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111 articles for “X-ray diffraction”
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Synthesis and Characterization of Sustainable, Low-Cost, Biomass-Derived Carbon Films from Hevea Brasiliensis (Rubber) Wood for Environmentally Friendly Gas Sensors with Enhanced Selectivity and Sensitivity to Polar Vapors and Hazardous Gases
Abstract: Hevea brasiliensis (rubber) wood sawdust was utilized to fabricate carbon gas sensors for detecting 1000 ppm of ethanol, methanol, acetone, carbon dioxide, and ammonia gases. The carbon particles were prepared by phosphoric acid impregnation followed by thermal activation and then fabricated into films on conductive and non-conductive substrates using the doctor blade method. X-ray diffraction (XRD) analysis revealed distinct graphitic features with peaks at the (002) and (100) planes, indicating …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 1, 2025 · pp. 22–36 Read article
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Comparative Evaluation of the Pozzolanic Activity of Artificial Pozzolans: Steel Slag, Fly Ash, and GGBFS
Abstract: Evaluating the pozzolanic activity of specific industrial waste is crucial given the growing demand for cementitious materials. This research aims to expand the possibilities of incorporating pozzolanic waste such as Steel Slag (SS) as additives to cement. SS is a byproduct of the steel production process. A byproduct of the steelmaking process, slags have long been used as aggregates in building materials like concrete and roads. A closed-loop structure and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 341–361 Read article
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Synthesis and Characterization of Forsterite Incorporated HDPE Composites for Microwave Substrate Application
Abstract: High Density Polyethylene (HDPE) combined with dispersed forsterite (Mg₂SiO₄) powder was utilized to fabricate polymer matrix composites (PMCs) aimed at high-frequency microwave substrate applications. Forsterite powders were synthesized using the mixed oxide method, and their phase purity was confirmed by X-ray diffraction (XRD) analysis. The dispersion and morphology of the ceramic filler within the HDPE matrix were examined through Scanning Electron Microscopy (SEM), ensuring a homogeneous distribution essential for optimal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 109–120 Read article
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Exploring the Luminescent Behavior of Dysprosium-Doped Halo-sulphate Compounds
Abstract: In essence, this study aims toward understanding the photo-luminescent properties of Dy³⁺ halogenated sulfates, viz., synthesis, characterization, and luminescent behavior of the materials. Dysprosium ions are introduced into the halo-sulfate matrices to investigate their suitability for solid-state lighting applications. The aim of the study is to explain the mechanisms of the photo luminescence of Dy³⁺ and study the influence of the doping concentration on luminescence efficiency and the thermal stability …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 01–06 Read article
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Synthesis of Thermal Resistant and Transparent Al2O3 Reinforced Epoxy-Based Composite Coatings
Abstract: This study explores the influence of thermal treatment on the structural, optical, and surface wettability characteristics of epoxy-based composite coatings reinforced with 3 wt.% aluminum oxide (Al₂O₃) nanoparticles. The coatings were synthesized via a dip-coating method on carbon fiber substrates and subjected to controlled thermal treatments at 300 °C, 400 °C, and 500 °C to assess their thermal resilience. X-ray diffraction (XRD) analysis confirmed the structural integrity of the composite …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 178–183 Read article
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Preparation of Transparent and Thermal Resistant Zirconia Reinforced Epoxy Based Polymer Matrix Composite Coatings
Abstract: This study investigates the thermal stability, structural characteristics, optical transparency, and surface wettability of epoxy-based composite coatings reinforced with 2 wt.% zirconia (ZrO₂) nanoparticles. The composite coatings were synthesized using a dip-coating technique on carbon fiber substrates and subsequently subjected to thermal treatments at 300 °C, 400 °C, and 500 °C. Structural analysis using X-ray diffraction (XRD) confirmed the amorphous nature of the epoxy matrix with no significant crystallization or …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 171–177 Read article
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Substitution of La3+ in Cu0.5Co0.5 LaxFe2-x O4 (x=0.02, 0.06) spinel ferrites improves the structural and dielectric Properties
Abstract: Nanosized Spinel ferrites with composition Cu0.5Co0.5 LaxFe2-x O4 (x=0.2, 0.6) synthesized by Sol-Gel auto Combustion method. The prepared sample was calcinated at 8000c for 4 hours. The substitution of La3+ effects the structural parameters, which is characterized by X-ray diffraction (XRD). The X-rd analysis shows that the crystallite size is 34.609 nm for 0.02 and 38.994 nm for 0.06 was calculated by using Debye-Scherrer’s formula. dislocation density shows at value …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 45–48 Read article
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Novel Poly (Methyl Cellulose-G-Acrylamide)/Sodium Alginate Based Zeolite 4A Filled Mixed Matrix Membranes for The Separation of Water-Isopropyl Alcohol Mixtures by Pervaporation
Abstract: The Filled blend matrix membranes of (Methyl Cellulose-g-Acryl amide)/Sodium Alginate {(MC-g-AAm)/NaAlg} prepared via solution casting method by in situ incorporation with 4A zeolite particles in 5, 10 and 15 mass % with respect to the weight of (MC-g-AAm)/NaAlg membrane. Several analytical tools such as scanning electron microscope (SEM), atomic force microscope (AFM), Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and thermo-gravimetric analysis (TGA) were …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 131–152 Read article
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Effect of Bi2O3 Content and Sintering Temperature on the Frequency-Dependent Magnetic Properties of Nanosized Barium Hexaferrite
Abstract: The magnetic properties of commercially available nanosized barium hexaferrite (BaFe12O19) are studied. The particles were characterized using X-ray diffraction (XRD), vibrating sample magnetometer (VSM), and high-frequency magnetic measurements. The frequency-dependent magnetic properties viz. complex permeability and loss tangent were analyzed within the 10 MHz to 1 GHz range. Variations in complex magnetic permeability and loss tangent were discussed under varying sintering parameters such as temperature and sintering aid content. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 107–113 Read article
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Facile Synthesis and Characterization of Cd²⁺ Doped NiAl₂O₄ Nanoparticles for Advanced Polymer Composite Integration
Abstract: Ni1-xCdxAl2O4, where 0 ≤ x ≤ 0.5, was successfully synthesized using the chemical co-precipitation technique, a scalable and cost-effective route suitable for composite material applications. X-ray diffraction (XRD) analysis revealed a crystalline cubic spinel structure for the resulting nanoparticles, with determined crystallite sizes ranging from 36 to 12 nm for NiAl2O4 and Cd-doped NiAl2O4. The respective band gaps for the materials were found to be 3.51 and 4.18 eV. Infrared …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 59–72 Read article
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Green Fabrication of Glutaraldehyde-Crosslinked Chitosan/PVA Biocomposite for Heavy Metal Removal from Wastewater
Abstract: Chitosan (CS) and Polyvinyl alcohol (PVA) are polymers that possess biodegradable, biocompatible, and non-toxic properties, making them suitable for wastewater treatment applications. The primary objective of this research is to chemically modify chitosan in a novel manner to enhance its ability to remove hexavalent chromium Cr(VI) from aqueous solutions. In this study, a composite material was synthesized by crosslinking PVA and CS with glutaraldehyde (GA), resulting in the formation of …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 59–83 Read article
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An Experimental Study on Multi-Criteria Parameters Optimization of Process for Al6351/SiC/Gr Metal Matrix Composites Using AHP-TOPSIS Approach
Abstract: This research focuses on optimizing the process parameters of Wire Electrical Discharge Machining (WEDM) for a hybrid Metal Matrix Composite (MMC) comprising Al6351 aluminum alloy reinforced with 4% SiC and 6% graphite (Gr), fabricated via squeeze casting. This technique enables the formation of dense, defect-free composites with uniform reinforcement distribution, enhancing both mechanical properties and structural integrity. Microstructural characterization using Scanning Electron Microscopy (SEM) confirmed the even dispersion and bonding …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 303–319 Read article
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Development and Characterization of Pseudo-Elastic Ternary Cu-Al-Be Shape Memory Alloy and Its Scope as Shape Memory Hybrid Composites
Abstract: This research investigated the potential of the Cu-11.95Al-0.51Be shape memory alloy (SMA) for vibration damping applications. This specific composition of the alloy was selected to ensure the presence of the austenite phase (ß-phase) and to evaluate the pseudo-elastic (SE) behavior. This research explores the design, fabrication, and characterization of a pseudo-elastic ternary alloy. The key parameters examined in this study were the alloy phase and pseudo-elastic behavior. Other important factors, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 370–385 Read article
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Role of Strontium in Structural and Dielectric characterstics of Barium Titanate
Abstract: Ba₀.₇₅Sr₀.₂₅TiO₃ (BST) compound was synthesized through the conventional solid-state reaction methodology, aimed at investigating its structural, microstructural, and dielectric characteristics. The structural characterization was executed employing X-ray diffraction (XRD), and the resultant diffraction patterns were refined utilizing the Rietveld method, which substantiated the establishment of a single-phase perovskite configuration exhibiting tetragonal symmetry and belonging to the P4mm space group. The refined lattice parameters revealed subtle distortions correlating with the substitution …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1157–1163 Read article
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Synthesis of Silver Nanoparticles of Cissus Quandrangularis and It’s Virtual Screening Against Gastric Cancer
Abstract: Gastric cancer, also known as stomach cancer, is the third leading cause of cancer-related deaths globally and remains a major health challenge due to its poor prognosis and high mortality, largely attributed to late-stage diagnosis. In this context, plant-based nanomaterials are gaining momentum for targeted therapeutic applications. Cissus quadrangularis, a medicinal plant native to India from the Vitaceae family, is traditionally used for its diverse healing properties. Its stem, in …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1551–1569 Read article
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Optimization of Direct Ink Writing Process Parameters for Liquid Silicone Rubber/TiO2 Composite Ink
Abstract: The purpose of this research is to develop and optimize the Liquid Silicone Rubber (LSR)/Titanium Dioxide (TiO₂) composite inks in Direct Ink Writing (DIW)-based 3D printing systems. The primary research objective was to use enhancement of mechanical, rheological, and dielectric characteristics of LSR using TiO₂ reinforcement but still retain extrusion stability and dimensional consistency. TiO₂ content (0, 5, 10, and 15 wt%) and catalyst and glycerol ratios were regulated and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 240–259 Read article
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Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
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Exploration of Copper Oxide PVA/PEG Paraffin Polymer Composites for Enhanced Thermal Performance of Nano-Enhanced Phase Change Materials and Their Environmental Impact
Abstract: This study investigates the synthesis, characterization, and application of copper oxide (CuO) nanoparticles integrated into polymer-based paraffin wax composites for advanced thermal management applications. CuO nanoparticles were synthesized using a wet chemical approach and characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and dynamic light scattering (DLS), confirming their crystalline structure, morphology, and nanoscale size distribution. The synthesized nanoparticles were incorporated into polymer-supported phase change …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 156–173 Read article
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Structural Modification of Sugarcane Bagasse using Alkaline, Acid, and Bleaching Pretreatments for Enhanced Yield of Poly (1→4)-β-D-glucopyranose (Cellulose) and Hemicellulose for Utilization as Biocomposites
Abstract: Sugarcane bagasse, a lignocellulosic byproduct generated in substantial quantities by the sugar industry, represents a promising feedstock for the sustainable production of enzymes and bio-based chemicals. Its high (1→4)-β-D-glucopyranose (cellulose) content, abundant availability, and low cost make it an ideal candidate for bioconversion processes. However, the inherent recalcitrance of bagasse, primarily due to its lignin-rich matrix, necessitates effective pretreatment strategies to enhance enzymatic digestibility. This study presents a comparative investigation …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 983–992 Read article
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Fabrication and Analysis of PBAT/Cyperus Rotundus Micro Crystalline Cellulose Biofilms for Food Packaging Applications
Abstract: Global plastic waste crisis has gained an increasing attention and many efforts have been made recently to develop biodegradable polymers as food packaging alternatives. Solution casting is used for fabrication and characterization of reinforced polybutylene adipate-co-terephthalate (PBAT) biofilm with Cyperus rotundus microcrystalline cellulose (CRC). PBAT-CRC biofilms with different CRC loadings (1%, and 2%) had been prepared and their structural, mechanical, thermal and morphological properties of fabricated biofilms were analyzed to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 591–599 Read article