphene Oxide (GO) and Thermally Reduced Graphene Oxide (TrGO) Using Ecofriendly Reducing Agent as Cow Urine
Abstract: The Graphene oxide (GO), the reduced form of GO i.e. (rGO) with thermally reduced graphene oxide (TrGO), have concerned significant interest in various fields with their exceptional properties. We investigate the electrochemical exfoliation processes of GO and rGO to understand their structural and electrochemical behavior of GO and TrGO through various characterization techniques. The electrochemical exfoliation method offers a versatile and scalable approach for the mass fabrication of the materials …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 89–100 Read article
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Improved Photocatalytic Activity for Removal of Methylene Blue Dye from Aqueous Solutions with La2O3-Modified Ceria Heterostructured Binary Oxide Nanocomposite Particles
Abstract: The current study aimed to examine the photocatalytic efficacy of a bimetallic CeO2-La2O3 hetero-NC in comparison to monometallic CeO2 and La2O3 nanoparticles (NPs), utilizing Methylene Blue (MB)as pollutant sample under natural solar and UV irradiation. The coprecipitation method was utilized to produce a bimetallic CeO2-La2O3 hetero-NC. Following this, the nanostructures underwent characterization through various techniques including FT-IR, FE-SEM, XRD, UV Vis- DRS, Raman, and Photoluminescence spectroscopy. The catalytic activity of …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 514–532 Read article
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A Review on Synthesis and Characterisation of Nanoclusters
Abstract: Nanoclusters are materials with size less than 2 nm. Because of their small size and high surface area, they have properties which can be used for various applications like bio-sensing, catalysis, fuel cells etc. The synthesis techniques are carried out in such a way that the size-selection of nanoclusters take place. The synthesis methods discussed in this review include both top-down and bottom-up techniques. The different characterization techniques taken into …
Published in Emerging Trends in Chemical Engineering · Vol. 8, Issue 1, 2021 · pp. 1–19 Read article
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Green Synthesis of Silver Nanoparticles Using Ficus Religiosa Linn Leaf Extract
Abstract: Nanotechnology is always a promising field for many new technological innovations. Turning Chemical process green also gains more attention of researchers due to high environmental concern. The process that involves ecofriendly procedures, use of less toxic solvents, less toxic byproducts, use of cheaper raw materials are all becoming ever increase in demand for current research scenario. Plants especially those having medicinal properties are beneficial for synthesizing nanoparticles as it will …
Published in Journal of Catalyst & Catalysis · Vol. 8, Issue 2, 2021 · pp. 45–52 Read article
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The Impact of Distinct Dopant Elements (Cu and Al) on the Electrochemical Characteristics of MgO Thin Films Formed Using the Electrodeposition Technique
Abstract: By using an aqueous electrodeposition technique, copper (Cu) and aluminum (Al) doped magnesium oxide (MgO) thin films were created. We examined how the dopant elements affected the electrochemical characteristics of MgO thin films deposited on stainless steel (SS) substrates in the current study. We annealed the MgO-based films at 450◦C. The MgO films doped with Cu and Al have been determined by X-ray diffraction (XRD) results. Cyclic voltammetric analyses (CV), …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 1, Issue 2, 2023 · pp. 12–17 Read article