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111 articles for “X-ray diffraction”
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Crystallinity of commercial carbon fibers from X-ray diffraction (XRD) studies
Abstract: Sized carbon fibers have commercial significance. Such carbon fibers serves has excellent reinforcing material with the polymer resin filler matrix leading to the formation of carbon fiber reinforced composites (CFRCs). Polarized carbon fibers find applications in the realms of health, energy, environment, defence, catalysis and smart materials. For brevities sake, the focus of the current research paper is only on the structural characterization of carbon fibers using XRD. The structure …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 1, Issue 1, 2023 · pp. 17–27 Read article
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Design of a Geopolymer Based on Fly Ash and Metakaolin with a Solid, Liquid, and Powdered Alkaline Activator at High Temperatures
Abstract: In this work, the fresh and hardened properties of geopolymer concrete activated using solid, liquid, and powder alkaline activator systems, including fly ash and different amounts of metakaolin, are examined. Compressive and flexural strengths were assessed at 7 and 28 days in accordance with IS 516 (1959). Workability was evaluated using a slump test in accordance with IS 1199 (Part 2): 2018. At an ideal replacement level of 30%, the …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 712–726 Read article
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A Comparative Study of the Structure-Property Relationships in CAD/CAM Milled vs. 3D-Printed High-Performance Polymers: Impact of Molecular Orientation on Abrasive Wear
Abstract: Background: The transition from subtractive to additive manufacturing in prosthetic dentistry has introduced significant variations in the macromolecular architecture of high-performance polymers. While CAD/CAM milling utilizes high-density, industrially polymerized blocks, 3D printing (Additive Manufacturing) relies on layer-by-layer deposition, which may induce anisotropic molecular orientation. This retrospective study investigates how these distinct manufacturing "thermal histories" influence the long-term abrasive wear resistance of PEEK and PEKK restorations.Materials and Methods: Data were retrospectively …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article
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Microstructure Analysis and Material Properties of Weld Slag as Fine Aggregate in Concrete
Abstract: To reduce the amount of river sand used, researchers and engineers have developed their own solutions. The well-known technique of submerged-arc welding can create high-quality welds in a variety of thicknesses for ferrous, stainless, and even some non-ferrous metals. The procedure involves an electric current flowing constantly between a welding wire and the work piece, creating an arc. In submerged arc welding, the shielding flux is transformed into slag during …
Published in Recent Trends in Civil Engineering & Technology · Vol. 15, Issue 2, 2025 · pp. 13–18 Read article
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Dielectric Studies of 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 Nanoceramic Fabricated by Chemo-mechanical Process
Abstract: The present investigation is aimed toward investigate a straightforward, inexpensive, and environmentally friendly chemo-mechanical method for preparing high-dielectric materials, specifically 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 (BCT-CCTO), by combining metal nitrate combustion with solid TiO2 powder and titanium isopropoxide, Ti (OR)4. The composite was prepared by the mixing of individual materials of Ba0.8Ca0.2TiO3 and CaCu3Ti4O12 through the chemo-mechanical method. Initially, 99% pure Ba (NO3)3, Cu (NO3)2∙3H2O, TiO2 and glycine were taken in their stoichiometry ratios. …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 12–21 Read article
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Comparative Study of Structural and Optical Properties of Bismuth Ferrite Nanoparticles for Photovoltaic Applications Synthesized via Different Sol-Gel Methods
Abstract: Pure multiferroic bismuth ferrite (BiFeO3) nanoparticles were successfully synthesized using an energy-efficient, low-temperature sol-gel method, comparing two distinct approaches: auto-combustion and non-auto-combustion. To ensure phase stability, the precursor solution's pH was strictly maintained between 1 and 2 using ammonia solution (NH4OH), while ethylene glycol (C2H6O2) was employed as a chelating agent for the Fe3+ and Bi3+ cations. All samples underwent a final annealing process at 500 °C to promote crystallization. …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 83–94 Read article
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Tb3+ activated Boro Phosphate Glass: Synthesis and Photoluminescence (PL) Characteristics
Abstract: The (40B2O3+ 3Al2O3+(10-x) P2O5 + xTb + 7ZnO+5LiCO3+ 10H6NO4P+25SrCO3) boro phosphate glass was successfully synthesized via melt quenching method. The structural confirmation is supported with X-ray diffraction (XRD) data and surface morphology was defined by scanning electron microscope (SEM). The (40B2O3+ 3Al2O3+(10-x) P2O5 + xTb+ 7ZnO+5LiCO3+ 10H6NO4P+25SrCO3) boro phosphate glass has been investigated for its Photoluminescence (PL) under UV excitation. At 544 nm, the excitation was observed, and at 222 …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 43–47 Read article
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Electrodeposition and Magnetron Sputtering of Rhenium Coatings on Carbon-Carbon Composites for Enhanced Corrosion Resistance and Structural Integrity
Abstract: It is well known that tailored materials are gaining in-roads to aviation and other manufacturing industries where stringent requirements are to be met, due to high temperature erosion, which is a problem. In order to counter these issues, materials which can resist a very high temperature are to be sought. One of the several methods to combat this high temperature issue is to provide a metallic refractory material coating on …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 35–44 Read article
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Exploring the Impact of Lattice Strain on the Debye-Waller Factor in Iron Nanoparticles: A Comprehensive Analysis
Abstract: This study systematically investigates the influence of lattice strain and particle size in iron powder produced through milling, employing X-ray powder diffraction. The determination of lattice strain (ε) and the Debye-Waller factor (B) is accomplished by analyzing Bragg reflection half-widths and integrated intensities. Significantly, the Debye-Waller factor exhibited a notable increase with lattice strain. By establishing a correlation between stress and the influential Debye-Waller factor, we derived a precise relationship …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 215–224 Read article
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Anisotropic Debye-Waller Factors and Debye Temperatures in Hexagonal Close-Packed Elements: A Comprehensive Compilation and Analysis
Abstract: In this study, we have investigated the anisotropic behavior of Debye-Waller factors (DWFs) and Debye temperatures (DTs) in three distinct materials: hexagonal rhenium (Re), osmium (Os), and thallium (Tl). We conducted a comparative analysis, aligning our experimental data on directional Debye temperatures with theoretical calculations. This exercise provided valuable insights into the concurrence between practical and theoretical approaches, thereby offering a critical evaluation of the accuracy and reliability of theoretical …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 32–39 Read article
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Synthesis And Application of Nano Zinc Oxide in Fabrication of Rubber Composites
Abstract: Nano zinc oxide (ZnO) has garnered significant attention in recent years due to its unique properties and potential applications in various fields. This paper discusses the synthesis of nano ZnO by precipitation method and characterizes them with various techniques such as X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and Fourier Transform Infra-Red (FTIR) Spectroscopy and explores its application in the preparation of rubber composites. These synthesized particles were measured to …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 1–10 Read article
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Revolutionizing Petrology and Mineralogy: The Study of AI and Advanced Sensor Technologies
Abstract: Petrology and mineralogy are fundamental to understanding Earth's intricate processes, from crustal evolution to economic resource formation. However, traditional methods, while precise, are often laborious, time-consuming, and occasionally subject to interpretive bias. This abstract explores the transformative potential of integrating cutting-edge Artificial Intelligence (AI) and advanced sensor technologies to revolutionize data acquisition, analysis, and interpretation in these critical geosciences. Advanced sensor technologies, including high-resolution spectral imaging (hyperspectral, Raman), automated X-ray …
Published in International Journal of Minerals · Vol. 2, Issue 2, 2025 · pp. 1–11 Read article
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Effect of Bismuth doping on Thiourea crystals : A NLO Material
Abstract: Single crystals of pure and thiourea-substituted bismuth were successfully grown using the slow evaporation solution growth technique at ambient temperature. The impact of thiourea doping on the crystal properties was thoroughly investigated. Solubility tests for the grown samples were conducted at various temperatures, providing crucial data on the dissolution characteristics. Structural characterization of these crystals was performed using single crystal X-ray diffraction (XRD), confirming their crystalline nature. Energy-dispersive X-ray spectroscopy …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 15, Issue 2, 2024 · pp. 10–16 Read article
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A Sol-Gel Approach for the Fabrication of Zinc Oxide Nanoparticles and Their Nanocomposite with Urea Formaldehyde (UF)
Abstract: In the performed work, zinc oxide nanoparticles were synthesized via the sol-gel method using zinc sulphate as the precursor material. Urea-formaldehyde (UF) resin was employed as a polymer matrix to encapsulate the produced ZnO through an acid-catalyzed polymerization process. This encapsulation aimed to improve the dispersion stability and surface reactivity of ZnO within the polymeric medium. The synthesized materials were subjected to comprehensive characterization using Fourier Transform Infrared Spectroscopy (FT-IR), …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 21–27 Read article
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Experimental Studies on the Mechanical and Microstructural Properties of Sustainable Concrete Incorporating Palm Oil Industrial Waste
Abstract: Diving into the world of concrete, normal concrete is widely used in construction but poses environmental challenges due to significant carbon dioxide emissions from cement production. Incorporating oil palm shells (OPS) and palm oil fuel ash (POFA) into concrete offers a sustainable alternative, utilizing waste products from the palm oil industry and reducing environmental impact. Experimental studies have examined the use of OPS and POFA as partial replacements for coarse …
Published in Journal of Polymer & Composites · Vol. 12, Issue 7, 2024 · pp. 19–40 Read article
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Tailoring The Electrochemical Interface of Graphene–Gd₂O₃ Nanocomposites for Advanced Energy Storage
Abstract: Graphene–Gd₂O₃ nanocomposites were synthesized by incorporating varying concentrations of reduced graphene oxide (rGO) into Gd₂O₃ using a straightforward room-temperature solution method. The composites were analyzed using various distinct characterization techniques, including X-ray diffraction (XRD), Fourier-transform infrared (FTIR) spectroscopy, Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). Electrochemical measurements, particularly cyclic voltammetry (CV), demonstrated that the incorporation of graphene significantly enhanced the electrochemical performance …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 369–388 Read article
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Geotechnical Influence Factors in Empirical Design of Highway Pavement: The A123 Ilorin – Lokoja Highway, Nigeria Case Studies
Abstract: Site investigation and application of geological and geotechnical influence factors on the highway were investigated. Method involved field sampling, geotechnical laboratory and x-ray diffraction analysis and use of SRTM extracted slope and drainage parameters; and their integration in a GIS based multi-criteria decision analysis to derive a subgrade suitability map as a design tool. The suitability criteria classified the highway into four (4) design sections. Section one for very low …
Published in Journal of Geotechnical Engineering · Vol. 11, Issue 3, 2024 · pp. 53–70 Read article
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Influence of Gd Doping in Structural, Morphological and Optical Properties of Zno Nanostructures Synthesised Via Sol-Gel Processes
Abstract: In this study, nanocrystalline Zn1-xGdx (x=0.0 and 0.03) samples were synthesised via the Sol-gel combustion process. An array of analytical techniques was employed to examine the prepared samples to determine their different physical features. For both pristine and Gd-doped samples, the crystal symmetry is hexagonal with the P63mc space group which is verified via the Rietveld refinement analysis of X-ray diffraction (XRD) data. The atoms' bond length Zn-O and bond …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 219–225 Read article
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Investigations into the Mechanical and Thermal Properties of Fe3C Compound: A Comprehensive Analysis
Abstract: Exploration of mechanical properties of Fe3C powder using Williamson-Hall analysis by using Mechanical alloying technique. The primary objective of this study is to investigate the lattice strain (LS) and nanocrystalline size (CS) in an Fe3C produced from powder using the Mechanical Alloying Method (MAM). By the repeated mechanical crushing, the LS created by MAM is expected to decrease while the CS is anticipated to reduce the particle size. To accomplish …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 225–234 Read article