Search
127 articles for “Fourier transform infrared (FTIR)”
-
Dosimetric Aspects of Sodium Polystyrene Sulfonate (NaPSS)
Abstract: Thermally stimulated luminescence (TSL), electron spin resonance (ESR), Fourier transform infrared spectroscopic techniques are used to study dosimetric applications of sodium polystyrene sulfonate (NaPSS). The TSL, ESR, FTIR spectra are recorded for NaPSS-exposed different amounts of gamma radiation doses. The spectra observed under different conditions suggest that the NaPSS can be used for dosimetric applications based on the condition of linear variation of physical properties against the radiation dose.
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 4, Issue 3, 2013 · pp. 7–10 Read article
-
Synthesis of Nanocrystalline Bismuth Ferrite by Solution Combustion Synthesis Method
Abstract: Normal 0 false false false EN-US X-NONE X-NONE The present paper describes a simple method of nanosized BiFeO3 by the solution combustion synthesis using bismuth and iron nitrates as oxidizers and the combination fuel of citric acid and ammonium nitrate, with fuel to oxidizer ratio (Ψ = 1) one. The average crystallite size of BiFeO3 nanoparticles was estimated from the full width half maximum of the X-ray diffraction peaks of …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 2, 2011 · pp. 52–58 Read article
-
Comparative Study of Mechanical Properties of Sisal/Epoxy, Fiber/Glass Epoxy, Sisal/Fiber Glass/Epoxy Composites
Abstract: The rate at which non-renewable resources are consumed increases, the research of using eco-friendly and sustainable materials has been in the spotlight lately. The companies from different industries are trying to find replacements for traditional synthetic materials to limit their environmental impact and promote sustainable eco-friendly initiatives. One such approach is the usage of natural fiber polymer composites as it provides a biodegradable and renewable structural alternative over traditional synthetic …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 1–11 Read article
-
Growth, XRD, FTIR and Second Order NLO studies of Undoped and Zinc Sulphate doped L-Histidine Single Crystals
Abstract: AbstractSingle crystals of pure (undoped) L-histidine and Zinc sulphate doped L-histidine have been synthesized and grown by slow evaporation method using water as the solvent. These grown crystals are characterized by FTIR, XRD and SHG. From Fourier transform infrared (FTIR) spectral analysis, the various functional groups present in the sample have been confirmed. The X-ray diffraction (XRD) study ensures that the grown crystal crystallizes in the orthorhombic system and the …
Published in Trends in Opto-electro & Optical Communication · Vol. 8, Issue 3, 2018 · pp. 31–36 Read article
-
Characterization and Gamma Irradiated MA-EMA Copolymer by ESR and FTIR Techniques
Abstract: AbstractGamma irradiation effect of methacrylamide-ethyl methacrylate (MA-EMA) copolymer has been investigated by electron spin resonance (ESR) and Fourier Transform infrared (FTIR) spectroscopic techniques. The ESR spectrum observed for gamma irradiated MA-EMA copolymer has shown resolved hyperfine (hf) pattern at lower temperatures (77K) while at higher temperatures the spectrum is appeared to be broadened. Fourier Transform Infrared spectra of pure and gamma irradiated MA-EMA copolymer have been recorded for the copolymer …
Published in Journal of Polymer & Composites · Vol. 4, Issue 3, 2016 · pp. 40–44 Read article
-
Synthesis and Characterization of Bamboo-Supported Nano Zerovalent Iron (NZVI-AB) for Cr(VI) Sequestration
Abstract: Remediation of chromium contaminated sites present both technological and economic challenges, as conventional methods are often too expensive and difficult to operate. In this study, bamboo supported Zero-valent iron (Fe0) nanoparticles were synthesized, characterized, and were tested for removal of Cr(VI). Fe0 nanoparticles were synthesized by the reduction of ferric chloride with avocado polyphenols and characterized by FTIR (Fourier transform infrared) spectroscopy and XRD (X-ray diffraction). Batch experiments were performed …
Published in Journal of Materials & Metallurgical Engineering · Vol. 10, Issue 3, 2020 · pp. 1–7 Read article
-
Modification of Ashaka and Tango Bentonites with Tetraphenyl Phosphonium and Hexadecyl Pyridinium Bromides for Possible Use in Polymer-Clay Nanocomposite Preparation
Abstract: Bentonites from Ashaka (GA) and Tango (GT) of Gombe State, Nigeria were surface modified with Tetraphenyl phosphonium (TPP) and Hexadecyl pyridinium bromides (HDP) by cation exchange method for their possible use in Clay/polymer nanocomposite preparation. The surfaces of the modified products were characterized by means of spectroscopic, diffraction and scanning methods [Fourier-transformed infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscopy (SEM)]. The basal spacing of the unmodified bentonite …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 22, Issue 2, 2020 · pp. 15–22 Read article
-
Preparation and Characterization of TiO2 Nanoparticles by Green Method
Abstract: In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 61–67 Read article
-
Influence of Gd Doping in Structural, Morphological and Optical Properties of Zno Nanostructures Synthesised Via Sol-Gel Processes
Abstract: In this study, nanocrystalline Zn1-xGdx (x=0.0 and 0.03) samples were synthesised via the Sol-gel combustion process. An array of analytical techniques was employed to examine the prepared samples to determine their different physical features. For both pristine and Gd-doped samples, the crystal symmetry is hexagonal with the P63mc space group which is verified via the Rietveld refinement analysis of X-ray diffraction (XRD) data. The atoms' bond length Zn-O and bond …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 219–225 Read article
-
Effect of Bismuth doping on Thiourea crystals : A NLO Material
Abstract: Single crystals of pure and thiourea-substituted bismuth were successfully grown using the slow evaporation solution growth technique at ambient temperature. The impact of thiourea doping on the crystal properties was thoroughly investigated. Solubility tests for the grown samples were conducted at various temperatures, providing crucial data on the dissolution characteristics. Structural characterization of these crystals was performed using single crystal X-ray diffraction (XRD), confirming their crystalline nature. Energy-dispersive X-ray spectroscopy …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 15, Issue 2, 2024 · pp. 10–16 Read article
-
Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
-
Experimental Studies on the Mechanical and Microstructural Properties of Sustainable Concrete Incorporating Palm Oil Industrial Waste
Abstract: Diving into the world of concrete, normal concrete is widely used in construction but poses environmental challenges due to significant carbon dioxide emissions from cement production. Incorporating oil palm shells (OPS) and palm oil fuel ash (POFA) into concrete offers a sustainable alternative, utilizing waste products from the palm oil industry and reducing environmental impact. Experimental studies have examined the use of OPS and POFA as partial replacements for coarse …
Published in Journal of Polymer & Composites · Vol. 12, Issue 7, 2024 · pp. 19–40 Read article
-
Biodegradation of Plastic Waste Using Various Fungal Isolates from Plastic-Polluted Sites in Meerut: Analysis of Polymers and Composites
Abstract: By isolating microorganisms from a dumpsite containing low-density polyethylene (LDPE), the potential for microbial decomposition of plastic waste was studied. Four different strains of Aspergillus niger (fungus) were identified and used to biodegrade plastic waste. The isolated fungal strains included Aspergillus niger, Alternaria, A. fumigatus, A. flavus, and A. luchuensis. Predominant fungal strains, Aspergillus niger and Alternaria, were selected for polyethylene degradation under laboratory conditions. In a controlled shaker culture, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 184–197 Read article
-
Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article
-
A non-hydrotreated feedstock’s polyaromatic cracking under FCC industrial operating conditions using an equilibrium catalyst
Abstract: Catalytic cracking of non-hydrotreated atmospheric residue’s main polyaromatic hydrocarbon (PAHs) in the presence of an equilibrium catalyst was investigated under industrial operating conditions. During the fluid catalytic cracking process, the catalyst that presented the key factor in hydrocarbon cracking (aromatic by hydrogen transfer reaction) quickly deactivated and compromised the process’s performance due to its acid surfaces and pores covered by the polyaromatic species. A deep study of the catalyst behavior …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 1, 2025 · pp. 10–26 Read article
-
Effect of Radiation Dose, Dose Rate and Annealing Temperature on Edible Potato Starch by Spectroscopic Methods
Abstract: Potato starch (PS) is a favorite food choice in different forms. During its storage and applications the PS is exposed to different radiations. In the present study the authors attempt to compare radiation effects (gamma and Electron beam of same radiation dose) in PS by Electron spin resonance (ESR) and Fourier transform infrared (FTIR) methods. ESR spectra of gamma irradiated PS appeared to have resolved shapes than the electron beam …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 198–209 Read article
-
Synthesis and Applications of Copper- Doped Pyridine Precipitate
Abstract: A metal organic nonlinear optical single crystal, copper doped pyridine material, was created at room temperature using the slow evaporation solution growth technique (SEST). The developed material's crystalline nature was revealed by a powder X-ray diffraction (XRD) analysis. Single crystal XRD study shows that the material synthesized possesses monoclinic system of cell parameters, a = 11.44 Å, b = 7.92 Å, C = 11.74 Å and alpha and gamma is …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 1, 2025 · pp. 51–60 Read article
-
Synthesis and Characterization of a Naphthalene-Derived Schiff Base for Fe³⁺ Sensing Applications
Abstract: The development of chemosensors for metal ions has gained significant attention due to their crucial role in industrial, environmental, and biological applications. Metal ion detection is essential for monitoring environmental pollution, industrial processes, and biological systems where metal homeostasis plays a vital role. In this study, we focus on the synthesis, characterization, and application of a novel naphthalene-based Schiff base ligand, derived from the condensation reaction between 1,8-diaminonaphthalene and 3-nitrobenzaldehyde. …
Published in International Journal of Cheminformatics · Vol. 2, Issue 2, 2024 · pp. 1–8 Read article
-
Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article
-
Synthesis of Thermal Resistant and Transparent Al2O3 Reinforced Epoxy-Based Composite Coatings
Abstract: This study explores the influence of thermal treatment on the structural, optical, and surface wettability characteristics of epoxy-based composite coatings reinforced with 3 wt.% aluminum oxide (Al₂O₃) nanoparticles. The coatings were synthesized via a dip-coating method on carbon fiber substrates and subjected to controlled thermal treatments at 300 °C, 400 °C, and 500 °C to assess their thermal resilience. X-ray diffraction (XRD) analysis confirmed the structural integrity of the composite …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 178–183 Read article