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66 articles for “X-ray powder diffraction”
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Synthesis and Synergistic Effects of Ciprofloxacin Conjugated Zinc Oxide Nanoparticles
Abstract: Zinc oxide nanoparticles (ZnO NPs) are known as a multifunctional material because of its unique physical and chemical properties. The result of zinc oxide nano powder was characterized using various analytical techniques, such as UV-Vis spectroscopy, Fourier Transform Infra-Red (FTIR), Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD) patterns. Synthesized zinc oxide nano powder was stored in dried form in the room temperature for further study. …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 1, 2019 · pp. 61–71 Read article
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Fabrication and Comparative Study of Synthetic and Eggshell Waste Derived Hydroxyapatite-Based Composites for Biomedical Applications
Abstract: Hydroxyapatite is widely used as a bioceramic material in orthopedic and dental field because of its exceptional biocompatibility and bioactivity. Hydroxyapatite (HAp) doped with several mineral ions has been frequently reported to further enhance its bioactive nature. Several studies indicate that biological waste materials can serve as calcium sources for hydroxyapatite synthesis, with eggshells being one such promising source. In the present work, two types of hydroxyapatite were synthesized: pure …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 33–46 Read article
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Combustion Synthesis of NiO-YSZ Precursor Nanocomposites for SOFC Anode and Its Characterization
Abstract: In the present work, the mixture of Nickel Oxide-Yttria Stabilized Zirconia (NiO-YSZ) composites of composition, mNiO–(1–m) Zr0⋅9Y0⋅1 O1⋅95 (m = 0⋅4), anode materials was synthesized by combustion process using glycine as fuel and nitrate as oxidizer. The study of prepared nanocomposites has been done by Fourier transform infrared spectroscopy (FTIR), differential thermal analysis-thermo gravimetric analysis (DTA-TGA), X-ray diffraction (XRD) and scanning electron microscopy (SEM) to determine the powder properties. The …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 3, 2012 · pp. 1–9 Read article
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A Comparative Study of Plant Mediated Synthesis of Silver, Copper and Zinc Nanoparticles from Tiliacora acuminata (lam.) Hook. F. and Their Antibacterial Activity Studies
Abstract: Green synthesis of nanoparticles is becoming more and more popular due to its compensation over physical or chemical methods. This research was carried out to the synthesis of nanoparticles employing three different metals (silver nitrate, copper and zinc sulphate) using Tiliacora acuminata (family: Menispermaceae) fruit powder. The synthesized nanoparticles were characterized through the UV-Vis Spectrophotometer, FT-IR and X-Ray Diffraction studies. The antibacterial activity of nanoparticles was studied against disease causing …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 1, 2019 · pp. 72–83 Read article
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Synthesis and Characterization of Forsterite Incorporated HDPE Composites for Microwave Substrate Application
Abstract: High Density Polyethylene (HDPE) combined with dispersed forsterite (Mg₂SiO₄) powder was utilized to fabricate polymer matrix composites (PMCs) aimed at high-frequency microwave substrate applications. Forsterite powders were synthesized using the mixed oxide method, and their phase purity was confirmed by X-ray diffraction (XRD) analysis. The dispersion and morphology of the ceramic filler within the HDPE matrix were examined through Scanning Electron Microscopy (SEM), ensuring a homogeneous distribution essential for optimal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 109–120 Read article
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Corrosion Resistance of HVOF and Plasma Sprayed Ni-Cr/WC-Co Coatings
Abstract: In this work, Ni-Cr/WC-Co composite coating with an approximate thickness of appr. 100 µm was produced by atmospheric plasma and HVOF thermal spraying on SS 304 substrate. The main objective was to characterize the Ni-Cr/WC-Co coating. The microstructure and composition of powder and coatings were studied by Scanning Electron Microscopy (SEM), Optical Microscope and X-ray diffraction (XRD). The coating characteristics such as porosity, and micro-hardness were evaluated. Finally the corrosion …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 1, Issue 2, 2014 · pp. 51–57 Read article
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Structural, Magnetic and Dielectric Properties of Barium Cobalt Hexaferrite-powder and Barium Cobalt Hexaferrite- Epoxy Resin Composite Film
Abstract: The W-type barium cobalt hexaferrite powder with chemical composition BaCo2Fe16O27 was prepared using a simple heat treatment method. The precursor was calcinated at 650 °C for 3 h in a muffle furnace and then slowly cooled to room temperature in order to obtain barium cobalt hexaferrite powder. The flexible epoxy thin film of Ba-cobalt hexaferrite/epoxy composite was fabricated using the suitable amount of hardener and curing agent. Surface and morphological …
Published in Journal of Microelectronics and Solid State Devices · Vol. 1, Issue 1, 2015 · pp. 14–20 Read article
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Impact of Sol–Gel Processing on Dielectric and Energy Storage Properties of BaTiO3 Nanoceramics
Abstract: Barium titanate (BaTiO3) is a widely studied ferroelectric material because of its high dielectric permittivity and strong potential for electrostatic energy storage applications. In this study, BaTiO3 nanoceramics were synthesized using a controlled sol–gel processing route to investigate the influence of synthesis conditions on their dielectric relaxation and energy storage performance. The synthesized powders were calcined and subsequently sintered at temperatures ranging from 1100°C to 1300°C. Structural analysis using X-ray …
Published in Research & Reviews : Journal of Physics · Vol. 15, Issue 2, 2026 · pp. 11–25 Read article
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Structural and Dielectric Properties Hexaferrite/Poly (Vinyl Alcohol) Composites
Abstract: Magnetic barium cobalt hexaferrite particles-PVA composites with of different mass ratio: 9:1, 8:2, 7:3, 6:4 and 5:5 were prepared. Structural properties of the composites were characterized by Infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscope (SEM). The effect of the concentration of Ba2Co2Fe28O46 hexaferrites on structural and dielectric properties of magnetic-PVA composites were investigated. FTIR result revealed that composite samples show absorption peaks of both ferrites and PVA. …
Published in Research & Reviews : Journal of Physics · Vol. 2, Issue 3, 2013 · pp. 10–19 Read article
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Processing and Mechanical Characterization of Compression-Molded Ultrahigh Molecular Weight Polyethylene Biocomposite Reinforced with Aluminum Oxide
Abstract: Ultrahigh molecular weight polyethylene (UHMWPE) has been widely used as a bone implant material in orthopedic surgical applications in trauma due to its low coefficient of friction, good biocompatibility, and excellent wear and corrosion resistance properties in comparison to other polyolefins. But, due to the formation of wear debris, implants loosen and fail after 12–15 years of implantation. In order to enhance lifespan, the role of alumina (Al2O3) reinforcement on …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 4, Issue 3, 2014 · pp. 1–12 Read article
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Synthesis and Characterization of Zinc-doped CdO Nanopowder Prepared by Mechanochemical Method
Abstract: Zinc-doped cadmium oxide nanopowders with various Zn concentrations have been prepared using mechanochemical method. The structure and morphology of the as-prepared samples are investigated by means of X-ray diffraction (XRD), Scanning electron microscopy (SEM) and Energy dispersive spectroscopy (EDS). The XRD result indicates that the average size of Zn-CdO powder is in nano range having a desired cubic phase. Surface morphology of sample is determined by scanning electron microscopy (SEM) …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 17, Issue 1, 2015 · pp. 26–31 Read article
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Investigations into the Mechanical and Thermal Properties of Fe3C Compound: A Comprehensive Analysis
Abstract: Exploration of mechanical properties of Fe3C powder using Williamson-Hall analysis by using Mechanical alloying technique. The primary objective of this study is to investigate the lattice strain (LS) and nanocrystalline size (CS) in an Fe3C produced from powder using the Mechanical Alloying Method (MAM). By the repeated mechanical crushing, the LS created by MAM is expected to decrease while the CS is anticipated to reduce the particle size. To accomplish …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 225–234 Read article
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Structural and Electrical Characterization of Mn-Zn Substituted CaSr2: W-Type Hexaferrite
Abstract: AbstractIn the present investigation the samples with chemical composition CaSr2 (Mn-Zn)x/2Fe16- xO27 (x= 0.2, 0.4, 0.6, 0.8, 1.0) have been synthesized by using chemical co-precipitation method. X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used to study structure, lattice constants, crystallites size, x-ray density, bulk density, porosity and shape of ferrite powders. The prepared samples were found to have W-type hexagonal structure with the lattice parameters a= (5.77 Å–5.82 …
Published in Research & Reviews : Journal of Physics · Vol. 5, Issue 1, 2016 · pp. 11–17 Read article
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A New Approach of Synthesis Fe-Substituted Bi-2223 Superconductors
Abstract: Generally, the Bismuth based high temperature superconductors are utilizing in three phases as Bi-2201, Bi-2212 and Bi-2223. These have different transition temperature according to superconducting phase. Here, we studied about Bi-2223 phase by using complex Bi2Sr2Can-1 (Cu1-xFex)3O10+δ where n = 3. In this complex, we has been doped iron in Coper (Cu) site (x = 0.07%). This sample was prepared by solid state reaction method. The planetary Ball mill was …
Published in Research & Reviews : Journal of Physics · Vol. 10, Issue 3, 2021 · pp. 22–29 Read article
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Synthesis and Characterization of Ta Doped Nanostructured PZT
Abstract: Lead Zirconate Titanate (PZT) powder of composition Pb(Zr0.65Ti0.35)O3 was modified by incorporation of Tantalum (Ta5+) in a wide composition range (5–25 at%) by chemical co-precipitation method using PbO, Zr2O3, TiO2 and Ta2O5. X-ray diffraction patterns of the samples showed the formation of a single phase and confirmed the formation of a rhombohedral phase of all the samples after sintering. SEM analysis showed well-developed, uniformly packed grains. Both the linear particle …
Published in Journal of Materials & Metallurgical Engineering · Vol. 3, Issue 2, 2013 · pp. 41–48 Read article
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Enhancing Concrete Strength: Investigating the Impact of Glass Fines on Mechanical Properties
Abstract: The global emission of CO2 from cement industries poses a significant environmental challenge, being a primary contributor to environmental issues. Numerous researchers have explored alternative cementitious materials to formulate robust and long-lasting concrete. This study focuses on utilizing waste glass powder (GlP), derived from rejected soda-lime glass bottles collected from various sources, for experimental purposes. The laboratory experiments investigate the behavior of concrete incorporating glass as a partial substitute for …
Published in Recent Trends in Civil Engineering & Technology · Vol. 13, Issue 3, 2023 · pp. 15–23 Read article
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Growth, XRD, FTIR and Second Order NLO studies of Undoped and Zinc Sulphate doped L-Histidine Single Crystals
Abstract: AbstractSingle crystals of pure (undoped) L-histidine and Zinc sulphate doped L-histidine have been synthesized and grown by slow evaporation method using water as the solvent. These grown crystals are characterized by FTIR, XRD and SHG. From Fourier transform infrared (FTIR) spectral analysis, the various functional groups present in the sample have been confirmed. The X-ray diffraction (XRD) study ensures that the grown crystal crystallizes in the orthorhombic system and the …
Published in Trends in Opto-electro & Optical Communication · Vol. 8, Issue 3, 2018 · pp. 31–36 Read article
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Fabrication of Nanocrystalline Fe2Mn2Ni2Zn2O11 at Different Calcination Temperatures and Its Analysis
Abstract: The superconducting nanocrystalline ceramic powder Fe2Mn2Ni2Zn2O11 was designed and fabricated by a high-temperature special furnace. In the area of ceramic superconductors, particle size is an important factor. Here the authors analyzed the particle size and strain of the nanocrystalline ceramic super conducting material. The sample was analyzed by X-ray Diffraction (XRD), particle size determination, SEM and EDX. The comparison of XRD results with JCPDS files confirmed the orthorhombic structure of …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 16, Issue 3, 2014 · pp. 8–15 Read article
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Development and Characterization of a Solid Dispersion of an Anti-Diabetic Drug Using Pectin as a Natural Polymer
Abstract: Aim: The current study sought to improve the solubility and oral bioavailability of gliclazide by creating solid dispersions and oral dispersible tablets (ODTs) with enhanced physicochemical characteristics and maintained antidiabetic action. Methods: Preformulation studies were conducted to evaluate the physicochemical properties of gliclazide, including physical appearance, melting point, solubility, and partition coefficient. Solid dispersions were prepared using hydrophilic carriers-pectin and PVP K30, and subsequently characterized by Fourier Transform Infrared Spectroscopy …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 17, Issue 2, 2026 · pp. 01–12 Read article
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Dielectric Studies of 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 Nanoceramic Fabricated by Chemo-mechanical Process
Abstract: The present investigation is aimed toward investigate a straightforward, inexpensive, and environmentally friendly chemo-mechanical method for preparing high-dielectric materials, specifically 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 (BCT-CCTO), by combining metal nitrate combustion with solid TiO2 powder and titanium isopropoxide, Ti (OR)4. The composite was prepared by the mixing of individual materials of Ba0.8Ca0.2TiO3 and CaCu3Ti4O12 through the chemo-mechanical method. Initially, 99% pure Ba (NO3)3, Cu (NO3)2∙3H2O, TiO2 and glycine were taken in their stoichiometry ratios. …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 12–21 Read article