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174 articles for “Spectroscopy techniques”
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Biosynthesis of Magnetic Iron Oxide Nanoparticles Using Hibiscus as a Plant Source
Abstract: Green chemistry has significant role in improving and protecting the global environment and they are even competent over other conventional methods. This paper investigates the greener route to nanoparticles which were produced by coprecipitation technique using hibiscus leaf extract as a plant resource. This method has been proven cost effective, simple, economical, eco-friendly and non-hazardous. The formation and nature of synthesized magnetic iron oxide nanoparticles were characterized by UV–Vis spectroscopy, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 17, Issue 2, 2015 · pp. 1–9 Read article
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Evaluation of Bio-Based Polymer Composites Containing Guava Leaf Extract for Antimicrobial Functionality
Abstract: This study explores the formulation of an herbal soap using guava leaf extract as a primary ingredient. Guava leaves are a rich source of biopolymers like pectin and cellulose, which may contribute to the binding properties in the soap. The antimicrobial activity of the soap was evaluated against common skin pathogens (Staphylococcus aureus, Trichoderma spp., Aspergillus spp.). The formulated soap exhibited inhibitory effects against all tested pathogens. The weight, foaming …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 875–880 Read article
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Synthesis, characterization, and antibacterial activity of silver nanoparticles with expired minocycline as reducing agent: proposed as a recycling technique.
Abstract: In this research, expired minocycline, a broad-spectrum tetracycline antibiotic, was employed as both a reducing and stabilizing agent for the eco-friendly synthesis of silver nanoparticles. This sustainable method avoids the use of toxic chemical reducing agents, providing a greener alternative for nanoparticle production. The synthesized silver nanoparticles were analyzed using several characterization techniques, such as UV-Vis’s spectroscopy, scanning electron microscopy, transmission electron microscopy, and Edex analysis, to assess their structural, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 1, 2026 · pp. 30–43 Read article
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Identification of Some Imported Lubricating Oil Additives Used in Libya and Synthesis of the Most Consumed Ones from the Local Raw Materials
Abstract: This paper presents the identified six additives imported under trade names used in the lubricating oil blending factory of A-Zawia-Libya. Their structures have been completely confirmed by examining their physical properties and using modern analytical techniques such as nuclear magnetic resonance spectroscopy (NMR), infra-red (IR), atomic absorption (AAS) and gas chromatography (GC). The synthesis of most important and more consumed additives in lubricating oils in Libyan oil industry from local …
Published in Journal of Catalyst & Catalysis · Vol. 3, Issue 3, 2016 · pp. 10–17 Read article
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AI-Assisted Kinetic Modeling of PLA Hydrolysis Under Subcritical Water Conditions for Sustainable Polymer Recycling
Abstract: The accumulation of poly (lactic acid) (PLA) in terrestrial and marine ecosystems has intensified the demand for closed-loop, green recycling technologies. Subcritical water (SCW) hydrolysis offers a promising, catalyst-free pathway for the rapid depolymerization of PLA into its constituent monomer, lactic acid. However, the complex, highly non-linear kinetics governing macro-molecular degradation under variable hydrothermal conditions limit real-time process optimization and industrial scalability. This study develops a novel artificial intelligence (AI)-assisted …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 2, 2026 · pp. 65–74 Read article
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Recent Advances in Crystal Defect Engineering of Semiconductor Photocatalysts for Sustainable Environmental and Energy Applications
Abstract: Semiconductor photocatalysis has emerged as one of the most promising green technologies for addressing environmental pollution and global energy challenges through solar energy utilization. Nevertheless, the practical application of conventional semiconductor photocatalysts is often limited by their narrow visible-light absorption, rapid recombination of photogenerated electron–hole pairs, insufficient active sites, and poor charge-transfer efficiency. Defect engineering has recently attracted significant attention as an effective strategy to overcome these limitations by deliberately …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 4, Issue 2, 2026 Read article
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Synthesis and Synergistic Effects of Ciprofloxacin Conjugated Zinc Oxide Nanoparticles
Abstract: Zinc oxide nanoparticles (ZnO NPs) are known as a multifunctional material because of its unique physical and chemical properties. The result of zinc oxide nano powder was characterized using various analytical techniques, such as UV-Vis spectroscopy, Fourier Transform Infra-Red (FTIR), Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD) patterns. Synthesized zinc oxide nano powder was stored in dried form in the room temperature for further study. …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 1, 2019 · pp. 61–71 Read article
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Rapid Determination of Content of Etoricoxib in Pharmaceutical Formulations by Mid-Infrared Spectroscopy
Abstract: The present paper is an attempt to highlight a new technique FTIR-ATR along with its referenced validated method, UV spectrophotometric analysis. Different concentrations of etoricoxib were used as samples to draw standard plot. From different samples, a transmission spectrum was recorded according to the prominence of peaks. The present study has chosen the three most prominent peaks for analytical purpose in case of samples of etoricoxib and marketed formulations. All …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 4, Issue 3, 2013 · pp. 20–32 Read article
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Properties and antimicrobial activity of bacterial nanocellulose composite incorporated with silver nanoparticles based on green synthesis
Abstract: Green silver nanoparticles (AgNPs) synthesized using medical plant extracts as capping and reducing agents demonstrate broad applicability in addressing the threat posed by infections. In this study, we present a sustainable, low-toxicity, and cost-effective bacterial nanocellulose composite with silver nanoparticles based on green synthesis that uses Origanum vulgare as a reducing agent due to numerous biological components. The formation of AgNPs in composite and morphological properties was analyzed using scanning …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 323–328 Read article
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Dosimetric Aspects of Poly(ethylene- g - maleic anhydride)
Abstract: Electron spin resonance (ESR) spectroscopy is considered to be finger print technique to identify chemical structures of irradiated polymers. To prove this, ESR spectra of unirradiated and irradiated maleic anhydride grafted poly ethylene (MANPE)are recorded under different conditions. The ESR spectra show multiplehyperfine lines with latent structure corresponding to macro radicals . Radiation dose dependency on chemical structure of MANPE has been investigated by recording ESR spectra at various radiation …
Published in Journal of Polymer & Composites · Vol. 7, Issue 3, 2019 · pp. 20–23 Read article
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Growth, Optical, Mechanical and Electrical Properties of Zinc Sulphate Admixtured N-N’-dimethylurea Single Crystals (DMUZS)
Abstract: AbstractThe single crystals of zinc sulphate admixtured N-N’-dimethylurea (DMUZS) were grown by slow evaporation technique from aqueous solution at room temperature. Good quality crystals of size 16×12×5 mm3 had been obtained after 35 days. The grown crystals were characterized by single crystal XRD analysis to determine the lattice constant of the sample. Powder X-ray diffraction studies confirm the crystalline nature of the grown crystal. Fourier transform infrared (FT-IR) studies were …
Published in Research & Reviews : Journal of Physics · Vol. 7, Issue 1, 2018 · pp. 24–33 Read article
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Sustainable Innovations in Green Nanotechnology for Nanoparticle Synthesis
Abstract: Green nanotechnology is an emerging field that focuses on the environmentally friendly production of nanoparticles through biological and sustainable processes. This approach has diverse applications across industries such as pharmaceuticals, energy, electronics, and bioengineering. Compared to conventional methods, biologically driven nanoparticle synthesis, particularly utilizing green chemistry principles, offers a safer, eco- friendly, non-toxic, and cost-effective alternative. Metal nanoparticles are commonly synthesized through top-down and bottom-up strategies using physical, chemical, and …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 1, 2025 · pp. 31–37 Read article
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An Efficient Synthesis of Some Novel Benzo Coumarin Derivatives Under Solvent Conditions from 2-acetyl-benzo[f]chromen-3-one
Abstract: The synthesis of the target compounds began with the preparation of 2-[3-dimethylamino[acryloyl-3H-benzo[f]chromen-3-one. This intermediate was obtained through the reaction of 2-acetylbenzo[f]coumarin-3-one with N,N-dimethylformamide dimethyl acetal [DMFDMA[ under reflux conditions in xylene. The enaminone thus formed was subsequently reacted with 6-aminothiouracil in acetic acid, leading to the formation of 2-thioxo-2,3-dihydro-1H-pyrido[2,3-d]pyrimidin-4-one. This compound served as a pivotal intermediate for the synthesis of a series of pyridotriazolopyrimidinones. These derivatives were synthesized by reacting …
Published in International Journal of Cheminformatics · Vol. 2, Issue 2, 2024 · pp. 33–46 Read article
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A Comprehensive Review of Analytical Method – Development and Method Validation of Digoxin Tablets
Abstract: The main objective of this review is to give an outline of the method development and validation process of digoxin, and this review covers the different types of spectroscopic and chromatographic techniques, such as HPLC, UHPLC-Tandem mass spectroscopy, TLC, and LC-MS. A novel method for the determination of digoxin in biological samples has been developed and validated, focusing on improving sensitivity, specificity, and reproducibility. The method was validated in terms …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 12, Issue 1, 2025 · pp. 47–58 Read article
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Structure–Optical Property Correlation of Co-Doped TiO₂ and ZnO Nanofillers for Advanced Functional Composite Applications
Abstract: This study investigates the enhancement of the structural and optical properties of titanium dioxide (TiO₂) and zinc oxide (ZnO) nanoparticles through cobalt (Co) doping. Pristine TiO₂ and ZnO are widely studied metal oxides; however, their large band gaps and limited visible-light absorption restrict their performance in optoelectronic, photocatalytic, and environmental applications. Co doping is employed as an effective strategy to overcome these limitations by inducing band-gap narrowing, creating defect-related electronic …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1374–1394 Read article
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Theoretical Study of Surface Excitations at Planar Surface of Zinc Selenide (ZnSe)
Abstract: ZnSe is a II-VI semiconductor material and has very novel properties. So it is currently demanding for various applications. Dispersion relation is employed here to study the elementary surface excitations at the planar surface of Zinc Selenide (ZnSe) semiconductor. These excitations are of various types such as plasmons, phonons, excitons etc. Plasmons are the quanta of valence electron oscillations, phonons are the quanta of lattice vibrations and excitons are the …
Published in Research & Reviews : Journal of Physics · Vol. 11, Issue 3, 2022 · pp. 1–5 Read article
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Patterning of Carbon Nanotubes on Silicon Wafer Using Self-Assembly Techniques
Abstract: Nanotechnology is an emerging technology that enables scientists to develop new materials and products at the molecular level. A carbon nanotube (CNT) is a rolled sheet of carbon atoms, coaxially arranged in cylindrical shape. Single-walled CNTs are ideal quantum systems for exploring basic science in one dimension. To find use in electronics, single-walled CNTs need to be efficiently separated by electronic type and aligned to ensure optimal and reproducible electronic …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 2, 2015 · pp. 6–15 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts: Properties and Applications
Abstract: The main study and the development of CeO2 and Cu-doped CeO2 nanocrystals containing transition- metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu-doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. The structural properties of Ce1-xCuxO2 nanocrystals were examined by investigating the influence of cerium dioxide and Cu dopant ions. The CeO2 single-phase cubic system was successfully incorporated with Cu …
Published in Journal of Catalyst & Catalysis · Vol. 11, Issue 3, 2024 · pp. 29–38 Read article
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Raman Spectroscopy for The Determination of Relative Crystallinity of Carbon Fibers
Abstract: Analogous to X-ray diffraction technique, the light scattering technique discovered by Sir CV Raman has great potential in quantifying the crystallinity of new materials, like the highly crystalline pitch based carbon fibers (NX90 and NX100). For comparison the Raman spectra of polyacrylonitrile based carbon fibers (T700SC) were also recorded. From the Raman spectral analysis, it was found that the pitch based carbon fibers exhibit far far higher degree of crystallinity …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 1, 2024 · pp. 30–38 Read article
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Nanostructured Cr-WS2 Solid Lubricant Coating for Space Applications
Abstract: Abstract Tungsten disulphide (WS2) is one of the widely used intrinsic low friction materials, which is commonly used in the form of coating. WS2 offers very low coefficient of friction only in non humid conditions. Presence of humidity destroys this property and restricts its utility. Modifying the structure of WS2 by adding certain metals helps in overcoming this limitation and in addition improves the mechanical properties. Further, deposition technique and …
Published in Journal of Instrumentation Technology & Innovations · Vol. 9, Issue 1, 2019 · pp. 12–18 Read article