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44 articles for “FESEM”
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Morphological and Optical Characterization of Zinc Sulphide Nanostructure Synthesized by Green Route of Musa Peels
Abstract: AbstractZinc sulphide nanoparticles are very good candidate for optoelectronic applications. In this paper we have reported green synthesis of zinc sulphide nanoparticles using Musa peels available in abundance as organic waste. Various precursor ratios and various extract concentrations were used. The samples obtained were analyzed using optical and morphological characterization. Strong blue shift in absorption edges was observed for increasing concentration of thiourea. It also was influenced by concentration of …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 7, Issue 2, 2017 · pp. 23–28 Read article
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A Benign Route for the Synthesis of MgO Nanoparticles and Their Antifungal Activity
Abstract: Magnesium oxide nanoparticles (MgO NP’s) with particle size 50±10 nm were prepared by hydrothermal method and further characterized by X-ray Diffractometry (XRD) and high resolution field emission scanning electron microscopy (FESEM). The prepared MgO NP’s were also evaluated for their antifungal activity against Trichothecium roseum, Cladosporium herbarum, and Alternaria alternata. The antifungal activity of the synthesized nanoparticles against the selected fungi was assessed as reduction in spore germination and by …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 23, Issue 3, 2021 · pp. 37–44 Read article
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The Formation of Bi-2223 Superconductor with Fe-Substitution
Abstract: Presently, we have studied about synthesis and characterization of Bi-2223 Superconductors in the form of Bi2Sr2Ca3(Cu0.97Fe0.03)3O10+δ complex. The sample was established with solid state method and characterized by XRD, (FESEM) and (FTIR). The DC electrical resistivity of the sample was measured at liquid helium temperature. The XRD parameters shows the orthorhombic structure with lattice constant a = 5.7429Å, b = 5.0845 Å, c = 36.5569 Å and grain size confirm …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 2, 2020 · pp. 32–41 Read article
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A New Approach of Synthesis Fe-Substituted Bi-2223 Superconductors
Abstract: Generally, the Bismuth based high temperature superconductors are utilizing in three phases as Bi-2201, Bi-2212 and Bi-2223. These have different transition temperature according to superconducting phase. Here, we studied about Bi-2223 phase by using complex Bi2Sr2Can-1 (Cu1-xFex)3O10+δ where n = 3. In this complex, we has been doped iron in Coper (Cu) site (x = 0.07%). This sample was prepared by solid state reaction method. The planetary Ball mill was …
Published in Research & Reviews : Journal of Physics · Vol. 10, Issue 3, 2021 · pp. 22–29 Read article
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Experimental Investigation of Micro-Hardness & Tribological Behavior of Composite Coating for Wear Resistance Application
Abstract: The author effectively created a composite coating with enhanced durability utilizing the HVOF technique in this investigation. The automobile business has encountered fierce worldwide rivalry, rapid technical breakthroughs, and strict regulatory regulations in recent year.. Producers of lubricants, gasoline additives, and worldwide original equipment manufacturers (OEMs) are striving to address the difficulties presented by changing consumer preferences and emerging energy conservation and environmental protection regulations. We have successfully created and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1097–1103 Read article
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Green Fabrication of Glutaraldehyde-Crosslinked Chitosan/PVA Biocomposite for Heavy Metal Removal from Wastewater
Abstract: Chitosan (CS) and Polyvinyl alcohol (PVA) are polymers that possess biodegradable, biocompatible, and non-toxic properties, making them suitable for wastewater treatment applications. The primary objective of this research is to chemically modify chitosan in a novel manner to enhance its ability to remove hexavalent chromium Cr(VI) from aqueous solutions. In this study, a composite material was synthesized by crosslinking PVA and CS with glutaraldehyde (GA), resulting in the formation of …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 59–83 Read article
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Fabrication and Assessment of Tribological Performance of Nickel-Graphene-MXene Hybrid Nano-composites
Abstract: As industries such as aerospace, automotive, defence, and electronics demand materials with superior wear resistance, high strength, and thermal stability, traditional metals are reaching their performance limits. Hybrid nanocomposites offer a pathway to meet these stringent requirements. In this study, novel Nickel-Graphene-MXene hybrid nanocomposites were fabricated using a powder metallurgy route, incorporating varying weight percentages (up to 2 wt.%) of MXene and 1 wt.% graphene nanosheets into a nickel matrix …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 780–798 Read article
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Ag₂S–Ag Nanocomposites: A Bottom-Up Approach to Enhance Thermoelectric Power Factor at Near Room Temperature
Abstract: The intrinsic ductility, low toxicity, and naturally occurring abundance of silver sulphide (Ag₂S) have made it a potential thermoelectric material in recent years. However, high electrical resistance severely limits its practical application. Here, we present a thorough analysis of how metallic Ag nanoinclusions affect the structural, electrical, and thermoelectric characteristics of Ag₂S nanocomposites made using a simple bottom-up polyol approach. (Ag₂S)₁₋ₓAgₓ nanocomposites with an Ag content ranging from 0 to …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 4, Issue 1, 2026 · pp. 40–55 Read article
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Polymer-Coated Composite Granules of Clarithromycin: Design, Characterization, and Functional Evaluation for Taste Masking and Antibacterial Performance
Abstract: Background: Masking the unpleasant taste of clarithromycin is essential to improve patient adherence, especially among pediatric and elderly groups. However, enhancing palatability while maintaining its antibacterial effectiveness remains a significant formulation challenge. This study focused on developing polymer-coated clarithromycin granules (B1–B10) using novel non-sugar-based polymers and assessing their antibacterial activity against Staphylococcus aureus Methods: Clarithromycin granules were produced using a fluidized bed coating technique with non-saccharide polymers, specifically Eudragit E-100 …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1042–1050 Read article
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Effect of Voltage on Aluminium Nanopore Images using Digital Image Processing Techniques
Abstract: Research on nanotechnology, by and large is dedicated to ordered, controlled and customized fabrication of nanopores. The proposed study emphases on groping the morphology of alumina through FESEM images and characterization using automatic tool developed using image processing software. The proposed automatic tool measures the effect of variable voltage (35, 40 and 45 V) on alumina at constant concentration (4.7%), time (8 min) and temperature (5oC). It has been observed …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 8, Issue 3, 2018 · pp. 8–14 Read article
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Structural Investigation on Synthesized Ag Doped ZnO-MWCNT and its applications
Abstract: Metal doped multiwalled carbon nanotube with metal oxide has unique properties which provide the remarkable studies in the field many applications. Zinc oxide nanoparticles (ZnO NPs) is a semiconducting material with a large excitation binding energy of 60 meV and wide energy band gap of 3.367 eV. The doping of silver naoparticle with ZnO/MWCNT composite materials offer values and makes it as advanced multifunctional materials. Silver nanoparticles are a highly …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 8, Issue 2, 2018 · pp. 49–59 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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Characterization of Al6082 and Magnesium AZ3lB Composite Produced by The Friction Stir Additive Manufacturing
Abstract: In this modern era, lighter and stronger materials are needed. This is especially true for materials needed in aerospace, robotics, light aircraft, defence, and transportation. When comparison to backbone products in order composite goods have a higher durability & stiffness-to-weight proportion .Most of the newer fabricating methods, called friction stir additive manufacturing (FSAM), uses solid-state drives friction stirring technology to produce bilayer structures by sequentially fusing discrete strata. In this …
Published in International Journal of Manufacturing and Production Engineering · Vol. 1, Issue 1, 2023 · pp. 1–14 Read article
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Green synthesis of Ag-Fe2O3-CuO-PANI nanocomposite and its application as an Apple Vinegar sensor
Abstract: Green synthesis of nanoparticles is inexpensive and environmentally safe, herein we report green approach for the synthesis of Ag, Fe2O3, CuO nanoparticles by using Asparagus Racemosus plant to detect carboxylate vapours. Synthesized Ag, Fe2O3, CuO nanoparticles were taken in 1:1:1 ratio and PANI (polyaniline) was added in ratio 5:1 to form Ag-Fe2O3-CuO–PANI nanocomposite. Synthesized Ag-Fe2O3-CuO-PANI were characterized by XRD, FESEM and FTIR whose size was in the range of 16–60 …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 41–53 Read article
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Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article
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Process Parameters Optimization of Fiber Laser Cladded SS316 Surface Using RSM Analysis
Abstract: This paper presents the laser cladding experiments on the surface of SS316 to study the variations in process parameters, such as scanning speed (100-250 mm/min), laser power (50-250 W), and % volume of B4C (5- 25%) + SS316 powder on the mechanical, metallurgical and tribological performance of the modified surface. A central composite design (CCD) was used to develop the response surface methodology (RSM) to design the experiments and for …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 186–201 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 45–59 Read article
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Comparative Study of Structural, Optical, Morphological, and Magnetic Properties of BifeO3 Nanoparticles Synthesized Via Green and Chemical Methods
Abstract: BiFeO3 nanoparticles were synthesized via a green route using Strychnos nux-vomica leaf extract and a conventional chemical sol–gel method to study the effect of synthesis routes on their properties. XRD analysis confirmed phase-pure rhombohedral BiFeO3 for both samples. FTIR analysis was carried out to confirm the formation of the perovskite structure and to detect surface functional groups. FESEM analysis indicated a significant effect of phytochemicals in controlling particle growth and …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 1, 2026 · pp. 1–8 Read article
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High-Performance Carbon Nanotube-Reinforced Biodegradable Polymer Composites for Packaging
Abstract: The growing issues concerning the properties of petroleum-based plastics on the environment increased the demand for biodegradable alternatives and polylactic acid (PLA) is one of the most promising options available. However, its poor toughness, thermal resistance, and barrier properties limit broader applications in sustainable packaging. This study reports the fabrication and characterization of PLA-based nanocomposites reinforced with carbon nanotubes (CNTs) at varying loadings (0.1-2 wt.%). Structural analysis (FTIR, XRD) confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 183–194 Read article
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Comparative Study of Structural and Optical Properties of Bismuth Ferrite Nanoparticles for Photovoltaic Applications Synthesized via Different Sol-Gel Methods
Abstract: Pure multiferroic bismuth ferrite (BiFeO3) nanoparticles were successfully synthesized using an energy-efficient, low-temperature sol-gel method, comparing two distinct approaches: auto-combustion and non-auto-combustion. To ensure phase stability, the precursor solution's pH was strictly maintained between 1 and 2 using ammonia solution (NH4OH), while ethylene glycol (C2H6O2) was employed as a chelating agent for the Fe3+ and Bi3+ cations. All samples underwent a final annealing process at 500 °C to promote crystallization. …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 83–94 Read article