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81 articles for “X-ray Diffraction (XRD)”
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Preparation of Transparent and Thermal Resistant Zirconia Reinforced Epoxy Based Polymer Matrix Composite Coatings
Abstract: This study investigates the thermal stability, structural characteristics, optical transparency, and surface wettability of epoxy-based composite coatings reinforced with 2 wt.% zirconia (ZrO₂) nanoparticles. The composite coatings were synthesized using a dip-coating technique on carbon fiber substrates and subsequently subjected to thermal treatments at 300 °C, 400 °C, and 500 °C. Structural analysis using X-ray diffraction (XRD) confirmed the amorphous nature of the epoxy matrix with no significant crystallization or …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 171–177 Read article
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Substitution of La3+ in Cu0.5Co0.5 LaxFe2-x O4 (x=0.02, 0.06) spinel ferrites improves the structural and dielectric Properties
Abstract: Nanosized Spinel ferrites with composition Cu0.5Co0.5 LaxFe2-x O4 (x=0.2, 0.6) synthesized by Sol-Gel auto Combustion method. The prepared sample was calcinated at 8000c for 4 hours. The substitution of La3+ effects the structural parameters, which is characterized by X-ray diffraction (XRD). The X-rd analysis shows that the crystallite size is 34.609 nm for 0.02 and 38.994 nm for 0.06 was calculated by using Debye-Scherrer’s formula. dislocation density shows at value …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 45–48 Read article
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Effect of Bi2O3 Content and Sintering Temperature on the Frequency-Dependent Magnetic Properties of Nanosized Barium Hexaferrite
Abstract: The magnetic properties of commercially available nanosized barium hexaferrite (BaFe12O19) are studied. The particles were characterized using X-ray diffraction (XRD), vibrating sample magnetometer (VSM), and high-frequency magnetic measurements. The frequency-dependent magnetic properties viz. complex permeability and loss tangent were analyzed within the 10 MHz to 1 GHz range. Variations in complex magnetic permeability and loss tangent were discussed under varying sintering parameters such as temperature and sintering aid content. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 107–113 Read article
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Facile Synthesis and Characterization of Cd²⁺ Doped NiAl₂O₄ Nanoparticles for Advanced Polymer Composite Integration
Abstract: Ni1-xCdxAl2O4, where 0 ≤ x ≤ 0.5, was successfully synthesized using the chemical co-precipitation technique, a scalable and cost-effective route suitable for composite material applications. X-ray diffraction (XRD) analysis revealed a crystalline cubic spinel structure for the resulting nanoparticles, with determined crystallite sizes ranging from 36 to 12 nm for NiAl2O4 and Cd-doped NiAl2O4. The respective band gaps for the materials were found to be 3.51 and 4.18 eV. Infrared …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 59–72 Read article
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Green Fabrication of Glutaraldehyde-Crosslinked Chitosan/PVA Biocomposite for Heavy Metal Removal from Wastewater
Abstract: Chitosan (CS) and Polyvinyl alcohol (PVA) are polymers that possess biodegradable, biocompatible, and non-toxic properties, making them suitable for wastewater treatment applications. The primary objective of this research is to chemically modify chitosan in a novel manner to enhance its ability to remove hexavalent chromium Cr(VI) from aqueous solutions. In this study, a composite material was synthesized by crosslinking PVA and CS with glutaraldehyde (GA), resulting in the formation of …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 59–83 Read article
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An Experimental Study on Multi-Criteria Parameters Optimization of Process for Al6351/SiC/Gr Metal Matrix Composites Using AHP-TOPSIS Approach
Abstract: This research focuses on optimizing the process parameters of Wire Electrical Discharge Machining (WEDM) for a hybrid Metal Matrix Composite (MMC) comprising Al6351 aluminum alloy reinforced with 4% SiC and 6% graphite (Gr), fabricated via squeeze casting. This technique enables the formation of dense, defect-free composites with uniform reinforcement distribution, enhancing both mechanical properties and structural integrity. Microstructural characterization using Scanning Electron Microscopy (SEM) confirmed the even dispersion and bonding …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 303–319 Read article
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Development and Characterization of Pseudo-Elastic Ternary Cu-Al-Be Shape Memory Alloy and Its Scope as Shape Memory Hybrid Composites
Abstract: This research investigated the potential of the Cu-11.95Al-0.51Be shape memory alloy (SMA) for vibration damping applications. This specific composition of the alloy was selected to ensure the presence of the austenite phase (ß-phase) and to evaluate the pseudo-elastic (SE) behavior. This research explores the design, fabrication, and characterization of a pseudo-elastic ternary alloy. The key parameters examined in this study were the alloy phase and pseudo-elastic behavior. Other important factors, …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 370–385 Read article
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Role of Strontium in Structural and Dielectric characterstics of Barium Titanate
Abstract: Ba₀.₇₅Sr₀.₂₅TiO₃ (BST) compound was synthesized through the conventional solid-state reaction methodology, aimed at investigating its structural, microstructural, and dielectric characteristics. The structural characterization was executed employing X-ray diffraction (XRD), and the resultant diffraction patterns were refined utilizing the Rietveld method, which substantiated the establishment of a single-phase perovskite configuration exhibiting tetragonal symmetry and belonging to the P4mm space group. The refined lattice parameters revealed subtle distortions correlating with the substitution …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1157–1163 Read article
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Synthesis of Silver Nanoparticles of Cissus Quandrangularis and It’s Virtual Screening Against Gastric Cancer
Abstract: Gastric cancer, also known as stomach cancer, is the third leading cause of cancer-related deaths globally and remains a major health challenge due to its poor prognosis and high mortality, largely attributed to late-stage diagnosis. In this context, plant-based nanomaterials are gaining momentum for targeted therapeutic applications. Cissus quadrangularis, a medicinal plant native to India from the Vitaceae family, is traditionally used for its diverse healing properties. Its stem, in …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1551–1569 Read article
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Optimization of Direct Ink Writing Process Parameters for Liquid Silicone Rubber/TiO2 Composite Ink
Abstract: The purpose of this research is to develop and optimize the Liquid Silicone Rubber (LSR)/Titanium Dioxide (TiO₂) composite inks in Direct Ink Writing (DIW)-based 3D printing systems. The primary research objective was to use enhancement of mechanical, rheological, and dielectric characteristics of LSR using TiO₂ reinforcement but still retain extrusion stability and dimensional consistency. TiO₂ content (0, 5, 10, and 15 wt%) and catalyst and glycerol ratios were regulated and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 240–259 Read article
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Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
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Exploration of Copper Oxide PVA/PEG Paraffin Polymer Composites for Enhanced Thermal Performance of Nano-Enhanced Phase Change Materials and Their Environmental Impact
Abstract: This study investigates the synthesis, characterization, and application of copper oxide (CuO) nanoparticles integrated into polymer-based paraffin wax composites for advanced thermal management applications. CuO nanoparticles were synthesized using a wet chemical approach and characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and dynamic light scattering (DLS), confirming their crystalline structure, morphology, and nanoscale size distribution. The synthesized nanoparticles were incorporated into polymer-supported phase change …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 156–173 Read article
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Structural Modification of Sugarcane Bagasse using Alkaline, Acid, and Bleaching Pretreatments for Enhanced Yield of Poly (1→4)-β-D-glucopyranose (Cellulose) and Hemicellulose for Utilization as Biocomposites
Abstract: Sugarcane bagasse, a lignocellulosic byproduct generated in substantial quantities by the sugar industry, represents a promising feedstock for the sustainable production of enzymes and bio-based chemicals. Its high (1→4)-β-D-glucopyranose (cellulose) content, abundant availability, and low cost make it an ideal candidate for bioconversion processes. However, the inherent recalcitrance of bagasse, primarily due to its lignin-rich matrix, necessitates effective pretreatment strategies to enhance enzymatic digestibility. This study presents a comparative investigation …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 983–992 Read article
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Fabrication and Analysis of PBAT/Cyperus Rotundus Micro Crystalline Cellulose Biofilms for Food Packaging Applications
Abstract: Global plastic waste crisis has gained an increasing attention and many efforts have been made recently to develop biodegradable polymers as food packaging alternatives. Solution casting is used for fabrication and characterization of reinforced polybutylene adipate-co-terephthalate (PBAT) biofilm with Cyperus rotundus microcrystalline cellulose (CRC). PBAT-CRC biofilms with different CRC loadings (1%, and 2%) had been prepared and their structural, mechanical, thermal and morphological properties of fabricated biofilms were analyzed to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 591–599 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 44–60 Read article
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Synthesis, Characterization and Dielectric Properties of Polymer Materials for Microwave Communication Applications
Abstract: The rapid advancement in wireless communication technologies has necessitated the development of advanced materials with tailored dielectric properties. Polymer materials, because of their flexibility, lightweight nature, and processing ease, are currently being used in initiatives to formulate low-dielectric materials specifically tailored for microwave communication applications. In the current investigation, the authors concentrate on the synthesis, characterization, and dielectric properties of five distinct novel polymer materials. The synthesized polymers are characterized …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1482–1495 Read article
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Activated Carbon Materials as Ideal Adsorbents for the Desulfurization of Fossil Fuels
Abstract: Removal of organosulfur compounds from diesel is of interest from scientific, social, economic, and environmental viewpoints. Production of clean fuel remains a primary goal of the petroleum refining industry. The reduction of sulfur content below stringent ppm levels in diesel fuels becomesincreasingly challenging due to the presence of sterically hindered sulfur compounds, such as 4,6- dialkyldibenzothiophenes, which are resistant to removal over conventional supported mixed sulfide hydrodesulfurization catalysts. Consequently, alternative …
Published in International Journal of Pollution: Prevention & Control · Vol. 4, Issue 1, 2026 · pp. 28–34 Read article
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Structure–Optical Property Correlation of Co-Doped TiO₂ and ZnO Nanofillers for Advanced Functional Composite Applications
Abstract: This study investigates the enhancement of the structural and optical properties of titanium dioxide (TiO₂) and zinc oxide (ZnO) nanoparticles through cobalt (Co) doping. Pristine TiO₂ and ZnO are widely studied metal oxides; however, their large band gaps and limited visible-light absorption restrict their performance in optoelectronic, photocatalytic, and environmental applications. Co doping is employed as an effective strategy to overcome these limitations by inducing band-gap narrowing, creating defect-related electronic …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1374–1394 Read article
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Spin Coated Polyvinylidene Difluoride / Ionic Liquid Nanocomposite Thin Films with Enhanced Dielectric and Piezoelectric Properties
Abstract: This study introduces a novel approach to enhance the piezoelectric and dielectric properties of polyvinylidene difluoride (PVDF) by incorporating 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIM][BF₄]) ionic liquid via a spin-coating method— a processing route that has been rarely reported for PVDF/ionic liquid composites. Structural and morphological analyses using X-ray diffraction (XRD), Raman spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) confirm the successful integration of [BMIM][BF₄] into the PVDF matrix. The …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1190–1204 Read article
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Utilization of Treated Textile Dyeing Wastewater and GGBFS–Perlite Blends for Sustainable Cementitious Composite Development
Abstract: The increasing global demand for concrete critically intensifies the consumption of potable water, raising significant environmental concerns and depleting vital resources. Concurrently, the textile dyeing industry generates substantial volumes of wastewater, posing considerable disposal and pollution challenges. Our investigation explores a dual solution by utilizing treated textile dyeing wastewater as an alternative mixing water source, combined with ground granulated blast furnace slag (GGBFS) and perlite as supplementary cementitious materials (SCMs), …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 291–300 Read article