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117 articles for “scanning electron spectroscopy (SEM)”
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Green synthesis of zinc oxide and copper oxide nanoparticles and their effect against wilt fungus, Fusarium udum.
Abstract: Nowadays nanoparticles (NPs) come out as powerful tools to enhance crop production and protection. Biosynthesis of NPs has a vital role and an alternate to chemical and physical methods because it is simple, easy, eco-friendly, and free from chemical hazards. Zinc oxide (ZnO) and copper oxide (CuO) NPs were synthesized from leaves extract of Lantana camara (L.) and Nerium oleander (L.) and characterized by using several techniques such as transmission …
Published in Research and Reviews : A Journal of Life Sciences · Vol. 13, Issue 3, 2023 · pp. 1–5 Read article
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Influence of Gd Doping in Structural, Morphological and Optical Properties of Zno Nanostructures Synthesised Via Sol-Gel Processes
Abstract: In this study, nanocrystalline Zn1-xGdx (x=0.0 and 0.03) samples were synthesised via the Sol-gel combustion process. An array of analytical techniques was employed to examine the prepared samples to determine their different physical features. For both pristine and Gd-doped samples, the crystal symmetry is hexagonal with the P63mc space group which is verified via the Rietveld refinement analysis of X-ray diffraction (XRD) data. The atoms' bond length Zn-O and bond …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 219–225 Read article
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A Review on Synthesis and Characterisation of Nanoclusters
Abstract: Nanoclusters are materials with size less than 2 nm. Because of their small size and high surface area, they have properties which can be used for various applications like bio-sensing, catalysis, fuel cells etc. The synthesis techniques are carried out in such a way that the size-selection of nanoclusters take place. The synthesis methods discussed in this review include both top-down and bottom-up techniques. The different characterization techniques taken into …
Published in Emerging Trends in Chemical Engineering · Vol. 8, Issue 1, 2021 · pp. 1–19 Read article
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Preparation and Characterization of Microwave-assisted Candesartan Cilexetil Solid Dispersions
Abstract: The aim of the present study was to enhance the solubility & dissolution rate of a poorly soluble, BCS class II drug candesartan cilexetil (CC), using its solid dispersions (SDs) with polyethylene glycol (PEG) 6000 & hydroxypropyl methylcellulose (HPMC) E5. Solid dispersions were prepared by melting, solvent evaporation & microwave method. The dispersions were evaluated for various in vitro parameters such as solubility study, dissolution study, fourier transform infrared spectroscopy …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 4, Issue 3, 2013 · pp. 9–19 Read article
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Development and Characterization of Antimicrobial Polymer Composites for Food Packaging Applications
Abstract: The increasing demand for sustainable and antimicrobial food packaging materials has led to extensive research in polymer-based composites. This study focuses on developing a polyethylene terephthalate-ethylene vinyl acetate (PET-EVA) composite reinforced with metal oxide nanoparticles (MONs), including Cu₂O, ZnO, and MgO₂. These nanoparticles were selected for their antimicrobial properties and ability to enhance the functional characteristics of the composite. Structural, chemical, mechanical, and barrier properties were extensively evaluated to determine …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 86–93 Read article
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Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
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Characterization of Polyurethane at Multiple Scales for Erosion Mechanisms Under Sand Particle Impact
Abstract: Thin polyurethane layers have been widely used as erosion-resistant coatings on helicopter rotor blades such as UH-60 Black Hawk and Eurocopter SA 315. Published research has mainly focused on empirical studies that relate the mechanical properties such as rebound resilience and hardness of polyurethane to solid particle erosion resistance. However, polyurethane possesses phase mixing at multiple scales and thus sand particle erosion resistance depends also on the microstructure and the …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 13, Issue 1, 2026 · pp. 1–13 Read article
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Characterization Techniques for Thin Film Coatings Based on SiO₂, TiO₂, and ZrO₂
Abstract: Thin film coatings made from silicon dioxide (SiO₂), titanium dioxide (TiO₂) and zirconium dioxide (ZrO₂) have attracted great interest owing to their excellent optical, electrical, mechanical and chemical properties. These oxide thin films are widely used in microelectronics, solar cells, sensors, biomedical devices, photocatalysis, anti-reflective coatings and protective layers. The structural, morphological, compositional, optical and mechanical properties of these coatings are closely related to their performance and reliability. Therefore, thorough …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 Read article
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Experimental Investigation for Strengthening the Nanocomposite Cementitious Materials with a Nanoscale Modification
Abstract: For the last few decades, researchers have widely used nanopolymer to control the mechanical properties of cementitious materials as a micro reinforcement. This paper examines and compares the mechanical and microstructure property of nanofiber cementitious material. Twenty-four sets of beam/cube cast with carbon nanofibers (CNFs) cementitious material where CNFs were used from 0.1%, 0.2%, and 0.3% of cement weight. The nanoparticles were scattered using a surfactant and an ultrasonic probe …
Published in Recent Trends in Civil Engineering & Technology · Vol. 12, Issue 2, 2022 · pp. 10–24 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Synthesis and Characterization of In2S3 Nanoflake Thin Film for Photosensor Applications
Abstract: Indium sulphide (In2S3) thin films in the form of nanoflakes are synthesized by using chemical vapour deposition method on glass substrate with the intension to test its photosensor applications. These as deposited nanoflake thin films are characterized for physicochemical properties using X-ray diffraction (XRD) pattern, energy dispersive X-ray (EDAX) analysis,scanning electron microscopy (SEM) while optoelectronic properties were studied using optical and electrical characteristics obtained through UV-Vis transmission spectroscopy and I-V …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 4, Issue 3, 2017 · pp. 21–26 Read article
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Combustion Synthesis of NiO-YSZ Precursor Nanocomposites for SOFC Anode and Its Characterization
Abstract: In the present work, the mixture of Nickel Oxide-Yttria Stabilized Zirconia (NiO-YSZ) composites of composition, mNiO–(1–m) Zr0⋅9Y0⋅1 O1⋅95 (m = 0⋅4), anode materials was synthesized by combustion process using glycine as fuel and nitrate as oxidizer. The study of prepared nanocomposites has been done by Fourier transform infrared spectroscopy (FTIR), differential thermal analysis-thermo gravimetric analysis (DTA-TGA), X-ray diffraction (XRD) and scanning electron microscopy (SEM) to determine the powder properties. The …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 3, 2012 · pp. 1–9 Read article
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Electrospun Antibacterial Polymer Composite Scaffolds Incorporating Silver Nanoparticles for Enhanced Wound Healing
Abstract: The present study focuses on the synthesis and characterization of electrospun polycaprolactone (PCL)/chitosan nanofiber scaffolds incorporated with silver nanoparticles (AgNPs) to enhance antibacterial activity and biological performance. Uniform nanofibers with controlled morphology were fabricated using electrospinning, and different AgNP concentrations were introduced to investigate their influence on fiber structure, antimicrobial response, and cellular interactions. Scanning electron microscopy (SEM) revealed that increasing AgNP content resulted in well-distributed fibers with reduced diameters, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 1025–1051 Read article
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Effect of machining parameters on the tool wear in drilling of 3D PF C/C composite
Abstract: Carbon–carbon (C/C) composites are broadly used in aerospace, defence, shipbuilding, chemical, and nuclear industries owing to their high strength-to-weight and stiffness-to-weight ratios. However, they are brittle, anisotropic and non-homogeneous in nature, making them difficult to machine. Incorrect machining parameters can cause defects such as burrs, delamination, and fibre bundles pullout. This paper aims to study the hole surface and tool wear during drilling of 3D pierced fabric (PF) carbon-carbon (C/C) …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 269–281 Read article
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Recent Advances in Crystal Defect Engineering of Semiconductor Photocatalysts for Sustainable Environmental and Energy Applications
Abstract: Semiconductor photocatalysis has emerged as one of the most promising green technologies for addressing environmental pollution and global energy challenges through solar energy utilization. Nevertheless, the practical application of conventional semiconductor photocatalysts is often limited by their narrow visible-light absorption, rapid recombination of photogenerated electron–hole pairs, insufficient active sites, and poor charge-transfer efficiency. Defect engineering has recently attracted significant attention as an effective strategy to overcome these limitations by deliberately …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 4, Issue 2, 2026 Read article
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Quantum dots: Properties, Synthesis and Applications
Abstract: AbstractSemiconductor nanocrystal or quantum dots are Nano particles composed of ten to few hundreds of atoms but confined in a very small region. These are zero dimensional materials and are gaining attention to the researchers because of their interesting optical, electronic and opto-electronic properties compared to bulk. Quantum mechanical confinement plays a key role in determining the peculiar behaviour compared to bulk. Various preparation methods such as chemical, colloidal synthesis, …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 1, 2020 · pp. 1–4 Read article
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Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
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Synthesis and Characterization of Sustainable, Low-Cost, Biomass-Derived Carbon Films from Hevea Brasiliensis (Rubber) Wood for Environmentally Friendly Gas Sensors with Enhanced Selectivity and Sensitivity to Polar Vapors and Hazardous Gases
Abstract: Hevea brasiliensis (rubber) wood sawdust was utilized to fabricate carbon gas sensors for detecting 1000 ppm of ethanol, methanol, acetone, carbon dioxide, and ammonia gases. The carbon particles were prepared by phosphoric acid impregnation followed by thermal activation and then fabricated into films on conductive and non-conductive substrates using the doctor blade method. X-ray diffraction (XRD) analysis revealed distinct graphitic features with peaks at the (002) and (100) planes, indicating …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 1, 2025 · pp. 22–36 Read article
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Effect of Red Mud Loading on the Thermal and Mechanical Performance of Polypropylene Composites
Abstract: Waste red mud (RM) serves as a low-cost and sustainable filler material in a polypropylene (PP) matrix. This study investigate the effects of different red mud contents on the dynamic mechanical and thermal properties of polypropylene-red mud (RM-PP) composites where red mud levels range from 0% to 40% (based on weight percentage). Fourier Transform Infrared Spectroscopy (FTIR) was conducted for verifying the presence of both polypropylene and red mud in …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 161–169 Read article
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Development of PLLA-based Bio Inks Applicable in the Medical Field
Abstract: Some synthetic polymers, such as Poly (L-lactic acid) (PLLA), are interesting to use in 3D bioprinting because they can have adaptable and resilient mechanical properties that also facilitate bioprinting processes. PLLA is a biocompatible polymer which makes it very interesting for medical applications, it is an aliphatic polyester obtained from α-hydroxy acids in different ways: ring-opening polymerization, and direct polycondensation. The use of one path over the other depends on …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 24, Issue 2, 2022 · pp. 38–46 Read article