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217 articles for “synthesis methods”
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Green Synthesis and Functional Evaluation of Ag–Polypyrrole/TeO2 Nanocomposites for Advanced Electronic Applications
Abstract: Ag–PPy/TeO₂ nanocomposites with TeO₂ loadings ranging from 2% to 10% were synthesized using an in-situ chemical polymerization method. Green tea extract, rich in phytochemicals, acted as both a reducing and stabilizing agent to facilitate the formation of metal oxide nanoparticles. The structural and morphological characteristics of the nanocomposites were analyzed using FTIR, PXRD, and SEM techniques. FTIR confirmed the successful integration of Ag, TeO₂, and PPy functional groups. PXRD patterns …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 64–76 Read article
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Steel Structural and Functional Characteristics Focusing on Corrosion Mechanisms
Abstract: This research article examines steel structural and functional characteristics, focusing on corrosion mechanisms and inhibitor protection strategies. Steel corrosion affects numerous industries, causing significant economic losses and safety risks. Fundamental electrochemical processes behind various corrosion forms including uniform, pitting, crevice, galvanic, intergranular, and stress-induced corrosion are explained. The chapter highlights the steel industry's importance while investigating how corrosion impacts performance and longevity. Protection methods discussed include material selection, environmental modification, …
Published in International Journal of Minerals · Vol. 2, Issue 2, 2025 · pp. 25–34 Read article
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A comprehensive review on Sustainable Pathways to Synthesize 2, 5-Furandicarboxylic Acid (FDCA) from 5-Hydroxymethylfurfural (HMF) via Oxidative Processes
Abstract: The increasing global concern over the environmental impact of traditional plastics derived from petroleum and natural gas has spurred a search for more sustainable alternatives. Bioplastics, which are derived from renewable sources and may be biodegradable, have garnered significant interest as eco-friendly materials. Among the promising building blocks for bioplastics, 2,5-Furandicarboxylic Acid (FDCA) has emerged due to its potential to enhance polymer properties. One key precursor for bioplastics, 5-Hydroxymethylfurfural (5-HMF), …
Published in Emerging Trends in Chemical Engineering · Vol. 11, Issue 2, 2024 · pp. 01–13 Read article
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Quality Control and Assurance Practices in Modern Pharmaceutical Industry
Abstract: This brief overview outlines the global techniques for figuring out the prevalence of geotaxis impurities (residual solvents and various inorganic and organic impurities) in medications. It is now necessary to reveal a pharmaceutical product's purity and impurity profiles due to both national and international regulations. These elements are discussed, together with the kinds of impurities, their origins, their control, and regulatory issues, as well as the significance of pharmaceutical quality, …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 12, Issue 3, 2025 · pp. 07–13 Read article
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Energy Storage Properties of hy-BST3/PVDF Nanocomposite for Dielectric Capacitor Application
Abstract: In the present research work, we have synthesized the ferroelectric ceramic Ba0.7 Sr0.3TiO3 (BST3)/PVDF (Polyvinylidene difluoride). Polymer nanocomposites for energy storage applications, designed to synergistically combine the high dielectric permittivity of hydroxylated barium strontium titanate (hy-BST3) with the mechanical flexibility and electroactive properties of poly(vinylidene fluoride) (PVDF). Hydroxylated Barium Strontium Titanate (hy-BST3) has been synthesized using the sol-gel combustion method followed by surface hydroxylation using H2O2 to achieve nanoscale particles …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 908–918 Read article
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SYNTHESIS AND CHARACTERIZATION OF Mn2+ DOPED LiPbX3(X = Cl, Br, I)
Abstract: In this paper the structural, electronic and optical properties of Mn doped Pb based cubic perovskites LiPbX3(X= Cl, Br and I) were studied by wet chemical method (sol gel method). For Mn doped LiPbX3(X= Cl, Br and I) NCs, MnCl2 and PbBr2 were added in molar feed ratio 1.35 mole% and nan crystal were examine with the help of TEM and their structure were confirmed by X-ray diffraction (XRD). Additionally, …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 48–54 Read article
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Synthesis, spectroscopic, crystal structure, Hirshfeld surface, computational, and biological investigations on Isophorone derivatives: 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one
Abstract: FT-IR, 1H NMR, and 13C NMR spectroscopy were among the spectroscopic methods used to synthesize and analyze 3-(3,4-dimethoxystyryl)-5,5-dimethylcyclohex-2-en-1-one, a new isophorone derivative. Single-crystal X-ray diffraction (SCXRD) was used to determine the crystal structure, which showed that the molecule crystallizes in a monoclinic system (space group P121/c1) with packing configurations and intermolecular interactions. To learn more about the non-covalent interactions influencing the crystal packing, Hirshfeld surface analysis was used. In order …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 2, 2025 · pp. 51–69 Read article
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Design, Synthesis, and Spectroscopic Elucidation of 3-Methyl-1-Phenylpyrazol-5-One: A Cheminformatics-Aided Approach to Heterocyclic Drug Scaffolds
Abstract: Pyrazolone, a notable heterocyclic compound, has drawn increasing interest due to its broad pharmacological profile and structural versatility. The synthesis, characterisation, and biological assessment of new pyrazolone derivatives are examined in this work. A comprehensive review of existing synthetic strategies is presented, emphasizing green and efficient methodologies. Novel derivatives were synthesized using varied starting materials and catalytic systems, followed by structural confirmation through spectroscopic analyses, including NMR, IR, and mass …
Published in International Journal of Cheminformatics · Vol. 3, Issue 1, 2025 · pp. 29–40 Read article
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Adsorptive Removal of Rhodamine-B Using Eco- Synthesized Green Tea–Aluminium Nanoparticles
Abstract: This study examines the use of Green Tea–Aluminium Nanoparticles (GT-Al NPs), a unique and eco-friendly adsorbent, to remove the dangerous Rhodamine-B dye from water. For characterisation, SEM, FTIR, TGA, and EDX were employed. We evaluated the effects of pH, temperature, dosage, contact time, and initial dye concentration on adsorption efficiency. First- and second-order pseudo models were used to characterize adsorption kinetics, and the Langmuir model explained equilibrium, as well as …
Published in Emerging Trends in Chemical Engineering · Vol. 12, Issue 3, 2025 · pp. 61–72 Read article
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Innovative Approaches in Bioinspired and Biomimetic Membrane Technologies: Bridging Nature and Engineering
Abstract: Bioinspired and biomimetic membranes represent a ground breaking advancement in membrane technology, offering innovative solutions to critical global challenges in water purification, chemical separation, and energy conversion. These membranes leverage the exceptional transport properties of biological systems, particularly through the incorporation of aquaporin proteins, which facilitate rapid and selective water transport. This review synthesises recent developments in aquaporin-based membranes, highlighting their remarkable efficiency in desalination processes, where they serve as …
Published in International Journal of Membranes · Vol. 1, Issue 2, 2024 · pp. 53–60 Read article
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Synthesis, Characterization, and Thermogravimetric Analysis of Polylactic Acid-Based Bio-Adhesive for Industrial Applications
Abstract: This study investigated the synthesis, characterization, and thermogravimetric analysis of polylactic acid (PLA)-based bio-adhesives for industrial applications. The adhesive was synthesized using an emulsion polymerization method with varying compositions of PLA and vinyl acetate. The physicochemical, mechanical, and thermal properties of the synthesized adhesives were assessed through pH analysis, viscosity measurement, peel strength evaluation, tack tests, biodegradability investigations, Fourier Transform Infrared Spectroscopy (FTIR), Differential Scanning Calorimetry (DSC), and Thermogravimetric Analysis …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 · pp. 39–54 Read article
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Synthesis and Characterization of Forsterite Incorporated HDPE Composites for Microwave Substrate Application
Abstract: High Density Polyethylene (HDPE) combined with dispersed forsterite (Mg₂SiO₄) powder was utilized to fabricate polymer matrix composites (PMCs) aimed at high-frequency microwave substrate applications. Forsterite powders were synthesized using the mixed oxide method, and their phase purity was confirmed by X-ray diffraction (XRD) analysis. The dispersion and morphology of the ceramic filler within the HDPE matrix were examined through Scanning Electron Microscopy (SEM), ensuring a homogeneous distribution essential for optimal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 109–120 Read article
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Intelligent Electromagnetic Synthesis: An AI-Driven IoT Framework for Adaptive Antenna Design in Missile Navigation
Abstract: The rapid evolution of hypersonic and long-range tactical missile systems necessitates antenna architecture capable of maintaining robust communication links under extreme thermal, mechanical, and signal-jamming environments. Traditional antenna design methodologies often relying on iterative simulation cycles and static optimization are increasingly insufficient for the real-time requirements of modern aerospace navigation. This paper proposes an AI-driven, IoT- integrated framework that facilitates autonomous antenna design and performance optimization. By deploying a distributed …
Published in International Journal of Radio Frequency Innovations · Vol. 4, Issue 1, 2026 Read article
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Wettability and Physiothermal Analysis of Silver-Reinforced Eggshell-Derived Hydroxyapatite Based Biocomposite
Abstract: Hydroxyapatite (HAp), a biocompatible ceramic material, has garnered significant interest in medical applications due to its natural bone type replica. The current study investigates the physical, wettability, and thermal properties of a novel HAp derived from eggshell waste and reinforced with silver nanoparticles at 0.0, 0.1, 0.2 and 0.5 weight % concentration using chemical precipitation method and termed as HAP0.0Ag, HAP0.1Ag, HAP0.2Ag and HAP0.5Ag respectively. As observed, the Fourier transform …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 300–314 Read article
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Squeeze Casting of Hybrid Aluminum Matrix Composites: A Critical Review of Process Optimization, Reinforcement Strategies, and Performance Outcomes
Abstract: Increasing demand for lightweight, performance-oriented components in automotive, aerospace, and defense industries has driven advancements in squeeze casting, a hybrid technique merging forging and die-casting advantages to produce near-net-shape aluminum matrix composites (AMCs) with superior mechanical-tribological properties. This review critically examines the interplay of process parameters (e.g., squeeze pressure: 70–150 MPa, melt temperature: 650–800°C), reinforcement characteristics (volume fraction ≤10%, particle size: 10–71µm), and interfacial engineering strategies (flux-assisted bonding, ultrasonic dispersion) …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 2, 2025 · pp. 52–60 Read article
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A Mini Review of Synthesis and Applications of Functionally Graded Materials
Abstract: Material composition or microstructure varies gradually along the thickness over a specific volume in functionally graded material (FGM) that results in spatial change in properties like thermal conductivity, strength, stiffness, electrical, magnetic, and light properties, etc. Application of the concept of FGM leads to a single product that has multiple properties in it as demanded by the operational or functional requirements of the product under service conditions. It also allows …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 54–65 Read article
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Synthesis of Thermal Resistant and Transparent Al2O3 Reinforced Epoxy-Based Composite Coatings
Abstract: This study explores the influence of thermal treatment on the structural, optical, and surface wettability characteristics of epoxy-based composite coatings reinforced with 3 wt.% aluminum oxide (Al₂O₃) nanoparticles. The coatings were synthesized via a dip-coating method on carbon fiber substrates and subjected to controlled thermal treatments at 300 °C, 400 °C, and 500 °C to assess their thermal resilience. X-ray diffraction (XRD) analysis confirmed the structural integrity of the composite …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 178–183 Read article
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Role of biosynthesized Copper nanoparticles in Agriculture and other fields
Abstract: In the last decades, nanotechnology has emerged as a new field of technology because of its unique qualities. The use of chemicals in medicines and agriculture such as fertilizers, pesticides, herbicides, and insecticides are very harmful to the environment so by the use of this revolutionary technology we can reduce the toxic effects on the environment. However, a biological method is very easy, simple, and free from any chemical hazards, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 14, Issue 2, 2024 · pp. 39–53 Read article
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Advancements in Machine Learning: A Comprehensive Review of Algorithms, Applications, and Future Directions
Abstract: Gaining knowledge of Machine learning (ML)-guided format algorithms leverage predictive models to generate novel devices with optimized properties across several domains, which include drug discovery, fabric synthesis, and biomolecular engineering. Selecting an effective format set of policies consists of identifying appropriate hyperparameters, predictive models, and generative mechanisms to maximize format fulfilment. This study introduces an established method for set of policies requirements, ensuring that generated designs meet predefined fulfilment criteria, …
Published in Recent Trends in Programming languages · Vol. 12, Issue 2, 2025 · pp. 17–33 Read article
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Synthesis of Green Nanoparticles for Degradation of Cellulose
Abstract: Late advances in nano-science and technology have also prompted the advance of novel nanomaterials, which eventually increment potential eudaimonia and ecological perils. Enthusiasm for growing Earth's thoughtful ways for the mix of auriferous nanoparticles has been enlarged. The intention is to limit the negative effects of the designed methodology with artificial compounds and subordinate mixes. The abuse of assorted biomaterials for the mix of nanoparticles is a profitable methodology in …
Published in Journal of Modern Chemistry & Chemical Technology Read article