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111 articles for “XRD results.”
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Experimental Investigation for Strengthening the Nanocomposite Cementitious Materials with a Nanoscale Modification
Abstract: For the last few decades, researchers have widely used nanopolymer to control the mechanical properties of cementitious materials as a micro reinforcement. This paper examines and compares the mechanical and microstructure property of nanofiber cementitious material. Twenty-four sets of beam/cube cast with carbon nanofibers (CNFs) cementitious material where CNFs were used from 0.1%, 0.2%, and 0.3% of cement weight. The nanoparticles were scattered using a surfactant and an ultrasonic probe …
Published in Recent Trends in Civil Engineering & Technology · Vol. 12, Issue 2, 2022 · pp. 10–24 Read article
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Microstructural Evolution and Mechanical Performance of Ambient-Cured Fly Ash–Metakaolin Inorganic Polymer Composites Activated by Anhydrous Sodium Silicate Powder
Abstract: Inorganic geopolymer networks offer a low-carbon and sustainable solution to traditional binder systems through the alkali-activation of industrials-grade aluminosilicate material. The present paper focuses on the microstructure development and the mechanical performance of the ambient-cured fly ash – metakaolin inorganic polymer composite activated with solid anhydrous sodium silicate powder. Five inorganic polymer binder combinations were formulated by replacing fly ash with metakaolin at mass fractions of 0%, 10%, 20%, 30%, …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article
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Correlation Between XRD Analysis and Mechanical Characterization Using Lens Manufactured Specimens Based on IoT Sensors
Abstract: The advent of the Internet of Things (IoT) has enabled the seamless integration of sensors into the manufacturing process, facilitating the collection of real-time data for analysis and optimization. The correlation between X-ray diffraction (XRD) analysis and mechanical characterization is investigated using specimens manufactured through the Laser Engineered Net Shaping (LENS) technique. The study focuses on three different materials: brass, SS202, and SS304. XRD analysis is employed to determine the …
Published in Journal of Polymer & Composites · Vol. 12, Issue 2, 2024 · pp. 41–58 Read article
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Standardization of Rakta-Akika Bhasma and Pisthi: An Ayurvedic Formulation
Abstract: Background: Standardization of the classically prepared medicines is a must apart from other organoleptic tests as mentioned in the ancient text. Rakta Akika Bhasma (RAB) and Pishti (RAP) is a traditional Ayurvedic preparation for Hridaroga (Cardiac disease), Shiroroga (headache due to vitiated Dosha), Kasa (cough), Raktaja Vikara (bleeding disorders) and many more. Aim: The present research work was conducted to analyze raw and processed Rakta Akika Bhasma and Pishti for …
Published in Research and Reviews : A Journal of Ayurvedic Science, Yoga and Naturopathy · Vol. 10, Issue 2, 2023 · pp. 28–39 Read article
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Experimental investigation of thermally grown Indium film’s structural and tribological properties
Abstract: Indium thin film growth found numerous applications, such as cold welding of infrared detectors and readout-integrated circuits (ROIC) to form sensor chips. In film is grown on the Si substrate by thermal evaporation. The XRD results indicated the tetragonal bcc phase in the (101) preferential plane. Scanning electron microscopy (SEM) indicated an uniform, continuous film covering the whole surface. The EDS examination confirmed the pure In film. The atomic force …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 58–66 Read article
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The Impact of Distinct Dopant Elements (Cu and Al) on the Electrochemical Characteristics of MgO Thin Films Formed Using the Electrodeposition Technique
Abstract: By using an aqueous electrodeposition technique, copper (Cu) and aluminum (Al) doped magnesium oxide (MgO) thin films were created. We examined how the dopant elements affected the electrochemical characteristics of MgO thin films deposited on stainless steel (SS) substrates in the current study. We annealed the MgO-based films at 450◦C. The MgO films doped with Cu and Al have been determined by X-ray diffraction (XRD) results. Cyclic voltammetric analyses (CV), …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 1, Issue 2, 2023 · pp. 12–17 Read article
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Toxicological Optimization and Assessment of Buccal Films Containing Felodipine Co-crystals to Enhance Bioavailability
Abstract: The preformulation study of felodipine was carried out and it was found that the drug is poorly water soluble. The co-crystals were prepared using three different co-formers sorbitol, ascorbic acid and oxalic acid. The solublity enhancement was observed in combination with sorbitol compared to other co-formers used. The characterization of co crystals was performed like PXRD, FTIR, SEM Analysis. XRD results indicates the amorphous form of the drug. The co-crystals …
Published in Research and Reviews: A Journal of Toxicology · Vol. 14, Issue 2, 2024 · pp. 10–29 Read article
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Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis Read article
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Feasibility of Cryogenic Treatment for Improving Lattice Strain Distribution in AA7010 Alloy
Abstract: In the present investigation, AA7010 was subjected to two different cycles of cryogenic treatment. In one cycle, the cryogenic treatment was given after the quenching and aging, whereas in another cycle the treatment was given immediately after quenching before aging. The hardness and XRD results of these samples were compared with that of T6 conditioned sample, taken as the reference. The samples, which were given cryo-treatment immediately after quenching before …
Published in Journal of Materials & Metallurgical Engineering · Vol. 4, Issue 1, 2014 · pp. 7–12 Read article
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Synthesis and Characterization of Green Synthesized Iron Nano Particle (GInP) Using Eucalyptus globulus for Lead Removal
Abstract: The application of green synthesized iron nanoparticle for the removal of lead is researched in this study. The FT-IR and XRD results reveal that a nanoparticle with 80 nm size could be synthesized using Eucalyptus globulus leaf extract. The specific surface area of the nanoparticle was found to be 59 m2/g. The lead removal capability of the green synthesized iron nanoparticle (GInP) was investigated for lead concentration ranging from 50–250 …
Published in Journal of Materials & Metallurgical Engineering · Vol. 10, Issue 3, 2020 · pp. 20–25 Read article
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TiO2-ZrO2 Supported Nickel Oxide Catalysts for Hydrogenation of Levulinic Acid to -Valerolcatone
Abstract: The Titania-Zirconia (TZ) mixed oxide sample (50:50 wt.% percent) was prepared by a simple coprecipitation method and used as a support for the nickel catalyst. The various loadings of nickel content from 1 to 20 wt.% were synthesized for the production of γ-valerolactone (GVL) from levulinic acid (LA). Among all the tested samples, the 5 wt.% Ni/TZ sample exhibited the 98% conversion of LA and 96% selectivity to GVL and …
Published in Emerging Trends in Chemical Engineering · Vol. 9, Issue 3, 2022 · pp. 35–44 Read article
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A Comparative Study of the Structure–Property Relationships in CAD/CAM Milled vs. 3D-Printed High-Performance Polymers: Impact of Molecular Orientation on Abrasive-Wear Resistance
Abstract: Background: The transition from subtractive to additive manufacturing in prosthetic dentistry has introduced significant variations in the macromolecular architecture of high-performance polymers. While CAD/CAM milling utilizes high-density, industrially polymerized blocks, 3D printing (Additive Manufacturing) relies on layer-by-layer deposition, which may induce anisotropic molecular orientation. This retrospective study investigates how these distinct manufacturing “thermal histories” influence the long-term abrasive-wear resistance of PEEK and PEKK restorations. Materials and Methods: Data were retrospectively …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 133–140 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 45–59 Read article
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Strength Studies of Fly Ash Stabilized with Lime and Gypsum
Abstract: An experimental study was conducted to investigate the performance of a composite derived from stabilizing fly ash with lime and gypsum. The initial part of the study examines the effect of lime (4%, 8%, and 12% by mass of dry fly ash) on compaction (in terms of density/moisture relationship) and unconfined compressive strength (UCS) of fly ash. Further the effect of adding small amount of gypsum (1%) on strength was …
Published in Journal of Geotechnical Engineering · Vol. 2, Issue 3, 2015 · pp. 10–16 Read article
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Structural, Electrical and Optical Properties of RGO-Incorporated PVA Nanocomposites for UV Shielding Applications
Abstract: Polymer matrix-based nanocomposites reinforced with appropriate nanoparticles have the potential to exhibit improved electrical, optical and mechanical properties, as well as improved UV-shielding capabilities. These materials are currently being utilised for various commercial applications, such as window shields and automotive components. We prepared reduced graphene oxide (rGO)-incorporated polyvinyl alcohol (PVA) polymer nanocomposites employing a solution casting method. XRD and SEM results confirmed that the rGO nanosheets were dispersed well in …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 119–137 Read article
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Role of Strontium in Structural and Dielectric characterstics of Barium Titanate
Abstract: Ba₀.₇₅Sr₀.₂₅TiO₃ (BST) compound was synthesized through the conventional solid-state reaction methodology, aimed at investigating its structural, microstructural, and dielectric characteristics. The structural characterization was executed employing X-ray diffraction (XRD), and the resultant diffraction patterns were refined utilizing the Rietveld method, which substantiated the establishment of a single-phase perovskite configuration exhibiting tetragonal symmetry and belonging to the P4mm space group. The refined lattice parameters revealed subtle distortions correlating with the substitution …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1157–1163 Read article
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Preparation and Characterization of Aluminium Doped ZnO Thin Films by Spin Coating Technique
Abstract: In this work, the preparation of Al-doped ZnO (AZO) thin films by the sol-gel spin-coating method is reported. The structural properties and surface morphologies of film prepared at RT were characterized by X-ray diffraction (XRD) and field emission scanning electron microscope (FE-SEM). The XRD and SEM results disclosed that the crystallization quality and grain size of as-prepared films were highly influenced by Al doping. Laser Raman Spectrometer results indicated that …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 7, Issue 2, 2020 · pp. 16–22 Read article
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Solid acidity of MoO3 synthesized by solution combustion method and acetalization of formaldehyde using it
Abstract: MoO 3 nanoparticles were synthesized via solution combustion approach. Ammonium nitrate was used as oxidant and ammonium molybdate as fuel in combustion reaction. XRD, FTIR and Raman spectroscopy results showed that MoO 3 nanoparticles were successfully synthesized by the solution combustion reaction. The SEM analysis showed that synthesized MoO 3 nanoparticles have rod-like shape with width and thickness of 50-200nm and length of 0.2-1μm, respectively. The XRD pattern and morphology …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 3, 2025 · pp. 01–09 Read article
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Structural Modification of Sugarcane Bagasse using Alkaline, Acid, and Bleaching Pretreatments for Enhanced Yield of Poly (1→4)-β-D-glucopyranose (Cellulose) and Hemicellulose for Utilization as Biocomposites
Abstract: Sugarcane bagasse, a lignocellulosic byproduct generated in substantial quantities by the sugar industry, represents a promising feedstock for the sustainable production of enzymes and bio-based chemicals. Its high (1→4)-β-D-glucopyranose (cellulose) content, abundant availability, and low cost make it an ideal candidate for bioconversion processes. However, the inherent recalcitrance of bagasse, primarily due to its lignin-rich matrix, necessitates effective pretreatment strategies to enhance enzymatic digestibility. This study presents a comparative investigation …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 983–992 Read article