Search
16 articles for “Single crystal XRD”
-
Bismuth's Doping Effect on Organic Non linear Optical Materials
Abstract: Using the method of slow evaporation solution growth, single crystals of pure and bismuth-doped urea were produced. Many interesting results on several properties of Bismuth fluoride impurity added to Urea single crystals have been observed and studied. The different morphology of bismuth doped urea crystals was noticed. By using FTIR analysis, the functional group's existence has been approximated. The generated crystals' lattice properties were examined using the single crystal X-ray …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 3, 2023 · pp. 17–24 Read article
-
Synthesis and Applications of Copper- Doped Pyridine Precipitate
Abstract: A metal organic nonlinear optical single crystal, copper doped pyridine material, was created at room temperature using the slow evaporation solution growth technique (SEST). The developed material's crystalline nature was revealed by a powder X-ray diffraction (XRD) analysis. Single crystal XRD study shows that the material synthesized possesses monoclinic system of cell parameters, a = 11.44 Å, b = 7.92 Å, C = 11.74 Å and alpha and gamma is …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 1, 2025 · pp. 51–60 Read article
-
Growth, Structural and Optical characteristics of Citric Acid Doped Copper Sulphate Single Crystals Polymer Composites Photonic Applications
Abstract: The organic material Citric Acid doped Copper Sulphate single crystals (CACS) was synthesized and single crystal was grown by slow evaporation method. The incorporation of citric acid, an organic compound, introduces polymer-like functional behavior into the crystal matrix, forming an organic-inorganic hybrid composite with enhanced optical and structural characteristics. Single crystal XRD confirmed the triclinic system with unit cell parameters: a = 5.96 Å, b = 6.11 Å, c = …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 482–488 Read article
-
Growth, XRD, FTIR and Second Order NLO studies of Undoped and Zinc Sulphate doped L-Histidine Single Crystals
Abstract: AbstractSingle crystals of pure (undoped) L-histidine and Zinc sulphate doped L-histidine have been synthesized and grown by slow evaporation method using water as the solvent. These grown crystals are characterized by FTIR, XRD and SHG. From Fourier transform infrared (FTIR) spectral analysis, the various functional groups present in the sample have been confirmed. The X-ray diffraction (XRD) study ensures that the grown crystal crystallizes in the orthorhombic system and the …
Published in Trends in Opto-electro & Optical Communication · Vol. 8, Issue 3, 2018 · pp. 31–36 Read article
-
Optimization of gas sensitivity of CuO/carbon composites with carbon particles synthesized from acacia auriculiformis branches
Abstract: Carbon particles fabricated from the core of acacia tree branches were utilized to synthesize CuO/carbon composite films. The gas sensing properties of these films grown on glass substrates using the doctor blade method were measured in 1000 ppm of methanol vapor at the room temperature. All the films were annealed at 75 0C for 1 hour in air. The structure, the optical band gap and the surface morphology of the …
Published in International Journal of Membranes · Vol. 1, Issue 1, 2024 · pp. 22–30 Read article
-
Effect of Bismuth doping on Thiourea crystals : A NLO Material
Abstract: Single crystals of pure and thiourea-substituted bismuth were successfully grown using the slow evaporation solution growth technique at ambient temperature. The impact of thiourea doping on the crystal properties was thoroughly investigated. Solubility tests for the grown samples were conducted at various temperatures, providing crucial data on the dissolution characteristics. Structural characterization of these crystals was performed using single crystal X-ray diffraction (XRD), confirming their crystalline nature. Energy-dispersive X-ray spectroscopy …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 15, Issue 2, 2024 · pp. 10–16 Read article
-
Gas Sensors Fabricated using Carbon Powder Derived from Dried Banana Peels Waste to detect Methanol, Ethanol, Acetone Vapors and Carbon Dioxide Gas
Abstract: Low cost and environmentally friendly activated carbon powder was synthesized using waste banana peels. Phosphoric acid was utilized as activation agent. Doctor blade method was employed to fabricate films of activated carbon on conductive or nonconductive glass substrates. Films were subsequently annealed at 70 0C for 30 minutes in air. According to XRD patterns, single phase of activated carbon was crystallized in thin film form. Carbon prepared from banana peels …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 14–25 Read article
-
Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
-
Synthesis and Characterizations of GeS0.5Se0.5 (I2) Single Crystals
Abstract: Material processing of layered structure remains a widely investigated subject in recent time due to their anisotropic properties. The large volume of work carried out in this field is of importance not only in basic science but also in industrial as well as energy applications. In this paper authors report growth of GeS0.5Se0.5 (I2) single crystals using Chemical Vapour Transport (CVT) technique with iodine as a transporting agent. Photograph of …
Published in Research & Reviews: A Journal of Embedded System & Applications · Vol. 7, Issue 1, 2019 · pp. 10–16 Read article
-
Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis Read article
-
Comparative Study of Structural and Optical Properties of Bismuth Ferrite Nanoparticles for Photovoltaic Applications Synthesized via Different Sol-Gel Methods
Abstract: Pure multiferroic bismuth ferrite (BiFeO3) nanoparticles were successfully synthesized using an energy-efficient, low-temperature sol-gel method, comparing two distinct approaches: auto-combustion and non-auto-combustion. To ensure phase stability, the precursor solution's pH was strictly maintained between 1 and 2 using ammonia solution (NH4OH), while ethylene glycol (C2H6O2) was employed as a chelating agent for the Fe3+ and Bi3+ cations. All samples underwent a final annealing process at 500 °C to promote crystallization. …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 83–94 Read article
-
Effect of Annealling on Optical Band Gap of Fe2O3 Thin Films on Amorphos Transparent Glass Substrate by Spray Pyrolysis Method
Abstract: The Fe 2 O 3 thin film has widely used photo-electrochemical cells. In this paper, the optical properties like band gap of thin films is depend on annealed temperature at 100 o C and 200 o C was discussed. The optical property of Fe 2 O 3 are studied by UV- Vis spectroscopy .The optical band gap decreased after increasing annealing temperature. The refractive index of Fe 2 O 3 …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 2, 2023 · pp. 25–29 Read article
-
Role of Strontium in Structural and Dielectric characterstics of Barium Titanate
Abstract: Ba₀.₇₅Sr₀.₂₅TiO₃ (BST) compound was synthesized through the conventional solid-state reaction methodology, aimed at investigating its structural, microstructural, and dielectric characteristics. The structural characterization was executed employing X-ray diffraction (XRD), and the resultant diffraction patterns were refined utilizing the Rietveld method, which substantiated the establishment of a single-phase perovskite configuration exhibiting tetragonal symmetry and belonging to the P4mm space group. The refined lattice parameters revealed subtle distortions correlating with the substitution …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1157–1163 Read article
-
A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
-
Synthesis of YSZ nanopowders by using PVA-metallic nitrate combustion method
Abstract: Yttria-stabilized zirconia (8YSZ) powder is widely used as a thermal barrier coatings material for various aeronautical gas turbine engine components and structures operating in high temperature environment as well as for the nozzle of solid rocket engine due to its relatively high thermal expansion coefficient, thermal reflectivity, low thermal and good corrosion resistance. The synthesis of single or composite metal oxides by combustion of metal-polyvinyl alcohol gel precursors (Me-PVA) has …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 14, Issue 3, 2024 · pp. 24–32 Read article
-
Effect of Bi2O3 Content and Sintering Temperature on the Frequency-Dependent Magnetic Properties of Nanosized Barium Hexaferrite
Abstract: The magnetic properties of commercially available nanosized barium hexaferrite (BaFe12O19) are studied. The particles were characterized using X-ray diffraction (XRD), vibrating sample magnetometer (VSM), and high-frequency magnetic measurements. The frequency-dependent magnetic properties viz. complex permeability and loss tangent were analyzed within the 10 MHz to 1 GHz range. Variations in complex magnetic permeability and loss tangent were discussed under varying sintering parameters such as temperature and sintering aid content. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 107–113 Read article