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149 articles for “Crystals and Sizes”
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Synthesis and Surface Studies of ZnS/PVK Nanocomposites
Abstract: ZnS/PVK nanocomposites have been successfully prepared by chemical method. The optical and electrical properties of nanomaterials can be controlled by their particle size and therefore attracted much interest for their fundamental and applied aspects. The sizes of the particles were varied with different ZnS concentrations. The XRD pattern showed that the ZnS nanoparticles have zinc-blend structure and line broadening suggests the formation of the amorphous compound. The observations show that …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 20, Issue 2, 2018 · pp. 1–8 Read article
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Doping of Metal Precursors on Cadmium Selenide Quantum dots—A Review
Abstract: In this article, we review effects of doping on Cadmium-Selenide (CdSe) Quantum dots (QDs). Different dopants critically influence the properties and functionalities of nanocrystals (QDs). It is of strong interest to understand the structural characteristics of dopants and how they interact with the QDs. Differently, doped CdSe QDs were characterized by X-ray diffraction (XRD) technique, UV-Visible absorption spectroscopy, photoluminescence (PL) spectroscopy. The important results and measurements are discussed. CdSe quantum …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 7, Issue 3, 2017 · pp. 1–4 Read article
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Synthesis and Synergistic Effects of Ciprofloxacin Conjugated Zinc Oxide Nanoparticles
Abstract: Zinc oxide nanoparticles (ZnO NPs) are known as a multifunctional material because of its unique physical and chemical properties. The result of zinc oxide nano powder was characterized using various analytical techniques, such as UV-Vis spectroscopy, Fourier Transform Infra-Red (FTIR), Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD) patterns. Synthesized zinc oxide nano powder was stored in dried form in the room temperature for further study. …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 1, 2019 · pp. 61–71 Read article
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Chemical Synthesis of Zinc Oxide Nanoparticles and Characterization
Abstract: Chemical precipitation method was followed to synthesize zinc oxide nanoparticles. Zinc acetate and ethylene glycol were used in the preparation, and polyvinyl alcohol was also used along with zinc acetate to control the size and morphology. The precipitated particles were subjected to oxidation. The ZnO nanoparticles were characterized by analytical methods like XRD, FTIR, DLS, AFM, SEM and TEM. ZnO nanoparticles had crystal-like structures with size range of 6.17 to …
Published in Journal of Materials & Metallurgical Engineering · Vol. 3, Issue 2, 2013 · pp. 14–20 Read article
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Studies in Effect of Methyl Methacrylate to Butylacrylate Ratio on the Properties of TiO2/poly(methyl methacrylate-co-butylacrylate) Core–Shell Composite Nanoparticles Prepared by Microemulsion Polymerization
Abstract: AbstractTitanium dioxide, as a core, was coupled with the poly(methyl methacrylate-co-butyl acrylate) using amino propyltriethoxy silane as a coupling agent. A two-stage semi-continuous microemulsion polymerization method was used for the synthesis of these core–shell nanoparticles. Ratio of methyl methacrylate to butyl acrylate was varied in the shell of the nanoparticles and the prepared core–shell composite nanoparticles were characterized by Fourier transform infrared spectroscopy, X-ray diffractometer, differential scanning calorimetry, scanning electron …
Published in Journal of Polymer & Composites · Vol. 1, Issue 3, 2013 · pp. 32–39 Read article
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Preparation and Characterization of Aluminium Doped ZnO Thin Films by Spin Coating Technique
Abstract: In this work, the preparation of Al-doped ZnO (AZO) thin films by the sol-gel spin-coating method is reported. The structural properties and surface morphologies of film prepared at RT were characterized by X-ray diffraction (XRD) and field emission scanning electron microscope (FE-SEM). The XRD and SEM results disclosed that the crystallization quality and grain size of as-prepared films were highly influenced by Al doping. Laser Raman Spectrometer results indicated that …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 7, Issue 2, 2020 · pp. 16–22 Read article
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Synthesis, Characterization and Applications of Poly (2-Methyl Aniline-co-2-Chloro Aniline) and Poly (2-Methyl Aniline-co-2-Chloro Aniline)-Nanocomposite-CuO
Abstract: The copolymer and its composite, poly (2-methyl aniline-co-2-chloro aniline) and poly (2-methyl aniline-co-2-chloro aniline)-nanocomposite-CuO respectively were synthesized by chemical oxidative polymerization method using ammonium persulphate as oxidant, sodium lauryl sulphate as surfactant and HCl as dopant. The synthesized copolymer and composite were characterized by FTIR, UV-Visible and 1H NMR spectroscopy. The thermal stability was determined by TGA/DTA. The copolymer and copolymer nanocomposite with CuO were found to be thermally more …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 7, Issue 3, 2016 · pp. 35–45 Read article
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Study of CdS/AZO/FTO, CdS/FTO and CdS Thin Films Deposited by Modified Double Layer Thermal Evaporation
Abstract: The CdS/AZO/FTO, CdS/FTO and CdS thin films were deposited by a modified double-layer vacuum evaporation technique. The 90 nm of double-layer CdS thin films were prepared with the bottom layer 50 nm thick and the upper one was 40 nm thick and respective substrate temperatures were 100oC and 70oC. The physical properties of thus prepared films were characterized using X-ray diffraction (XRD), UV-VIS-NIR spectrophotometer, Hall Effect Measurement System and Scanning …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 2, 2019 · pp. 56–63 Read article
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Synthesis and Characterization of Nickel doped Barium Niobate Ba (Ni0.5Nb0.5)O3 (BNN) Nanomaterial
Abstract: AbstractFerroelectric materials are of great interest for researchers worldwide, because of their unique physical properties and wide range of applications. The composite nanomaterial Ba(NiNb)0.5O3 (BNN) was synthesized by conventional solid state reaction method. The structural characterization was done by x-ray diffraction (XRD). The research was carried out to investigate structural properties of BNN nanomaterial as a function of sintering duration. BNN was sintered at 10000C and different samples were prepared …
Published in Journal of Microelectronics and Solid State Devices · Vol. 5, Issue 2, 2018 · pp. 29–33 Read article
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Exploration of Copper Oxide PVA/PEG Paraffin Polymer Composites for Enhanced Thermal Performance of Nano-Enhanced Phase Change Materials and Their Environmental Impact
Abstract: This study investigates the synthesis, characterization, and application of copper oxide (CuO) nanoparticles integrated into polymer-based paraffin wax composites for advanced thermal management applications. CuO nanoparticles were synthesized using a wet chemical approach and characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and dynamic light scattering (DLS), confirming their crystalline structure, morphology, and nanoscale size distribution. The synthesized nanoparticles were incorporated into polymer-supported phase change …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 156–173 Read article
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Activated Carbon Materials as Ideal Adsorbents for the Desulfurization of Fossil Fuels
Abstract: Removal of organosulfur compounds from diesel is of interest from scientific, social, economic, and environmental viewpoints. Production of clean fuel remains a primary goal of the petroleum refining industry. The reduction of sulfur content below stringent ppm levels in diesel fuels becomesincreasingly challenging due to the presence of sterically hindered sulfur compounds, such as 4,6- dialkyldibenzothiophenes, which are resistant to removal over conventional supported mixed sulfide hydrodesulfurization catalysts. Consequently, alternative …
Published in International Journal of Pollution: Prevention & Control · Vol. 4, Issue 1, 2026 · pp. 28–34 Read article
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Synthesis of YSZ nanopowders by using PVA-metallic nitrate combustion method
Abstract: Yttria-stabilized zirconia (8YSZ) powder is widely used as a thermal barrier coatings material for various aeronautical gas turbine engine components and structures operating in high temperature environment as well as for the nozzle of solid rocket engine due to its relatively high thermal expansion coefficient, thermal reflectivity, low thermal and good corrosion resistance. The synthesis of single or composite metal oxides by combustion of metal-polyvinyl alcohol gel precursors (Me-PVA) has …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 14, Issue 3, 2024 · pp. 24–32 Read article
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The Effect of Rare Earth (RE) Metal Doping of Zno, On Magnetic and Optical Properties of Zno Crystals Structure
Abstract: The magnetic and optical properties of magnetic semiconductors relays on the crystal structure, type and amount of dopant ions, and particle size. Then, the effect of rare earth metal (Dy, Eu, and La) doping on crystal structures, magnetic properties and optical properties are seen. It is revealed that the optical band gap of ZnO decrease down from 3.37eV up on doping with RE metals. Then, the Hamiltonian of the system …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 28–40 Read article
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Advanced x-Ray Analysis for Less-Crystalline Materials
Abstract: An effort to manufacture materials with the least and precise radar signature for stealth and controlled guidance respectively, inevitably requires advanced techniques to characterize materials, for detecting the confinement of crystallinity in still smaller volumes, to estimate entity sizes, unwanted noise and structure factors. Raison d’etre for selection of advanced and special materials with less crystallinity, combined with control over precise weathering, to minimize crystal development, for acquiring stealth and …
Published in Journal of Aerospace Engineering & Technology · Vol. 12, Issue 1, 2022 · pp. 8–12 Read article
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Study of Nano Germanium and Composited Forms
Abstract: This article has reviewed refinement synergism to same as earlier bulk semi-conduction. Colloidal 5 nm suspension from photolysis and pyrolysis for aerogel of II-VI quantum dots has subsidized extinction contour of semiconductor nano-crystal. Thereby transitional has accused between 0.6 to 5 eV to access from size-dependent optical and electrical effect instead of precipitation technique. Structure-oriented electronic and optical property has relevance to nano-semiconductor preparation method synergistic to earlier bulk. Nano-crystals …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 8, Issue 2, 2021 · pp. 8–15 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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Synthesis and Ion Transport Studies of a New Potassium Ion-Conducting Nanocomposite Polymer Electrolyte
Abstract: The pursuit of safe, efficient, and sustainable energy storage solutions has intensified research on nanocomposite polymer electrolytes, especially for next-generation battery technologies. This work reports the synthesis and ion transport characteristics of potassium ion-conducting nanocomposite polymer electrolytes (NCPEs), emphasizing their structural, electrical, and electrochemical performance. To enhance ionic conductivity and mechanical strength, polymer matrices were reinforced with nanoscale ceramic fillers. A new potassium ion-conducting NCPEs: (1-x)[70PEO:30KCl] + x SiO₂ (where …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1496–1504 Read article
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High-strength Indian Kaolin Development by Adding Vanadium Pentoxide (V2O5) by Sol-gel Method
Abstract: The development of high strength in Indian kaolinite has been studied in the presence of vanadium pentoxide. It is observed that the strength of Indian kaolinite is increased with addition of V2O5 by sol-gel techniques and characterized by Vickers hardness, X-ray diffraction and scanning electronmicroscopy studies. The kaolinite was compacted with different proportions of V2O5 additives and sintered at four different high temperatures. It was observed that V2O5 showed a …
Published in Journal of Catalyst & Catalysis · Vol. 10, Issue 1, 2023 · pp. 28–32 Read article
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Exposure of Nanoparticle Leads to Health Hazards
Abstract: Nanotechnology is a technique used for the production of materials of the nanoscale level. This is a new development in technology which usually entails some hazards as well as advantage to society. Thus nanomaterials are well known for their various beneficial uses in the medicines, engineering, computer, etc., in spite of that it is associated with many hazards related to human health. The exposure of nanomaterials through dermal contact, inhalation, …
Published in Research and Reviews: A Journal of Toxicology · Vol. 9, Issue 3, 2019 · pp. 7–18 Read article
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Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article