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42 articles for “SEM/EDX”
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Dielectric Studies of 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 Nanoceramic Fabricated by Chemo-mechanical Process
Abstract: The present investigation is aimed toward investigate a straightforward, inexpensive, and environmentally friendly chemo-mechanical method for preparing high-dielectric materials, specifically 0.5Ba0.8Ca0.2TiO3.0.5CaCu3Ti4O12 (BCT-CCTO), by combining metal nitrate combustion with solid TiO2 powder and titanium isopropoxide, Ti (OR)4. The composite was prepared by the mixing of individual materials of Ba0.8Ca0.2TiO3 and CaCu3Ti4O12 through the chemo-mechanical method. Initially, 99% pure Ba (NO3)3, Cu (NO3)2∙3H2O, TiO2 and glycine were taken in their stoichiometry ratios. …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 12–21 Read article
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Characterization of Mn Dopped SrAlO Nano-Phosphors Prepared via Sol-Gel Method
Abstract: Strontium aluminate with Mn dopped phosphor was synthesized by Sol-Gel method using Strontium Acetate, Aluminium Acetate as raw material and 2-methoxyethanol as complexing agent. The transparent sol was preheated at 100°C for 2 h and then the precursor was finally annealed at 950°C for 2 h. The phosphor emits luminescence with peak wavelength at 395 nm and 520 nm under near-ultraviolet excitation at 360 nm. The morphology, composition and structure …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 6, Issue 3, 2016 · pp. 5–10 Read article
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Surface Structure of Hydroxyl Apatite from Fluorosis Enamel
Abstract: Fluorosis is a condition due to ingestion of excessive amounts of Fluor that can cause the change in teeth structure and strength. Currently, a poor explanation was available to describe the surface structure of crystal hydroxylapatite that contributes to influence the macro characteristic of fluorosis enamel. The objective of this research is to describe the surface structure of crystal hydroxylapatite (HA) in fluorosis enamel. Scanning Electron Microscopy/ Energy Disperse X-Ray …
Published in Research and Reviews: A Journal of Dentistry · Vol. 2, Issue 1-3, 2011 · pp. 60–68 Read article
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Fabrication of Nanocrystalline Fe2Mn2Ni2Zn2O11 at Different Calcination Temperatures and Its Analysis
Abstract: The superconducting nanocrystalline ceramic powder Fe2Mn2Ni2Zn2O11 was designed and fabricated by a high-temperature special furnace. In the area of ceramic superconductors, particle size is an important factor. Here the authors analyzed the particle size and strain of the nanocrystalline ceramic super conducting material. The sample was analyzed by X-ray Diffraction (XRD), particle size determination, SEM and EDX. The comparison of XRD results with JCPDS files confirmed the orthorhombic structure of …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 16, Issue 3, 2014 · pp. 8–15 Read article
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High Power Nd: YAG Laser Treatment of Zirconium Silicate Surface
Abstract: The surface modification obtained by laser beam irradiation requires a proper relationship among the laser beam parameters, to assure the irradiated surface morphology and physical chemistry properties surface. In this study, the photothermal effect of high power Nd: YAG laser at 1064 nm wavelength for different durations on the surface properties of zirconium silicate (ZrSiO4) ceramics was investigated. Specimens of zirconium silicate (ZrSiO4) ceramic pieces were divided into four samples …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 3, 2020 · pp. 16–24 Read article
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Preparation and Characterization of PVA-MgO Nanocomposite Films
Abstract: In this work, Magnesium Oxide Nanoparticles (MgO NPs) doped with 3 g of polyvinyl alcohol (PVA) at different weight percentages (0, 2, 4, 6, and 8 wt.%) using the solvent casting method, to fabricate thin PVA-MgO nanocomposite (NC) films. These films were characterized by (i) XRD, SEM, EDX, DLS, and Zeta Potential for morphological studies, (ii) FTIR spectra and UV-Visible techniques for spectroscopic studies and (iii) DSC for thermal studies. …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 27, Issue 2, 2025 · pp. 40–62 Read article
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Bio Materials and Nanotechnology: Green Tea (Waste)– Aluminium Nanoparticles (Gt-Al Nps) For Methylene Blue Adsorption
Abstract: This study examines the adsorption of Methylene Blue (MB) dye from aqueous solutions using Aluminium Nanoparticles synthesized with green tea powder as a biological reducing agent. Methylene Blue, an aromatic phenothiazine dye, is widely applied in medical diagnostics and various industrial processes, but its uncontrolled release into water bodies leads to environmental pollution due to its intense colour, stability, and potential toxicity. Therefore, identifying an efficient and eco-friendly adsorbent for …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 96–107 Read article
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Water Chestnut Stem-Derived Biochar Supported AgNPs/AC-CTS-PVA Composite Gel for Wastewater Treatment and Potent Antibacterial Performance
Abstract: In the present study, green and efficient Ag-NPs functionalized activated carbon/chitosan-polyvinyl alcohol (AgNPs/AC-CTS-PVA) composite gel was successfully synthesized using water chestnut stem-derived biochar for wastewater treatment and antibacterial applications. The composite was characterized by FTIR, XRD, SEM-EDX, and TGA analyses, confirming the successful incorporation of crystalline Ag nanoparticles within the polymeric matrix and improved thermal stability. The material was tested regarding the removal of the dye of methylene blue (MB) …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1129–1144 Read article
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H2 Production by Methanol Steam Reforming over Copper Impregnated Anodized Aluminum Oxide (AAO)
Abstract: Hydrogen production by methanol steam reforming (MSR) is easy and simple as compared to other reforming methods using fossil fuels such as methane steam reforming. The catalysts for MSR are well developed and available commercially. When constructing a small or micro reformer, the catalyst often needs to be coated on the wall of the metal substrate. In this case, the bonding between the metal surface and the catalyst layer must …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 1, 2014 · pp. 23–28 Read article
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Ceria and Modified Ceria: A Reusable Catalyst for the Green Synthesis of 2,3-diphenyl Quinoxaline at Room Temperature
Abstract: Simple, highly versatile and efficient synthesis of 2,3-diphenylquinoxalines is achieved from benzil and o-phenylene diamine using ceria and modified ceria as the catalyst. Modification of ceria is done using different weight percentage of zirconia. The catalysts are characterized by XRD, FT-IR, BET surface area, TGA and EDX-SEM. The advantages of this method are short reaction times, milder conditions and easy work-up. The product could be separated from the heterogeneous catalyst …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 3, 2014 · pp. 1–11 Read article
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Preparation of Phase – Pure Nanocrystalline Anatase and Rutile TiO2 using Hydrolysis of TiCl4 in presence of surfactants
Abstract: Hydrolysis of TiCl4 was carried out in two different ways to prepare nano crystalline TiO2. In the first method the hydrolysis of TiCl4 was carried under high acidic conditions at low temperature. In the second method hydrolysis was carried out using (NH4)2SO4 as an additive. It can be seen that the hydrolysis of TiCl4 under high acidic conditions promotes the growth of rutile phase of TiO2, where as hydrolysis in …
Published in Journal of Materials & Metallurgical Engineering · Vol. 8, Issue 1, 2018 · pp. 31–40 Read article
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Effect of Curing Time on Physico-mechanical Properties on Dental Composite
Abstract: This study aim to investigate the influence of curing time on physical and mechanical properties of a dental composite cured by using LED light with intensity of 1500 mW/cm2 in the range of 440-480 nm. We prepared the glass ionomer powder by fusion of various inorganic components at high temperature and studied the influence of silica/alumina ratio keeping other inorganic salts such as Calcium fluoride (CaF2), Sodium Fluoride (NaF), Calcium …
Published in Journal of Polymer & Composites · Vol. 10, Issue 3, 2022 · pp. 36–47 Read article
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A Review on Removal of Heavy Metal from Polluted Water using Low Cost Bio-adsorbent
Abstract: ABSTRACTThis review paper presents the performance of natural low cost bio-adsorbent used for the removal of heavy metals from polluted water. The current study focuses on various natural low cost bio-absorbents such as native algae, papaya peel, bone powder, Nile rose plant, natural clayey, rice straw, rice bran, rice husk, coconut shell, Neem leaves, hyacinth roots, powder of heartwood, Moringa oleifera bark an agricultural solid waste, resin of mimosa tannin, …
Published in Journal of Water Pollution & Purification Research · Vol. 5, Issue 1, 2018 · pp. 1–8 Read article
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Sophisticated instrumental analysis of Trinakantamani Pishti by various methods.
Abstract: Trinakantamani Pishti was prepared by reference of Bheshaja Samhita, Bhasma-Pishti Prakarana 1 , which is indicated for Vataja, Pittaja and Kaphaja Galagraha, Gala Granthi, Gandamala. Aim- to standardize Trinakantamani Pishti pharmaceutically. Methods- Trinakantamani Pishti was prepared as per reference of Bheshaja Samhita, Bhasma-Pishti Prakarana and it was analysed by various sophisticated instrumental analysis method like SEM (Scanning Electron Microscopy) and EDX (Energy Dispersive Spectroscopy), X-ray Diffraction (XRD), Particle size analysis …
Published in Research & Reviews: A Journal of Drug Design & Discovery · Vol. 10, Issue 1, 2023 · pp. 7–13 Read article
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Green Synthesis and Functional Evaluation of Ag–Polypyrrole/TeO2 Nanocomposites for Advanced Electronic Applications
Abstract: Ag–PPy/TeO₂ nanocomposites with TeO₂ loadings ranging from 2% to 10% were synthesized using an in-situ chemical polymerization method. Green tea extract, rich in phytochemicals, acted as both a reducing and stabilizing agent to facilitate the formation of metal oxide nanoparticles. The structural and morphological characteristics of the nanocomposites were analyzed using FTIR, PXRD, and SEM techniques. FTIR confirmed the successful integration of Ag, TeO₂, and PPy functional groups. PXRD patterns …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 64–76 Read article
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Experimental Assessment and Statistical Argument of Al-Si/CSA/MoS2 Hybrid Composites for Mechanical and Tribological Characteristics
Abstract: To augment the mechanical and tribological properties of Al-Si matrix composites complement with molybdenum disulphide (MoS₂) and coconut shell ash (CSA), a mixed experimental and Face-Centered Composite (FCC)strategy was employed. A liquid metallurgical method called stir casting was used to create hybrid composites with 5–15 wt.% CSA and 1–3 wt.% MoS₂. A FCC experimental design with thirty runs was used to thoroughly evaluate the materials. This design allowed for the …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 792–802 Read article
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Silver Particles coating on polypropylene matrix for bacterial filter property
Abstract: Silver particles have a wide range of biomedical applications, including their use as drug. In this paper, we report on the synthesis of silver particles using crude aqueous extract of Manihot esculenta leaf extract. Two different (conventional stirring and ultrasonic) methods were employed in the reduction of AgNO3 process. Native extract as well Ag colloidal extract were checked cytotoxicity against Human Cervical Carcinoma cell. The anti cancer results achieved excellent …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 7, Issue 3, 2020 · pp. 16–25 Read article
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Green Synthesis of Selenium Nano-metalloid from the extract of Cabbage (Brassica oleracea var. capitata) leaf and its Antimicrobial Activities
Abstract: Green synthesis specifies the creation of nano-size particles (NPs) by a biological process using the reducing properties of metabolites in the plant extracts. The present work reports the use of cabbage (Brassica oleracea var. capitata.) leaf extract as a reducing and stabilizing agent to synthesize selenium nanoparticles (SeNPs) via the green route of synthesis. The as-prepared SeNPs were analyzed by UV–vis spectroscopy, FTIR, DLS, SEM, and EDX. Nano-crystalline SeNPs has …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 1, 2019 · pp. 12–20 Read article
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Biosynthesis of Zinc Oxide Nanoparticles and Their Revolutionary Impacts on Agroindustry: Review
Abstract: Nanotechnology is a new approach of science which provides alternative tool in many fields including agriculture. This comprehensive review focuses on the biosynthesis and characterization of zinc oxide nanoparticles (ZnO NPs), highlighting their vast potential in agroindustry applications. Unlike traditional physical and chemical methods, which are often costly, time-consuming, and involve hazardous materials, this review explores the promising biological synthesis routes, offering a more sustainable and eco-friendly alternative for producing …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 26, Issue 2, 2024 · pp. 33–50 Read article
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Extracellular Biosynthesis of Silver Nanoparticles using the Fungus Pleurotus ostreatus and their Antibacterial Activity
Abstract: In the present study, an eco-friendly process for the synthesis of nanomaterials using a fungus (Pleurotus ostreatus) has been attempted. The fungus supernatant of seed culture was used for the biosynthesis of silver nanoparticles. The aqueous silver ions were reduced to silver metal nanoparticles when treated with the fungal supernatant. After 72h of treatment, silver nanoparticles were obtained. These silver nanoparticles were characterized by UV–Vis spectroscopy, scanning electron microscopy (SEM), …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 2, 2012 · pp. 28–38 Read article