Search
116 articles for “IR spectroscopy”
-
Study of Elastic Properties of Copper Substituted Nickel – Zinc Nano Ferrites Through IR-Spectroscopy
Abstract: Nano crystalline Ni 0.65 Zn 0.35 Cu x Fe (2-2x/3) O 4, (x ranging from 0 – 0.05 in steps of 0.01) ferrites synthesized via hydrothermal route are characterized by FTIR spectroscopy. IR spectra of prepared ferrites demonstrated the two fingerprint absorption bands of spinels in the range of 400-600 cm-1. Lattice constant, X-ray density values obtained from XRD patterns used for evaluating the tetrahedral site and octahedral site force …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 25, Issue 2, 2023 · pp. 1–12 Read article
-
Diglycidyl Ether of Bisphenol A (DGEBA) Based Epoxy Sizing Agent Induces Surface Polarity in Carbon Fibers†
Abstract: Determination of the chemical structure and composition of the sizing agent is a challenge as its concentration is low, varying in the range from ~0.5 wt.% (for polyacrylonitrile, PAN, based carbon fibers) to ~1 wt.% (for pitch-based carbon fibers). Moreover, such a piece of knowledge is vital for designing compatible polymer matrices to prepare CFRPs for diverse applications. As a result, the sizing layer that is coated on the carbon …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 2, 2024 · pp. 24–34 Read article
-
The Use of Infrared Spectroscopy in the Medicine
Abstract: Infrared spectroscopy is a valuable analytical method that is used to study the structure of organic molecules, inorganic and coordination, as well as macromolecular compounds. The ability to obtain information about the presence of certain functional groups in a sample allows the use of medical infrared spectroscopy as a tool for studying tissue biochemistry, which means for diagnosing inflammatory processes in the human body, and for conducting of physicochemical studies …
Published in Research & Reviews: A Journal of Bioinformatics · Vol. 8, Issue 3, 2021 · pp. 44–51 Read article
-
Characterization of Synthesized Heterocyclic Oxadiazole Derivatives Using Mass, UV, IR, and NMR Spectroscopy, Among other Spectroscopic Techniques: Review
Abstract: The current study synthesized and assessed 3-heteroarylazo 4-hydroxy coumarin derivatives' initial antibacterial activities in vitro against four distinct pathogenic bacterial strains, including Pseudomonas aeruginosa, Bacillus subtilis, Escherichia coli, and Staphylococcus aureus. Ampicillin, a common medication, was used to compare each compound's antibacterial properties. UV, IR, 1H NMR, mass spectroscopy, and X-ray diffraction examinations were used to analyze the compounds. By using UV–vis spectra, the solute-chromic behavior of these compounds was …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 1, Issue 1, 2023 · pp. 28–33 Read article
-
Dodecahedron Methane Hydrate Cage Structure – An Ab initio Study
Abstract: Comparative study of 512clathrate hydrate cage having different numbers of methane guest molecules encapsulation is carried out by calculating interaction energy, encapsulation energy and thermo-chemical stability parameters using density functional theory-based calculation with B3LYP functional and 6-31G(d) basis set. Nuclear magnetic resonance spectroscopy(NMR), Infrared spectroscopy (IR spectroscopy) and Raman spectroscopy of empty and methane encapsulated 512clathrate hydrate cages, change in Gibbs free energy and methane hydrate formation enthalpy are predicted …
Published in Journal of Petroleum Engineering & Technology · Vol. 2, Issue 1-3, 2012 · pp. 51–64 Read article
-
Silver Nanoparticles Biosynthesis Using Grape Extract and Its Application in Photocatalytic Dye Degradation
Abstract: AbstractGrapes are known for its antioxidant properties. Aqueous grape extract is used in the current study as a reducing and stabilising agent in the production of silver nanoparticles. Silver nanoparticles were synthesized in single step method, at room temperature, under magnetic stirring without application of external energy. Silver nanoparticles are substantial for its application in numerous areas such as medicine, agriculture, food, chemical sector etc. Synthesis and optimization of silver …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 13, Issue 3, 2022 · pp. 1–8 Read article
-
Characterization and Gamma Irradiated MA-EMA Copolymer by ESR and FTIR Techniques
Abstract: AbstractGamma irradiation effect of methacrylamide-ethyl methacrylate (MA-EMA) copolymer has been investigated by electron spin resonance (ESR) and Fourier Transform infrared (FTIR) spectroscopic techniques. The ESR spectrum observed for gamma irradiated MA-EMA copolymer has shown resolved hyperfine (hf) pattern at lower temperatures (77K) while at higher temperatures the spectrum is appeared to be broadened. Fourier Transform Infrared spectra of pure and gamma irradiated MA-EMA copolymer have been recorded for the copolymer …
Published in Journal of Polymer & Composites · Vol. 4, Issue 3, 2016 · pp. 40–44 Read article
-
Modification of Acrylonitrile-Methylacrylate Copolymer by Gamma Irradiation
Abstract: AbstractRadiative degradation of acrylonitrile-methylacrylate (AM) copolymer has been investigated by electron spin resonance (ESR) and infrared (IR) spectroscopy. The ESR spectrum observed for AM copolymer irradiated to a dose of 12 Mrad is a triplet with an intensity ratio of 1:3:1. The ESR spectrum is simulated by total-curve-fitting method and component spectra are generated. Magnetic parameters of component spectra are evaluated. Component triplet spectrum with magnetic parameters ni=3, mi=1 is …
Published in Journal of Polymer & Composites · Vol. 3, Issue 3, 2015 · pp. 16–19 Read article
-
Development of Sodium Alginate Beads of Telmisartan Using Emulsion Gelation Method: Formulation and In-Vitro Characterization
Abstract: Introduction: The antihypertensive medication Telmisartan (TEL) is a member of BCS class II, which is distinguished by limited oral rate and extent and water solubility. By localizing the medication release in the stomach, gastro-retentive floating bead devices may be able to address the issues related to partial absorption and the low solubility of TEL. The preparation of TEL floating alginate beads was the aim of this investigation. The current work …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 11, Issue 3, 2024 · pp. 13–21 Read article
-
Development and Evaluation of a Novel Polyaniline/Polyvinyl Alcohol/Silver Nanocomposite for Antibacterial Applications: Synthesis and Characterization
Abstract: A novel nanocomposite made up of polyaniline, polyvinyl alcohol, and silver (PAL/PVA/Ag) was synthesized using the reduction of chemical technique in this study. Aniline was polymerized in situ with ammonium persulfate to create polyaniline (PAL), while Ag+ ions were employed to make an nanoparticle of Ag colloidal solution. The combination of Ag nanoparticles with the PAL/PVA composite resulted in the development of a new nanocomposite. Scanning electron microscopy (SEM) and …
Published in Journal of Polymer & Composites · Vol. 11, Issue 3, 2023 · pp. 39–47 Read article
-
Synthesis and Functional Group Analysis of Solution Processed Zinc Oxide Thin Film Grown on Polyethylene Terephthalate
Abstract: Flexible electronics field is growing every day. Existing technology is facing issues like brittleness, toxicity, inadequacy. Fabrication cost increases in processing of such materials. In this work, zinc oxide nanoparticles synthesized by solution processing technique were used to grow 120nm thick thin film (TF) on Polyethylene terephthalate (PET). This method reduces the processing cost and Zinc Oxide (ZnO) is cheaper and abundant in comparison to other semiconductors option. Material was …
Published in Journal of Polymer & Composites · Vol. 12, Issue 3, 2024 · pp. 56–66 Read article
-
Effect of Electrochemically Synthesized Zno/CoO Nanocomposites on Optical, Electrical and Viscosity Properties of Polyvinyl Alcohol Films
Abstract: AbstractZnO/CoO nanocomposites doped poly vinyl alcohol films were prepared by casting method using water as a solvent. X-ray diffraction, IR spectroscopy UV-visible spectroscopy, and scanning electron microscopy techniques were used to characterize the synthesized nanocomposite films. Study of the structural changes and complexation of nanoparticles with polymer matrix were performed using X-ray and IR techniques. Optical characterization studies revealed a blue shift in the absorption edge with increasing nanoparticle concentration …
Published in Journal of Polymer & Composites · Vol. 4, Issue 2, 2016 · pp. 52–62 Read article
-
Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
-
Characterization and Antimicrobial Investigations of Isomeric Pr(III) Juglonates
Abstract: Hydroxy napthoquinone derivatives constitute an interesting group of ligands which is recognized as ‘Juglones’. Isomeric Lawsone-Juglone and Phthiocol-Plumbagin are the most important members of the Juglone series and are biologically active, having natural origin. They form isomeric pairs of ligands resulting into isomeric pairs of metal chelates. The isomerism is occurring due to formation of either five or six membered rings in the metal chelates. In the present work Prasodymium …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 545–552 Read article
-
Reactivity of Monochlorotetrakis2-Isopropylphenoxoniobium(V), [NbCl(OC6H4CH(CH3)2-2)4] towards Chelating Ligands
Abstract: The niobium(V) complexes with the formula [NbCl(OC₆H₄CH(CH₃)₂-2)₄] were successfully synthesized in high yields through the reaction of niobium pentachloride with four equivalent amounts of 2-isopropylphenol in carbon tetrachloride. The synthesized complexes were characterized and confirmed by elemental analysis, molar conductance measurements, infrared (IR) spectroscopy, ^1H and ^13C NMR spectroscopy, as well as mass spectrometric analysis. The spectroscopic studies have shown these to exhibit dimeric structures bridging through isopropylphenoxo groups. The …
Published in International Journal of Minerals · Vol. 3, Issue 1, 2026 · pp. 37–45 Read article
-
Composition and Structure of Oil Finishing Agent †
Abstract: Use of oil finishing agent is widely used in the process of production of carbon fibers to impart unusual and exceptional strength to the carbon fibers, the key load-bearing component, of the advanced materials, namely, carbon fiber reinforced composites (CFRPs). CFRPs are being widely used in the realm of aeronautics, astronautics, aeronautics, geonautics, sports equipment, and many more. However, quite often, much of the knowledge on the composition of oil …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 1, 2025 · pp. 01–10 Read article
-
Properties of ZnO Thin Film deposited on Flexible Substrate using RF Sputtering
Abstract: Semiconductor materials demand is increased in recent years, due to new emerging technologies. There is need to find the alternate for silicon in electronics industry, as silicon is brittle in nature and has low efficiency, which makes it unsuitable for transparent and flexible device. Zinc oxide (ZnO) is emerging as popular choice of researchers due to its wide range of properties, abundancy and non-toxicity. This work explores the properties of …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 50–56 Read article
-
An Efficient Synthesis of Some Novel Benzo Coumarin Derivatives Under Solvent Conditions from 2-acetyl-benzo[f]chromen-3-one
Abstract: The synthesis of the target compounds began with the preparation of 2-[3-dimethylamino[acryloyl-3H-benzo[f]chromen-3-one. This intermediate was obtained through the reaction of 2-acetylbenzo[f]coumarin-3-one with N,N-dimethylformamide dimethyl acetal [DMFDMA[ under reflux conditions in xylene. The enaminone thus formed was subsequently reacted with 6-aminothiouracil in acetic acid, leading to the formation of 2-thioxo-2,3-dihydro-1H-pyrido[2,3-d]pyrimidin-4-one. This compound served as a pivotal intermediate for the synthesis of a series of pyridotriazolopyrimidinones. These derivatives were synthesized by reacting …
Published in International Journal of Cheminformatics · Vol. 2, Issue 2, 2024 · pp. 33–46 Read article
-
Preparation, Categorization and Anticancer Study of Novel Bicyclic Compounds from Various Types for (Five and Six)- Membered Ring
Abstract: The characteristics of ring systems change in the presence of functional groups, but in some cases, elements that are considered functional groups can be classified within the same ring. Compounds that contain only carbon and hydrogen are called homogeneous rings, while those that contain other elements are called heterogeneous rings. The atom substituted in place of the carbon atom is referred to as a heteroatom. Generally, the heterocyclic atom is …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 3, 2025 · pp. 18–30 Read article
-
Determination of Compatibility of Polymer Systems and Study of Chemical Properties of their Mixtures
Abstract: We have obtained mechanical strength of materials as a result not by synthesizing new polymers, but by using industrial polymers. We have developed a technology for obtaining new composite materials based on industrial multi-tonnage polymers of high-strength polyethylene (HSPE), polyvinyl chloride (PVC), polyurethane thermoplastic elastomer (DUTEP), butyl rubber (BR), chlorocarboxylate polyethylene (CCPE), ethylene propylene rubber (EPR). To obtain a composition from these polymers, their mixture compatibility was first determined using …
Published in International Journal of Cheminformatics · Vol. 4, Issue 1, 2026 · pp. 17–29 Read article