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240 articles for “and XRD”
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Correlation Between XRD Analysis and Mechanical Characterization Using Lens Manufactured Specimens Based on IoT Sensors
Abstract: The advent of the Internet of Things (IoT) has enabled the seamless integration of sensors into the manufacturing process, facilitating the collection of real-time data for analysis and optimization. The correlation between X-ray diffraction (XRD) analysis and mechanical characterization is investigated using specimens manufactured through the Laser Engineered Net Shaping (LENS) technique. The study focuses on three different materials: brass, SS202, and SS304. XRD analysis is employed to determine the …
Published in Journal of Polymer & Composites · Vol. 12, Issue 2, 2024 · pp. 41–58 Read article
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Evaluation of Crystallinity in Talc/Poly-styrene Composites by using FTIR and XRD
Abstract: Over the decade, polymers have found their usage in almost all types of industries ranging from food and beverage packaging to automobile industries. Though the polymers are considered highly inert and chemically stable, their performance under mechanical loading is not at par with their metallic counterparts. Thus, polymer composites have started gaining popularity over the years, but their properties are poorly understood. In this study, the effect of talc addition …
Published in Trends in Mechanical Engineering & Technology · Vol. 11, Issue 2, 2021 · pp. 10–16 Read article
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Growth, XRD, FTIR and Second Order NLO studies of Undoped and Zinc Sulphate doped L-Histidine Single Crystals
Abstract: AbstractSingle crystals of pure (undoped) L-histidine and Zinc sulphate doped L-histidine have been synthesized and grown by slow evaporation method using water as the solvent. These grown crystals are characterized by FTIR, XRD and SHG. From Fourier transform infrared (FTIR) spectral analysis, the various functional groups present in the sample have been confirmed. The X-ray diffraction (XRD) study ensures that the grown crystal crystallizes in the orthorhombic system and the …
Published in Trends in Opto-electro & Optical Communication · Vol. 8, Issue 3, 2018 · pp. 31–36 Read article
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Crystallinity of commercial carbon fibers from X-ray diffraction (XRD) studies
Abstract: Sized carbon fibers have commercial significance. Such carbon fibers serves has excellent reinforcing material with the polymer resin filler matrix leading to the formation of carbon fiber reinforced composites (CFRCs). Polarized carbon fibers find applications in the realms of health, energy, environment, defence, catalysis and smart materials. For brevities sake, the focus of the current research paper is only on the structural characterization of carbon fibers using XRD. The structure …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 1, Issue 1, 2023 · pp. 17–27 Read article
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Denoising of XRD Signals
Abstract: In this paper, different types of signal are discussed. Also various methods of signal transformation are studied. A detailed study of different wavelet families is done. By using different signal transformation methods, XRD signals are denoised here. Original and denoised signal for different wavelet families are plotted on the basis of their best threshold values. Keywords: Signals, denoising, wavelets, fourier transform, threshold value Cite this ArticleJyoti Yadav. Denoising of XRD …
Published in Journal of Semiconductor Devices and Circuits · Vol. 4, Issue 3, 2017 · pp. 1–10 Read article
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Bismuth's Doping Effect on Organic Non linear Optical Materials
Abstract: Using the method of slow evaporation solution growth, single crystals of pure and bismuth-doped urea were produced. Many interesting results on several properties of Bismuth fluoride impurity added to Urea single crystals have been observed and studied. The different morphology of bismuth doped urea crystals was noticed. By using FTIR analysis, the functional group's existence has been approximated. The generated crystals' lattice properties were examined using the single crystal X-ray …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 3, 2023 · pp. 17–24 Read article
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Doping of Cerium, Boron and Sulphur with ZnO Nanoparticles and their Impact on Lattice Parameters, Studied through UDM Model
Abstract: Un-doped and tri-doped ZnO nanoparticles were successfully synthesized by the simple sol-gel method. Tri-doped nanoparticles of ZnO were prepared by using Ce, B and S as a dopant in concentrations of 1, 2 and 4 wt% with respect to ZnO. The effect of Ce, B and S on the ZnO nanoparticles was investigated by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and Fourier transform infrared (FTIR) techniques against particles …
Published in Emerging Trends in Chemical Engineering · Vol. 4, Issue 1, 2017 · pp. 21–28 Read article
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Structural, Mechanical, Electrical and Magnetic Properties of Mn–Zn Substituted Ca-hexaferrites
Abstract: In the present investigation, the samples with chemical composition Ca(CoTi)0.5(MnZn)x/2Fe11–xO19 with (x = 0 to 1.0) have been synthesized using perfect stoichiometric proportions of reacting oxides by standard ceramic technique. The pellets of 15 mm diameter were prepared and sintered at 1313 K in air atmosphere for 106 h and characterized by using XRD and SEM. XRD studies of the samples showed hexagonal magnetoplumbite (M) structure with unit cell dimensions …
Published in Journal of Materials & Metallurgical Engineering · Vol. 1, Issue 1-3, 2011 · pp. 99–111 Read article
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Role of GO and rGO on the Structural Properties of PA6/PMMA Blend Nanocomposites
Abstract: To understand and assess the role of Graphene Oxide (GO) and reduced graphene oxide (rGO) in the PA6/PMMA blend, nanocomposites, the PA6/PMMA (50:50 wt%) blend-based nanocomposites were prepare by loading different wt% of GO and rGO (1wt% and 3wt%), through twin screw melt extrusion followed by injection moulding technique. Different compositions of the nanocomposites were prepared using melt mixed method at 2300C by applying a rotational torque 50 N. All …
Published in Journal of Polymer & Composites · Vol. 10, Issue 1, 2022 · pp. 1–10 Read article
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Synthesis and Characterization of Polymer Blend Electrolyte Based on Bio-degradable Polymers Doped with Ammonium Iodide
Abstract: A polymer blend of Polyvinylalchohol (PVA) and Polyvinylpyrrilodine (PVP) doped with ammonium iodide (NH4I) has been prepared by solution casting method to develop a new solid polymer electrolyte. The influence of NH4I on the structural, electrical characteristics of PVA/PVP blend was investigated utilizing XRD, FTIR and impedance spectroscopy techniques. Structural properties were studied by using the XRD technique and found that the pure polymer blend is in semi crystalline form, …
Published in Journal of Polymer & Composites · Vol. 10, Issue 2, 2022 · pp. 60–71 Read article
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Structural Studies on Glass Fiber Reinforced Poly-styrene Composites
Abstract: Polymers are used in various industries and majorly in aerospace and automobile industry where in fuel efficiency is a big challenge. Polymers are lightweight hence by volume they make up 50% of a new vehicle but by weight it is less than 10%. Current economic and environmental concerns make the creation of more fuel-efficient cars a top priority in the automotive industry. Hence the study of these polymers becomes very …
Published in Trends in Mechanical Engineering & Technology · Vol. 11, Issue 3, 2021 · pp. 32–38 Read article
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Oxidation Behaviour of Plasma Sprayed Carbon Nanotubes-Alumina Coated ASME-SA213-T291 Boiler Tube Steel
Abstract: In this research work, oxidation behaviour of Carbon Nanotubes reinforced Al2O3 coated ASME-SA213-T91 boiler tube steel specimens were investigated at 900°C temperature in air. The different CNTs-Alumina composite coatings were deposited using plasma spray technique and NiCr was used as bond coat before applying CNTs-Al2O3 coatings. The hot corrosion studies were conducted on all coated specimens in air at 900°C under cyclic conditions. The thermogravimetric technique was used to establish …
Published in Journal of Materials & Metallurgical Engineering · Vol. 7, Issue 3, 2017 · pp. 1–15 Read article
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Study on GP Zones Formation in the Sc Inoculated Ternary Al-Zn-Mg Alloys
Abstract: Mostly, ternary Al-Zn-Mg (7075) alloys are used in automotive and aerospace engineering due to readily age-hardening response and high specific strength-to-density ratio. Scandium (Sc) has great inoculation effect in Al-Zn-Mg alloys. The cast Al-Zn-Mg alloys system undergoes a complex transition sequence in order to gain maximum strength. This sequence consists of solutionizing then immediate quenching in water (T4), natural ageing and artificial ageing (T6); usually, in several temperature steps to …
Published in Journal of Materials & Metallurgical Engineering · Vol. 6, Issue 2, 2016 · pp. 53–69 Read article
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Synthesis and Characterization of Bamboo-Supported Nano Zerovalent Iron (NZVI-AB) for Cr(VI) Sequestration
Abstract: Remediation of chromium contaminated sites present both technological and economic challenges, as conventional methods are often too expensive and difficult to operate. In this study, bamboo supported Zero-valent iron (Fe0) nanoparticles were synthesized, characterized, and were tested for removal of Cr(VI). Fe0 nanoparticles were synthesized by the reduction of ferric chloride with avocado polyphenols and characterized by FTIR (Fourier transform infrared) spectroscopy and XRD (X-ray diffraction). Batch experiments were performed …
Published in Journal of Materials & Metallurgical Engineering · Vol. 10, Issue 3, 2020 · pp. 1–7 Read article
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Preparation and Charactrization of lead free piezoelectric ceramic/PVA polymer composites
Abstract: Sodium potassium niobate (Na0.5K0.5 NbO3 ) ceramic was prepared through conventional solid state reaction using AR grade NaNO3, KNO3 and Nb2O5 in stochiometric ratio. Poly vinyl alcohol (PVA) polymer - sodium potassium niobate composite films were prepared by solution casting method by changing the blend ratio of PVA / Na0.5K0.5NbO3. The prepared samples in the form of films were characterized by powder X-ray diffraction. The XRD studies revealed the presence …
Published in Journal of Polymer & Composites · Vol. 6, Issue 1, 2018 · pp. 1–8 Read article
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Role of Bimetallic (Ag-Cu) Nanoparticles on the Structural Properties of PVA/PVP Blend Green Nanocomposites
Abstract: This study reports the green synthesis of polymer blend nanocomposites of Polyvinyl alcohol (PVA) and Poly vinylpyrrolidone (PVP) embedded with Silver (Ag), Copper (Cu) mono metallic and Silver-Copper (Ag-Cu) bimetallic nanoparticles (NPs), generated using plant mediated solution casting method. The formation of blend, polymer-polymer interactions, interaction between polymer and nanoparticles and role of the nanoparticles on the interactions among PVA/PVP blend nanocomposites were studies by FTIR spectroscopy. The crystallinity of …
Published in Journal of Polymer & Composites · Vol. 10, Issue 1, 2022 · pp. 11–19 Read article
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Effect of ZrO2 nanoparticles on Electrical conductivity of PVA/PVP polymer blend doped with ammonium iodide
Abstract: This work reports the properties of solid polymer electrolyte films obtained via incorporating varying amounts of ZrO2 nanoparticles into the PVA/PVP polymer blend with ammonium iodide salt. Material synthesis was done by the solution casting technique. Frequency dependent impedance and conductivity parameters of polymer electrolyte films were investigated at different temperatures (303K-353K) using impedance spectroscopy. The results of ionic conductivity of prepared polymer blend samples at various temperatures were studied …
Published in Journal of Polymer & Composites · Vol. 10, Issue 3, 2022 · pp. 85–94 Read article
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Synthesis and Characterization of Al-Mg-Si Alloy based Hybrid Composite Reinforced with SiC and Graphite
Abstract: The present work is carried out to investigate the mechanical properties of Al-Mg-Si alloy matrix based hybrid metal matrix composites (MMCs) using stir casting method owing to its popularity and large scale productions. SiC and graphite reinforcements were added each with 1%, 2%, 3% and 4% respectively to fabricate four composites specimens. X-ray diffractometer and scanning electron microscope were used for phase identification and microstructure characterization (SEM). Density, hardness, compressive …
Published in Journal of Polymer & Composites · Vol. 10, Issue 3, 2022 · pp. 9–19 Read article
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THE THICKNESS EFFECT ON TiO 2 THIN FILMS FABRICATED BY USING SOL- GEL DIP COATING METHOD
Abstract: Titanium dioxide films were prepared by sol-gel dip-coating technique onto glass substrates at room temperature. The study focuses on the structural pattern of TiO 2 films which were dominated by the parameters such as the film thickness, pH, annealing temperature and number of dipping layers. At first the dipping speed is optimized with the refractive index of the film along with the number of dipping layers. Then the film deposited …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 1–10 Read article
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Performance of Ni3Al and TiO2 Coatings on T91 Boiler Tube Steel in Simulated Boiler Environment at 900°C
Abstract: Boiler steel tube corrosion in coal fired boiler is main subject during design and operation of thermal power plant and it leads to both direct and indirect loss of cost and energy, including losses due to plant shut down time and inefficiency of operation. One of the feasible solutions to solve out this problem is providing surface coating on boiler steel tube, which on one hand protects the tube from …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 3, Issue 2, 2016 · pp. 27–34 Read article