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141 articles for “XRD”
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Synthesis of Lawsonia Inermis (Henna) Carbon Supported AgO Nanocomposite, Characterizations and Photocatalytic Activity Studies
Abstract: Synthesis of Carbon supported AgO nanocomposite is reported for first time. Henna carbon was successfully synthesized from henna leaf. Bare AgO and C-AgO nanocomposites are effectively made using precipitation method. The synthesised composites structural, morphological, and optical properties are assessed using FT-IR, XRD, FE-SEM, UV-DRS, and PL techniques. FT-IR analysis proved that specific functional groups of synthesized materials. The uniform distribution of the composites is revealed in the FE-SEM. XRD …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 749–760 Read article
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Synthesis and Study of Photoluminescence properties of Sm3+ activated 7TiO2 + 3Al2O3 + (60-x)B2 O3 +xY+ 5LiCO3 +25SrCO3 Borate Glass for SSL Applications
Abstract: Melt quenching was used to successfully create the raddish orange light-emitting Sm3+activated 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 (X=0.001, 0.002, 0.005, 0.01 and 0.02, Y=Sm3+) borate glass. XRD examination confirmed the phase of the prepared Un-doped and Doped 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 glass. Its PL characteristics under ultraviolet (UV) light (302-468 nm) were later studied. At 602 nm, the excitation was detected, and at 402 nm, the emission. …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 55–60 Read article
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Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article
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Substitution of La3+ in Cu0.5Co0.5 LaxFe2-x O4 (x=0.02, 0.06) spinel ferrites improves the structural and dielectric Properties
Abstract: Nanosized Spinel ferrites with composition Cu0.5Co0.5 LaxFe2-x O4 (x=0.2, 0.6) synthesized by Sol-Gel auto Combustion method. The prepared sample was calcinated at 8000c for 4 hours. The substitution of La3+ effects the structural parameters, which is characterized by X-ray diffraction (XRD). The X-rd analysis shows that the crystallite size is 34.609 nm for 0.02 and 38.994 nm for 0.06 was calculated by using Debye-Scherrer’s formula. dislocation density shows at value …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 45–48 Read article
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Solid acidity of MoO3 synthesized by solution combustion method and acetalization of formaldehyde using it
Abstract: MoO 3 nanoparticles were synthesized via solution combustion approach. Ammonium nitrate was used as oxidant and ammonium molybdate as fuel in combustion reaction. XRD, FTIR and Raman spectroscopy results showed that MoO 3 nanoparticles were successfully synthesized by the solution combustion reaction. The SEM analysis showed that synthesized MoO 3 nanoparticles have rod-like shape with width and thickness of 50-200nm and length of 0.2-1μm, respectively. The XRD pattern and morphology …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 3, 2025 · pp. 01–09 Read article
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Evaluate The Engineering Properties of Low Load-Carrying Capacity of Expansive Soil by Using Magnesium Chloride and Dry Leaf Ash Powder
Abstract: The swell-shrink behavior of expansive soils poses numerous challenges with the substructure and distress in infrastructures such as buildings, pavements, breast walls, etc. The behavior of expanding soil has been carefully examined by geotechnical engineers, who have then put adequate management techniques into place. Present investigation intends to investigate potential benefits of dry leaf ash (DLA) powder and magnesium chloride (MgCl2) to enhance geological characteristics of soil, particularly addressing problems …
Published in Journal of Geotechnical Engineering · Vol. 12, Issue 1, 2025 · pp. 33–45 Read article
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A Sol-Gel Approach for the Fabrication of Zinc Oxide Nanoparticles and Their Nanocomposite with Urea Formaldehyde (UF)
Abstract: In the performed work, zinc oxide nanoparticles were synthesized via the sol-gel method using zinc sulphate as the precursor material. Urea-formaldehyde (UF) resin was employed as a polymer matrix to encapsulate the produced ZnO through an acid-catalyzed polymerization process. This encapsulation aimed to improve the dispersion stability and surface reactivity of ZnO within the polymeric medium. The synthesized materials were subjected to comprehensive characterization using Fourier Transform Infrared Spectroscopy (FT-IR), …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 21–27 Read article
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Growth, Structural and Optical characteristics of Citric Acid Doped Copper Sulphate Single Crystals Polymer Composites Photonic Applications
Abstract: The organic material Citric Acid doped Copper Sulphate single crystals (CACS) was synthesized and single crystal was grown by slow evaporation method. The incorporation of citric acid, an organic compound, introduces polymer-like functional behavior into the crystal matrix, forming an organic-inorganic hybrid composite with enhanced optical and structural characteristics. Single crystal XRD confirmed the triclinic system with unit cell parameters: a = 5.96 Å, b = 6.11 Å, c = …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 482–488 Read article
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Optimization of Direct Ink Writing Process Parameters for Liquid Silicone Rubber/TiO2 Composite Ink
Abstract: The purpose of this research is to develop and optimize the Liquid Silicone Rubber (LSR)/Titanium Dioxide (TiO₂) composite inks in Direct Ink Writing (DIW)-based 3D printing systems. The primary research objective was to use enhancement of mechanical, rheological, and dielectric characteristics of LSR using TiO₂ reinforcement but still retain extrusion stability and dimensional consistency. TiO₂ content (0, 5, 10, and 15 wt%) and catalyst and glycerol ratios were regulated and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 240–259 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 44–60 Read article
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Turning the Properties of Wastes Paper-Derived Cellulose Nanocrystals for Enhanced Erythromycin Adsorption
Abstract: This study explores the modification, characterization, and adsorption performance of waste paper-derived cellulose nanocrystals (CNCs) for the removal of erythromycin from aqueous solutions. CNCs were modified using organic acid, inorganic acid, and base treatments, and their structural changes were evaluated using FTIR, XRD, and BET analysis. FTIR confirmed the introduction of carboxyl and hydroxyl groups in acid-treated CNCs and deprotonation effects in base-treated CNCs. XRD analysis revealed that organic acid …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 1–24 Read article
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Effect of Red Mud Loading on the Thermal and Mechanical Performance of Polypropylene Composites
Abstract: Waste red mud (RM) serves as a low-cost and sustainable filler material in a polypropylene (PP) matrix. This study investigate the effects of different red mud contents on the dynamic mechanical and thermal properties of polypropylene-red mud (RM-PP) composites where red mud levels range from 0% to 40% (based on weight percentage). Fourier Transform Infrared Spectroscopy (FTIR) was conducted for verifying the presence of both polypropylene and red mud in …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 161–169 Read article
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High-Performance Polymer Composite Membranes for Selective Ion Transport in Advanced Energy Conversion Systems
Abstract: The development of high-performance Polymer Composite Membranes (PCM) with enhanced ion transport is essential for Polymer Electrolyte Membrane Fuel Cells (PEMFC). However, low-humidity conditions and filter agglomeration still limit long-term membrane stability. This research designs a functionalized PCM integrating cross-linked Poly (Vinyl Alcohol)/Poly (Ethylene Glycol) (PVA/PEG) matrix with sulfonic acid functional groups and Titanium Dioxide (TiO₂) nanofillers to improve selective ion transport under low-humidity conditions. Two types of PCM were …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 724–736 Read article
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An Optimize Formulation to Synthesis of size Controlled Hydrophobic Starch Acetate Nanoparticles using Box- Behnken Design
Abstract: The best way to improve the overall performance of native starch is by chemical modification. In recent years, hydrophobically modified starch has attracted considerable attention for the design and manufacture of novel nanoparticulate drug delivery carriers. The purpose of this research was to synthesize hydrophobic starch nanoparticles (NPs) and to optimize process factors through the use of response surface methodology (RSM). The corn starch acetate (CSA) NPs was synthesized using …
Published in Journal of Polymer & Composites Read article
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Preparation and Characterization of TiO2 Nanoparticles by Green Method
Abstract: In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 61–67 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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Experimental investigation of thermally grown Indium film’s structural and tribological properties
Abstract: Indium thin film growth found numerous applications, such as cold welding of infrared detectors and readout-integrated circuits (ROIC) to form sensor chips. In film is grown on the Si substrate by thermal evaporation. The XRD results indicated the tetragonal bcc phase in the (101) preferential plane. Scanning electron microscopy (SEM) indicated an uniform, continuous film covering the whole surface. The EDS examination confirmed the pure In film. The atomic force …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 58–66 Read article
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The Impact of Distinct Dopant Elements (Cu and Al) on the Electrochemical Characteristics of MgO Thin Films Formed Using the Electrodeposition Technique
Abstract: By using an aqueous electrodeposition technique, copper (Cu) and aluminum (Al) doped magnesium oxide (MgO) thin films were created. We examined how the dopant elements affected the electrochemical characteristics of MgO thin films deposited on stainless steel (SS) substrates in the current study. We annealed the MgO-based films at 450◦C. The MgO films doped with Cu and Al have been determined by X-ray diffraction (XRD) results. Cyclic voltammetric analyses (CV), …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 1, Issue 2, 2023 · pp. 12–17 Read article
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Green synthesis of Ag-Fe2O3-CuO-PANI nanocomposite and its application as an Apple Vinegar sensor
Abstract: Green synthesis of nanoparticles is inexpensive and environmentally safe, herein we report green approach for the synthesis of Ag, Fe2O3, CuO nanoparticles by using Asparagus Racemosus plant to detect carboxylate vapours. Synthesized Ag, Fe2O3, CuO nanoparticles were taken in 1:1:1 ratio and PANI (polyaniline) was added in ratio 5:1 to form Ag-Fe2O3-CuO–PANI nanocomposite. Synthesized Ag-Fe2O3-CuO-PANI were characterized by XRD, FESEM and FTIR whose size was in the range of 16–60 …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 41–53 Read article
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Advancements in Solubility Enhancement Through Liquisolid Compact Technology: A Comprehensive Review
Abstract: The study examines Liquisolid Compact Technology as an innovative approach for improving the bioavailability and solubility of drugs that are poorly soluble in water. Liquisolid systems, comprising solid carriers and liquid drugs, offer advantages such as improved drug release and bioavailability, reduced manufacturing costs, and controlled drug delivery. The technique involves dissolving or suspending the drug in non-volatile solvents, adding carrier materials, super disintegrants, and coating materials, and then compressing …
Published in Research & Reviews: A Journal of Drug Design & Discovery · Vol. 11, Issue 2, 2024 · pp. 25–34 Read article