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11 articles for “Solid-State Reaction”
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Solid-State Reactions: Mechanistic Insights, Kinetic Behavior and Emerging Applications in Advanced Materials
Abstract: Solid-state reactions are fundamental to the synthesis and transformation of inorganic materials, playing a crucial role in the development of ceramics, semiconductors, catalysts, and energy storage systems. Unlike reactions in liquid or gaseous phases, they are limited by restricted atomic mobility and typically require elevated temperatures to enhance diffusion and overcome activation energy barriers. These reactions proceed through interfacial contact between solid reactants, followed by nucleation of product phases and …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 1, 2026 · pp. 10–14 Read article
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Synthesis and Characterization of VO 2+ doped SrMg 2 (PO 4 ) 2 Nanopowder by Solid State Reaction technique suitable for White LED material
Abstract: VO2+ doped SrMg2(PO4)2 nanopowder was synthesized by using solid state reaction (SSR) technique. Various experimental techniques have been performed on prepared sample. XRD analysis has revealed that prepared nanopowder is in monoclinic phase. The average crystallite size, micro strain and dislocation density evaluated and make an analogy with W-H plot method. SEM micrographs shows that agglomerated stone like structure and EDS spectrum shows elemental compositions of synthesized sample. FTIR spectrum …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 95–110 Read article
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Unraveling Mixed Ionic-Electronic Conduction in Lithium-Substituted Rubidium Tetra Titanates via Dielectric Spectroscopy and EPR Analysis
Abstract: Lithium-substituted Rubidium Tetra Titanates with varying concentrations of lithium carbonate (Li₂CO₃) — specifically 0.01, 0.05, and 0.1 molar percentages — were successfully synthesized using a conventional high-temperature solid-state reaction method. The resulting compounds follow the general chemical formula Rb₂₋ₓLiₓTi₄O₉. X-ray diffraction (XRD) analysis confirmed that lithium ions were successfully incorporated into the crystal lattice without disrupting the fundamental layered structure of the host material. The crystal system remained monoclinic across …
Published in Research & Reviews : Journal of Physics · Vol. 14, Issue 2, 2025 · pp. 19–29 Read article
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Electrical Measurements on La-modified Four-Layered Aurivillius Ceramics
Abstract: Bismuth layered structure ferroelectric (BLSF) of Aurivillius family is found to be attractive owing to its scientific and technological point of view. These materials have potential ferroelectric applications owing to the fact of its high Curie temperature, high temperature piezo-devise and ferroelectric random access memory (FRAM), applications. In addition, Bi-modified compounds have shown improved ferroelectric properties. However, the plausible reason for improving ferroelectric properties in Bi-modified is still unclear. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 157–170 Read article
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Role of Strontium in Structural and Dielectric characterstics of Barium Titanate
Abstract: Ba₀.₇₅Sr₀.₂₅TiO₃ (BST) compound was synthesized through the conventional solid-state reaction methodology, aimed at investigating its structural, microstructural, and dielectric characteristics. The structural characterization was executed employing X-ray diffraction (XRD), and the resultant diffraction patterns were refined utilizing the Rietveld method, which substantiated the establishment of a single-phase perovskite configuration exhibiting tetragonal symmetry and belonging to the P4mm space group. The refined lattice parameters revealed subtle distortions correlating with the substitution …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1157–1163 Read article
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Microwave-Assisted Synthesis of Li₃Ba₂Gd₃(MoO₄)₈ Phosphors Doped with Pr³⁺ and Sm³⁺ for High-Performance Red Emission in LED Applications
Abstract: In this study, we report the successful synthesis of Li₃Ba₂Gd₃(MoO₄)₈ (RE³⁺ = Pr³⁺, Sm³⁺) phosphors using a novel, microwave-assisted solid-state reaction method at ambient temperature. The synthesis involved the use of analytical grade reagents including Lithium Nitrate (LiNO₃), Barium Nitrate, Gadolinium Nitrate (Gd(NO₃)₃·6H₂O), Ammonium Molybdate ((NH₄)₆Mo₇O₂₄·24H₂O), and high-purity oxides of Praseodymium (Pr₂O₃) and Samarium (Sm₂O₃). The reagents were mixed in stoichiometric ratios, ground thoroughly in a pestle and mortar, and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 18–32 Read article
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Synthesis, characterizations, and challenges of magnetic Zn x Fe 2-x O 3 nanoparticles
Abstract: Diluted magnetic semiconductors comprising magnetic nanoparticles are a driving force in a variety of applications, including biomedicine, bioelectronics, photocatalytic activities, and nanosensors. However, the functionality of these nanomaterials can be influenced by several factors, such as synthesis route, characterization procedures, source, crystal size, and morphology. In this research, emphasis is devoted to synthesizing and characterizing magnetic nanoparticles. Most importantly, it is focused on biological methods, Co-precipitation methods, hydrothermal Gravity methods, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 28, Issue 2, 2025 Read article
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Domino Reaction for the Synthesis of Nitroolefin Heterocyclic Compound Via Thiazole Formation Followed by Claisen Rearrangement
Abstract: The Baylis-Hillman adducts derived from nitroolefins have been conveniently transformed into Claisen rearrangement. These substances, which include benzothiazole moiety, are very biologically reactive substances. This novel nitro derivative of 2-((E)-2-nitro-3-phenylallyloxy)-3-ethoxybenzaldehyde was simply treated with mole percentage of 2-(2-(2-aminophenyl) disulfanyl) benzenamine in melt reactive condition. Hence this novel 2-(benzo[d]thiazol-2-yl)-6-ethoxy-4-((E)-2-nitro-3-phenylallyl)phenol core unit compounds was very intrusting and new opportunities for the preparation of closely related to the different [3,3] sigmatropic rearrangements related …
Published in Journal of Modern Chemistry & Chemical Technology Read article
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Polymer Composite-Assisted Crystal Engineering for Drug Synthesis and Property Control through Solid Solutions and Co-Crystals
Abstract: The long-standing problem of low aqueous solubility, which affects about 90% of all new drug molecules under development, requires an immediate need for alternative approaches apart from the usual practice of crystallization. Polymer-composite-assisted crystal engineering is a novel technique for overcoming the aforementioned problem. This involves the addition of accepted pharmaceutical polymers, such as HPMC, PVP, PEG, and Eudragit copolymers in a single process, which can promote nucleation, stabilize the …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 172–189 Read article
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Photochemical Materials for Light-responsive Optical Switching: AI-optimized Design of Dynamic Visual Effects
Abstract: This paper presents an in-depth investigation into the design and behavior of photochemical materials that generate optical illusions and dynamic visual effects through light-induced molecular transformations. The study focuses on advanced photoresponsive compounds such as azobenzene and spiropyran derivatives, emphasizing their reversible optical transitions governed by photoisomerization, phase transitions, and photochromism in solid-state and polymeric matrices. Spectroscopic and kinetic analyses are employed to evaluate the influence of light wavelength, material …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 2, 2025 · pp. 13–27 Read article
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Synthesis of A Supercapacitor Based on Nanomaterials
Abstract: Demand for various energy storage technologies in electronic and electrical devices continuously goes on increasing. In that context, objective of this research work is to develop and test an electrode of a energy storage module (supercapacitor) using nickel hydroxide and carbon-based nanocomposite materials. Electrochemical performance of electrode is enhanced by optimizing synthesis parameters and designing the electrochemical cell. Conventional and all solid-state supercapacitors are developed with notable electrochemical performance. Pure …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 4, Issue 1, 2026 · pp. 24–39 Read article