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42 articles for “SEM/EDX”
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Synthesis, characterizations, and challenges of magnetic Zn x Fe 2-x O 3 nanoparticles
Abstract: Diluted magnetic semiconductors comprising magnetic nanoparticles are a driving force in a variety of applications, including biomedicine, bioelectronics, photocatalytic activities, and nanosensors. However, the functionality of these nanomaterials can be influenced by several factors, such as synthesis route, characterization procedures, source, crystal size, and morphology. In this research, emphasis is devoted to synthesizing and characterizing magnetic nanoparticles. Most importantly, it is focused on biological methods, Co-precipitation methods, hydrothermal Gravity methods, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 28, Issue 2, 2025 · pp. 1–16 Read article
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Adsorptive Removal of Rhodamine-B Using Eco- Synthesized Green Tea–Aluminium Nanoparticles
Abstract: This study examines the use of Green Tea–Aluminium Nanoparticles (GT-Al NPs), a unique and eco-friendly adsorbent, to remove the dangerous Rhodamine-B dye from water. For characterisation, SEM, FTIR, TGA, and EDX were employed. We evaluated the effects of pH, temperature, dosage, contact time, and initial dye concentration on adsorption efficiency. First- and second-order pseudo models were used to characterize adsorption kinetics, and the Langmuir model explained equilibrium, as well as …
Published in Emerging Trends in Chemical Engineering · Vol. 12, Issue 3, 2025 · pp. 61–72 Read article
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A Sol-Gel Approach for the Fabrication of Zinc Oxide Nanoparticles and Their Nanocomposite with Urea Formaldehyde (UF)
Abstract: In the performed work, zinc oxide nanoparticles were synthesized via the sol-gel method using zinc sulphate as the precursor material. Urea-formaldehyde (UF) resin was employed as a polymer matrix to encapsulate the produced ZnO through an acid-catalyzed polymerization process. This encapsulation aimed to improve the dispersion stability and surface reactivity of ZnO within the polymeric medium. The synthesized materials were subjected to comprehensive characterization using Fourier Transform Infrared Spectroscopy (FT-IR), …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 21–27 Read article
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Biosynthesis, Characterization and Antibacterial Studies of Silver Nanoparticles from Tamil Nadu Major Crop Anacardium occidentale
Abstract: Recent studies have shown that Silver Nanoparticles have physical, optical and catalytic properties. Present work involves the eco-friendly and reproducible synthesis of Silver Nanoparticles from the Anacardium occidentale leaves extract. The synthesized silver Nanoparticle from 1 mM AgNO3 solution through the leaf extract were characterizing was monitored using Ultraviolet-visible (UV-vis) spectrophotometer, Scanning electron microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray powder diffraction (XRD) and Fourier transform infra-red spectroscopy (FT-IR).Scanning …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 20, Issue 3, 2018 · pp. 13–22 Read article
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Synthesis and Characterization of Strontium Aluminate Nanophosphors
Abstract: Monoclinic SrAl4O7 nanophosphors with different weight percentage of aluminium were synthesized by low temperature sol-gel method. The morphology, composition and structure of the synthesized phosphors were characterized by scanning electron microscope (SEM), energy dispersive X-ray (EDX), photoluminescence emission spectra (PL) and X-ray diffraction (XRD) respectively. It was found that PL emission was obtained at 395, 520, and 790 nm corresponding to blue, green and IR region of the spectrum, respectively. …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 18, Issue 2, 2016 · pp. 7–10 Read article
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Green synthesis of zinc oxide and copper oxide nanoparticles and their effect against wilt fungus, Fusarium udum.
Abstract: Nowadays nanoparticles (NPs) come out as powerful tools to enhance crop production and protection. Biosynthesis of NPs has a vital role and an alternate to chemical and physical methods because it is simple, easy, eco-friendly, and free from chemical hazards. Zinc oxide (ZnO) and copper oxide (CuO) NPs were synthesized from leaves extract of Lantana camara (L.) and Nerium oleander (L.) and characterized by using several techniques such as transmission …
Published in Research and Reviews : A Journal of Life Sciences · Vol. 13, Issue 3, 2023 · pp. 1–5 Read article
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California Bearing Ratio and Young’s Modulus Behavior of Clinker Stabilized Fly Ash-Mine Overburden Mixes
Abstract: Fly ash is a major byproduct of coal combustion. Fly ash often causes disposal problems and environmental pollution. This paper presents detailed laboratory investigation carried out on clinker stabilized fly ash-mine overburden mixes to find out its suitability for sub-base of mine haul road pavements. Proctor compaction test, Unconfined Compressive Strength (UCS) test, California Bearing Ratio (CBR) Test, Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDX) were conducted …
Published in Recent Trends in Civil Engineering & Technology · Vol. 3, Issue 3, 2013 · pp. 1–10 Read article
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A Study on Chemical Composition in Temperature Sensor
Abstract: As the demand for precision thermal monitoring in extreme environments – such as aerospace propulsion systems and micro-electromechanical systems (MEMS) – continues to escalate, the chemical stability of temperature sensing elements has become a critical focal point. This study investigates the correlation between the chemical composition of thin-film resistance temperature detectors (RTDs) and their operational longevity under thermal cycling. By employing X-ray Photoelectron Spectroscopy (XPS) and Energy-Dispersive X-ray Spectroscopy (EDS), …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 2, 2026 · pp. 1–7 Read article
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Analysis of C45 Steel Machining with Differentiated Tool Bits
Abstract: The tool material may be coated or uncoated, and cutting inserts are typically situated along the covered contact region. Work piece remains fixed while tool revolves for cutting and machining. Objective: A NABL-accredited metallurgical evaluation laboratory (machining) assessed two specimens. Machining profile and materials determine insert selection. Analytical results show material composition. The surface qualities of samples 1 and 2 were examined. As DOC, cutting speed and tool tip temperature …
Published in Journal of Polymer & Composites · Vol. 12, Issue 5, 2024 · pp. 244–252 Read article
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Characterization Techniques for Thin Film Coatings Based on SiO₂, TiO₂, and ZrO₂
Abstract: Thin film coatings made from silicon dioxide (SiO₂), titanium dioxide (TiO₂) and zirconium dioxide (ZrO₂) have attracted great interest owing to their excellent optical, electrical, mechanical and chemical properties. These oxide thin films are widely used in microelectronics, solar cells, sensors, biomedical devices, photocatalysis, anti-reflective coatings and protective layers. The structural, morphological, compositional, optical and mechanical properties of these coatings are closely related to their performance and reliability. Therefore, thorough …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 Read article
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Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
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Comparative Adsorption Studies on Raw Rice Husk, Acid Leached Rice Husk and Base Leached Rice Husk by Using Methylene Blue as Dye
Abstract: Current methods for removing dyes from wastewaters are costly and cannot effectively be used to treat wide range of such wastewaters. This work describes the use of raw rice husk (RRH), acid-leached rice husk (ALRH) and base-leached rice husk (BLRH) as adsorbents for decolorization. Characterization of raw rice was done by powder X-ray diffraction (P-XRD) analysis, surface area analysis and scanning electron microscopy. Raw rice husk was collected directly from …
Published in Journal of Catalyst & Catalysis · Vol. 2, Issue 1, 2015 · pp. 32–39 Read article
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The Formation of Bi-2223 Superconductor with Fe-Substitution
Abstract: Presently, we have studied about synthesis and characterization of Bi-2223 Superconductors in the form of Bi2Sr2Ca3(Cu0.97Fe0.03)3O10+δ complex. The sample was established with solid state method and characterized by XRD, (FESEM) and (FTIR). The DC electrical resistivity of the sample was measured at liquid helium temperature. The XRD parameters shows the orthorhombic structure with lattice constant a = 5.7429Å, b = 5.0845 Å, c = 36.5569 Å and grain size confirm …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 2, 2020 · pp. 32–41 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Fabrication and Characterization of Copper Nanowires: An Overview
Abstract: Copper (Cu) is one of the most important metals in modern electronic technology. Keeping in view its role in nanoelectronics, we have fabricated copper nanowires of diameters 100 and 200 nm using Anodic Alumina and polymer membranes as templates. Template-based growth of copper nanowires has been realized using conventional electro deposition technique in an electrochemical cell designed in our laboratory. Fabrication of copper nanowires is one of the most important …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 1, 2011 · pp. 1–16 Read article
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Au@Sio2@PVP-DCMD Membranes: A Breakthrough in Heavy Metal Removal and Antibacterial Defense
Abstract: This study investigates the development and characterization of multifunctional gold-doped silica (Au@SiO₂) membranes for water distillation and antibacterial applications. The manufacturing process integrated gold nanoparticles into silica matrices using sol-gel techniques. Structural analysis was conducted using SEM (showing uniform pore distribution with an average pore size of 40-50 nm), FTIR (confirming Si-O-Si and Si-Au-Si bonding peaks at 525 cm⁻¹ and 1310 cm⁻¹ respectively), EDX (revealing gold nanoparticle content of 1.5 …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 13–27 Read article
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Ag₂S–Ag Nanocomposites: A Bottom-Up Approach to Enhance Thermoelectric Power Factor at Near Room Temperature
Abstract: The intrinsic ductility, low toxicity, and naturally occurring abundance of silver sulphide (Ag₂S) have made it a potential thermoelectric material in recent years. However, high electrical resistance severely limits its practical application. Here, we present a thorough analysis of how metallic Ag nanoinclusions affect the structural, electrical, and thermoelectric characteristics of Ag₂S nanocomposites made using a simple bottom-up polyol approach. (Ag₂S)₁₋ₓAgₓ nanocomposites with an Ag content ranging from 0 to …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 4, Issue 1, 2026 · pp. 40–55 Read article
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Synthesis of Nanocrystalline Bismuth Ferrite by Solution Combustion Synthesis Method
Abstract: Normal 0 false false false EN-US X-NONE X-NONE The present paper describes a simple method of nanosized BiFeO3 by the solution combustion synthesis using bismuth and iron nitrates as oxidizers and the combination fuel of citric acid and ammonium nitrate, with fuel to oxidizer ratio (Ψ = 1) one. The average crystallite size of BiFeO3 nanoparticles was estimated from the full width half maximum of the X-ray diffraction peaks of …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 2, 2011 · pp. 52–58 Read article
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Properties of ZnO Thin Film deposited on Flexible Substrate using RF Sputtering
Abstract: Semiconductor materials demand is increased in recent years, due to new emerging technologies. There is need to find the alternate for silicon in electronics industry, as silicon is brittle in nature and has low efficiency, which makes it unsuitable for transparent and flexible device. Zinc oxide (ZnO) is emerging as popular choice of researchers due to its wide range of properties, abundancy and non-toxicity. This work explores the properties of …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 50–56 Read article