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163 articles for “X-Ray”
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
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Ag₂S–Ag Nanocomposites: A Bottom-Up Approach to Enhance Thermoelectric Power Factor at Near Room Temperature
Abstract: The intrinsic ductility, low toxicity, and naturally occurring abundance of silver sulphide (Ag₂S) have made it a potential thermoelectric material in recent years. However, high electrical resistance severely limits its practical application. Here, we present a thorough analysis of how metallic Ag nanoinclusions affect the structural, electrical, and thermoelectric characteristics of Ag₂S nanocomposites made using a simple bottom-up polyol approach. (Ag₂S)₁₋ₓAgₓ nanocomposites with an Ag content ranging from 0 to …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 4, Issue 1, 2026 · pp. 40–55 Read article
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Carbon-Coated Te-Doped Bi₂Se₃ as a Topological Quantum Anode Material for Sodium-Ion Batteries
Abstract: Sodium-ion batteries (SIBs) are increasingly investigated as cost-effective alternatives to lithium-ion systems for large-scale energy storage; however, the development of stable and conductive anode materials remains a major challenge. In this work, tellurium-doped bismuth selenide (Te-doped Bi₂Se₃) was synthesized and further modified with Super P conductive carbon to improve its sodium-storage behavior. The phase formation and structural retention of the active material were examined using X-ray diffraction, while elemental mapping …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 · pp. 55–61 Read article
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Preparation and characterization of High-performance ZnO/PVB Nanocomposite films for UV-shielding and Optoelectronics
Abstract: Zinc oxide nanoparticles can be incorporated into polymer matrices to create materials for various high-performance engineering applications. In this study, zinc oxide nanoparticles were reinforced at different loadings (0.5, 1.0, 0.5, 1.0, 1.5, and 2.0 wt.%) in polyvinyl butyral matrix to synthesize nanocomposite films using the solution casting method. The impact of zinc oxide nanofiller on the morphology and ultraviolet-shielding performance of polyvinyl butyral nanocomposite films was evaluated using various …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 27, Issue 3, 2025 · pp. 35–53 Read article
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Synthesis and Photoluminescence Dynamics of Europium (III) and Terbium (III) Co-doped of GdSrAl3O7 Color-Tunable Nanophosphors
Abstract: A series of Europium (III) and Terbium (III) co-doped GdSrAl3O7 color-tunable nanophosphors were synthesized by a simplistic, streamlined and self-propagating, urea-assisted solution combustion synthesis process. The structural and luminescence characteristics of synthesized Eu3+/Tb3+ co-doped Gadolinium Strontium Aluminate nanocrystalline phosphors were validated using powder X- ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X- ray analysis (EDAX), and photoluminescence spectra studies. The morphological studies revealed that …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1069–1082 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article
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Combustion Synthesis and Comprehensive Characterization of Pure and Ni-Doped CuFe₂O₄ Nanoparticles for Functional Composite Applications
Abstract: The CuFe2-xNixO4 (x = 0, 0.1, 0.3, and 0.5) nanoparticles were synthesized using a combustion method and comprehensively characterized to understand their suitability for polymer-based composite applications. X-ray diffraction confirmed the formation of a single-phase spinel ferrite structure with crystallite sizes of 20–30 nm. Energy-dispersive X-ray spectroscopy verified the successful incorporation of Ni ions into the CuFe₂O₄ lattice, while FE-SEM analysis revealed uniformly dispersed nanoscale particles desirable for composite reinforcement. …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1–11 Read article
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Geotechnical Influence Factors in Empirical Design of Highway Pavement: The A123 Ilorin – Lokoja Highway, Nigeria Case Studies
Abstract: Site investigation and application of geological and geotechnical influence factors on the highway were investigated. Method involved field sampling, geotechnical laboratory and x-ray diffraction analysis and use of SRTM extracted slope and drainage parameters; and their integration in a GIS based multi-criteria decision analysis to derive a subgrade suitability map as a design tool. The suitability criteria classified the highway into four (4) design sections. Section one for very low …
Published in Journal of Geotechnical Engineering · Vol. 11, Issue 3, 2024 · pp. 53–70 Read article
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Recent Development to Track Contraband using Muon
Abstract: The muon is one of nature’s fundamental particles discovered in 1937 by Carl Anderson. A muon is an elementary subatomic particle similar to electron, but with a mass approximately 207 times greater and, sometimes it is called as a “heavy electron”. Muons are generated naturally when cosmic rays collide with atoms in earth’s upper atmosphere and, then raining down all the times upon the surface of earth. Muons can be …
Published in International Journal of Universe · Vol. 2, Issue 1, 2026 · pp. 23–34 Read article
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Application of Sensor Effect on Chlorodiazepam of Polyaniline Doped Silver Nanocomposite
Abstract: In order to ease the creation of the polymeric nanocomposite known as PANI/Ag, pani-doped silver nanoparticles were oxidised chemically and then exposed to the oxidation process. Aniline with varying amounts of silver nanoparticles added to it can be used to make a nanocomposite known as PANI/Ag in an acid solution at room temperature by employing ammonium persulfate as the oxidising agent. This can be done by using aniline with different …
Published in Journal of Polymer & Composites Read article
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Preparation and Characterization of TiO2 Nanoparticles by Green Method
Abstract: In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 61–67 Read article
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Evaluation of Inhibition Effect of Nanohybrid Curcumin (Cur-ZnO) and Cur-free Against Some Types of Bacteria
Abstract: This study aimed to prepare an efficient nanohybrid food preservative by loading curcumin on zinc oxide. The prepared compound was characterized using microscopy and spectral methods. Fourier transform infrared spectrum of the nanohybrid curcumin showed a shift in the frequencies of some chemical groups towards high and low frequencies. X-ray diffraction (XRS) spectrum also revealed the emergence of new diffraction planes in the nanohybrid compound, Compared with the carrier spectrum …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 68–79 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
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The Impact of Distinct Dopant Elements (Cu and Al) on the Electrochemical Characteristics of MgO Thin Films Formed Using the Electrodeposition Technique
Abstract: By using an aqueous electrodeposition technique, copper (Cu) and aluminum (Al) doped magnesium oxide (MgO) thin films were created. We examined how the dopant elements affected the electrochemical characteristics of MgO thin films deposited on stainless steel (SS) substrates in the current study. We annealed the MgO-based films at 450◦C. The MgO films doped with Cu and Al have been determined by X-ray diffraction (XRD) results. Cyclic voltammetric analyses (CV), …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 1, Issue 2, 2023 · pp. 12–17 Read article
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SYNTHESIS AND CHARACTERIZATION OF Mn2+ DOPED LiPbX3(X = Cl, Br, I)
Abstract: In this paper the structural, electronic and optical properties of Mn doped Pb based cubic perovskites LiPbX3(X= Cl, Br and I) were studied by wet chemical method (sol gel method). For Mn doped LiPbX3(X= Cl, Br and I) NCs, MnCl2 and PbBr2 were added in molar feed ratio 1.35 mole% and nan crystal were examine with the help of TEM and their structure were confirmed by X-ray diffraction (XRD). Additionally, …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 48–54 Read article
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Enhanced Synthesis Methods and Comprehensive Material Response Analysis in Alloy-Infused Nanocomposites
Abstract: This study looks into the most advanced ways to make alloy-infused nanocomposites and how they react to different materials. It focuses on how these nanocomposites can be used to process and make plastics and composites. A lot of people are interested in alloy-infused nanocomposites because they have better mechanical, thermal, and electrical qualities than regular composites. The goal of this study is to improve the methods used for making nanocomposites …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 175–191 Read article
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Zn Doped CuO Nanoparticles for Increasing the Longevity of The Agricultural Products †
Abstract: Nanotechnology is an enabling technology at the service of mankind. Indeed, enhancing the long-term storage of agricultural products (post-harvest during transportation and storage) in general and apples and tomatoes, in particular, is a challenge. Zn-doped CuO is a proven nanomaterial with special ability to kill plant pathogens as well as a variety of microorganisms (bacteria, virus, and fungus). Much of the review is focused on the landmark papers published by …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 1, 2024 · pp. 14–29 Read article