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277 articles for “Spectroscopic methods.”
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Design and Synthesis of Functionalized Copolymers for Enhanced Interfacial Compatibility in Polymer Matrix Composites
Abstract: Interfacial adhesion between the polymer matrix reinforcing phase affects significantly the mechanical and thermal behavior of polymer composites. The study reports on the design and synthesis of functionalized copolymers in the efforts to establish interfacial compatibility based on chemical design. The reinforcements were functionalized doping polar functional groups such as glycidyl methacrylate and maleic anhydride during free-radical copolymerization to form copolymerizing reactive sites that interacted with the reinforcement surfaces. Confirmation …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1404–1418 Read article
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Ab Initio and Density Functional Theory Studies on D-Serine
Abstract: The Hartee-Fock and density functional method (B3LYP) with 6–311++G (d, p) basis set were employed to study the structural and spectroscopic properties of amino acid D-serine in ground state. The structural and vibrational parameters of amino acid D-serine were obtained using optimised conformer. Using Vibrational Energy Distribution Analysis (VEDA) 4 program and theoretically obtained FTIR and FT-Raman data complete assignment of vibrations and analysis of fundamental modes of the compound …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 3, 2020 · pp. 29–45 Read article
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Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article
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Influence of Supplementary Cementitious Materials on Chemical Shrinkage in Cement
Abstract: Chemical shrinkage is the volume reduction observed in cement during early hydration due to chemical reactions, which critically influences the internal stresses, cracking tendencies, and durability of cementitious system. Present study is focused on effect of supplementary cementitious material (SCM) on chemical shrinkage. Dilatometry method is used to assess the impacts of SCMs on chemical shrinkage, in this this study. The research incorporates experiments with laboratory-synthesized cement and three SCMs—fly …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 98–107 Read article
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Isolation and Characterization of Glucuronide Compound from Luffa Tuberosa (Roxb.) for Potential Applications in Polymer Chemistry
Abstract: This study explores the isolation process of glucuronide compounds from Luffa tuberosa (Roxb.) using an efficient and cost-effective method. The extracted compound, Gypsogenin-3β-O-β-D-Methyl glucuronide, is characterized using spectroscopic techniques such as IR, NMR, and Mass Spectrometry. The polymeric nature of glucuronide-based compounds and their potential applications in polymer and composite materials are discussed. The findings highlight the suitability of glucuronide derivatives in biomedical, pharmaceutical, and polymeric drug delivery systems. Additionally, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 566–572 Read article
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Analysis of Thermo-Mechanical Properties in Cement Mortar Using Synthesized Silicate Microencapsulation of Phase Change Materials by Sol-Gel Process
Abstract: This investigation delves into improving building thermal comfort using microencapsulated phase change materials (PCM@SiO2) in cement mortar. The encapsulation process, achieved via a sol-gel method, envelops PCM in a silicate shell Differential Scanning Calorimetry (DSC) and Fourier-Transform Infrared Spectroscopy (FTIR) were used to confirm the thermal properties and integrity of encapsulated PCM, which showed an encapsulation efficiency of 92.7% and a thermal storage capacity of 99.7%. The study involved the …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 152–160 Read article
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Using Artificial Intelligence for The Design of Polymeric Drug Delivery Systems
Abstract: AI is cost effective and time efficient process. Artificial intelligence is a method which uses high speed calculation, the improvement regarding algorithm along with collection about biological and chemical features in pharmaceutical exploration and development .Present day because continuous progress towards machine learning (ML),Artificial intelligence an effective statistics analysing technology might have been broadly utilized in drug design .In pharmaceutical exploration and research employ of AI in target identification, compound …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1018–1027 Read article
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Strategic Approaches to Sustainable Lithium Extraction: Advances in Technology, Resource Recovery, and Environmental Management
Abstract: Lithium, a critical mineral for modern technological advancements, is in high demand due to its role in the production of lithium-ion batteries, which power electric vehicles, portable electronics, and renewable energy storage solutions. This paper provides a comprehensive overview of lithium’s sources, including pegmatites, brine deposits, and sedimentary lithium minerals, while examining production, extraction methodologies, and challenges related to sustainability and environmental impact. Additionally, advancements in laser-induced breakdown spectroscopy (LIBS) …
Published in International Journal of Minerals · Vol. 1, Issue 2, 2024 · pp. 8–13 Read article
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Wettability and Physiothermal Analysis of Silver-Reinforced Eggshell-Derived Hydroxyapatite Based Biocomposite
Abstract: Hydroxyapatite (HAp), a biocompatible ceramic material, has garnered significant interest in medical applications due to its natural bone type replica. The current study investigates the physical, wettability, and thermal properties of a novel HAp derived from eggshell waste and reinforced with silver nanoparticles at 0.0, 0.1, 0.2 and 0.5 weight % concentration using chemical precipitation method and termed as HAP0.0Ag, HAP0.1Ag, HAP0.2Ag and HAP0.5Ag respectively. As observed, the Fourier transform …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 300–314 Read article
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Unraveling Mixed Ionic-Electronic Conduction in Lithium-Substituted Rubidium Tetra Titanates via Dielectric Spectroscopy and EPR Analysis
Abstract: Lithium-substituted Rubidium Tetra Titanates with varying concentrations of lithium carbonate (Li₂CO₃) — specifically 0.01, 0.05, and 0.1 molar percentages — were successfully synthesized using a conventional high-temperature solid-state reaction method. The resulting compounds follow the general chemical formula Rb₂₋ₓLiₓTi₄O₉. X-ray diffraction (XRD) analysis confirmed that lithium ions were successfully incorporated into the crystal lattice without disrupting the fundamental layered structure of the host material. The crystal system remained monoclinic across …
Published in Research & Reviews : Journal of Physics · Vol. 14, Issue 2, 2025 · pp. 19–29 Read article
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Photochemical Insights into Light: Responsive Heterocyclic Compounds
Abstract: eterocyclic compounds are significant in a wide range of chemical fields. They are crucial components of the structural makeup of bioactive substances. Such compounds can be conveniently transformed through photochemical processes. Chemical reagents are rarely utilized. It is possible for members of one compound family to change into members of another. There is discussion of three key categories of photochemical rearrangements involving heterocyclic compounds: Photochemical reactions involving hydrogen atom transfer …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 1, Issue 2, 2023 · pp. 01–07 Read article
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Properties and antimicrobial activity of bacterial nanocellulose composite incorporated with silver nanoparticles based on green synthesis
Abstract: Green silver nanoparticles (AgNPs) synthesized using medical plant extracts as capping and reducing agents demonstrate broad applicability in addressing the threat posed by infections. In this study, we present a sustainable, low-toxicity, and cost-effective bacterial nanocellulose composite with silver nanoparticles based on green synthesis that uses Origanum vulgare as a reducing agent due to numerous biological components. The formation of AgNPs in composite and morphological properties was analyzed using scanning …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 323–328 Read article
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Enhancement of Dielectric Properties of PVDF Composites with MWCNT and GCNF Fillers
Abstract: The paper discusses the role of multiwalled carbon nanotube (MWCNT) and graphitized carbon nanofibre (GCNF) in Polyvinylidene fluoride (PVDF) composites prepared by melt mixing method. Analytical studies were carried out using X-ray diffraction analysis (XRD) and Fourier transform infrared spectroscopy (FTIR) for understanding the role of fillers. Formation of β phase crystalline structure with a relative increase in β phase content is observed and is maximum at 5 wt.% of …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 43–52 Read article
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A Comparative Study of Structure, Morphology and Optical Properties of CaAl2O4 Phosphors by Sol–Gel Method
Abstract: In this paper, monoclinic CaAl2O4 phosphor with different weight percentage of aluminium was synthesized by low temperature sol–gel method. The prepared samples were characterized by X-ray diffraction (XRD) analysis, Fourier transform infra red (FTIR), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and photoluminescence emission spectra (PL). The XRD analysis showed that CaAl2O4 have monoclinic structure. The average size of the particles lies between 88 and 109 nm. It was …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 3, 2015 · pp. 1–10 Read article
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A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
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Electrical Measurements on La-modified Four-Layered Aurivillius Ceramics
Abstract: Bismuth layered structure ferroelectric (BLSF) of Aurivillius family is found to be attractive owing to its scientific and technological point of view. These materials have potential ferroelectric applications owing to the fact of its high Curie temperature, high temperature piezo-devise and ferroelectric random access memory (FRAM), applications. In addition, Bi-modified compounds have shown improved ferroelectric properties. However, the plausible reason for improving ferroelectric properties in Bi-modified is still unclear. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 157–170 Read article
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Preparation and Characterization of TiO2 Nanoparticles by Green Method
Abstract: In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 61–67 Read article
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Extraction of Essential oil from Curry leaves
Abstract: Murraya koenigii (Curry leaves) contain many useful chemical constituents. The leaves which known as daun kari in malaysia is belong to family Rutaceace and can be found in Malaysia, India, Bangladesh, Nepal, Sri Lanka. The aim of this study to characterize the components of essential oil of the leaves and compare yield percentage of the oil which is extracted from steam distillation and hydro-distillation. The essential oil is extracted by …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 10, Issue 1, 2019 · pp. 16–20 Read article
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Characterization of Activated Carbon Prepared from Citrus Sinensis (Orange) Peels by X-ray Fluorescence Spectroscopy (XRF)
Abstract: The orange (specifically, the sweet orange) is the fruit of the citrus species Citrus sinensis in the family rutaceae. Citrus sinensis (orange) fruit is one of the common traditional plants grown in many areas in India. The wastes of the Citrus sinensis (orange) fruit called orange peels were used to prepare activated carbon through chemical activation method. The activated carbon is an excellent adsorbent and its applications are widely described …
Published in Emerging Trends in Chemical Engineering · Vol. 2, Issue 3, 2015 · pp. 50–52 Read article
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Bergenin: Review of The Methods of Determination and Quantification
Abstract: Studies have shown that Bergenin has various pharmacological functions, such as Anti-lithiatic, Anti-oxidant, anti-inflammatory, Anti-bacterial, Anti-viral, Anti-cancer, Anti-cholinesterase, Anti-diabetic, Hypolipidemic, Anti-tussive, Hepatoprotective and Immunomodulatory. Bergenin is found in the Saxifragaceae, Euphorbiaceae, Myrsinaceae, Dipterocarpaceae, and Fabaceae genera and a range of beneficial effects on human health. The number of bioactive compounds in various bergenia species must be determined in order to achieve the best quality raw material for herbal preparations. As …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 8, Issue 2, 2023 · pp. 52–66 Read article