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111 articles for “X-ray diffraction”
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Synthesis and Applications of Copper- Doped Pyridine Precipitate
Abstract: A metal organic nonlinear optical single crystal, copper doped pyridine material, was created at room temperature using the slow evaporation solution growth technique (SEST). The developed material's crystalline nature was revealed by a powder X-ray diffraction (XRD) analysis. Single crystal XRD study shows that the material synthesized possesses monoclinic system of cell parameters, a = 11.44 Å, b = 7.92 Å, C = 11.74 Å and alpha and gamma is …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 1, 2025 · pp. 51–60 Read article
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Application of Sensor Effect on Chlorodiazepam of Polyaniline Doped Silver Nanocomposite
Abstract: In order to ease the creation of the polymeric nanocomposite known as PANI/Ag, pani-doped silver nanoparticles were oxidised chemically and then exposed to the oxidation process. Aniline with varying amounts of silver nanoparticles added to it can be used to make a nanocomposite known as PANI/Ag in an acid solution at room temperature by employing ammonium persulfate as the oxidising agent. This can be done by using aniline with different …
Published in Journal of Polymer & Composites Read article
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Preparation and Characterization of TiO2 Nanoparticles by Green Method
Abstract: In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 61–67 Read article
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Evaluation of Inhibition Effect of Nanohybrid Curcumin (Cur-ZnO) and Cur-free Against Some Types of Bacteria
Abstract: This study aimed to prepare an efficient nanohybrid food preservative by loading curcumin on zinc oxide. The prepared compound was characterized using microscopy and spectral methods. Fourier transform infrared spectrum of the nanohybrid curcumin showed a shift in the frequencies of some chemical groups towards high and low frequencies. X-ray diffraction (XRS) spectrum also revealed the emergence of new diffraction planes in the nanohybrid compound, Compared with the carrier spectrum …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 68–79 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
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The Impact of Distinct Dopant Elements (Cu and Al) on the Electrochemical Characteristics of MgO Thin Films Formed Using the Electrodeposition Technique
Abstract: By using an aqueous electrodeposition technique, copper (Cu) and aluminum (Al) doped magnesium oxide (MgO) thin films were created. We examined how the dopant elements affected the electrochemical characteristics of MgO thin films deposited on stainless steel (SS) substrates in the current study. We annealed the MgO-based films at 450◦C. The MgO films doped with Cu and Al have been determined by X-ray diffraction (XRD) results. Cyclic voltammetric analyses (CV), …
Published in International Journal of Electro-Mechanics and Material Behaviour · Vol. 1, Issue 2, 2023 · pp. 12–17 Read article
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Synthesis and Functional Group Analysis of Solution Processed Zinc Oxide Thin Film Grown on Polyethylene Terephthalate
Abstract: Flexible electronics field is growing every day. Existing technology is facing issues like brittleness, toxicity, inadequacy. Fabrication cost increases in processing of such materials. In this work, zinc oxide nanoparticles synthesized by solution processing technique were used to grow 120nm thick thin film (TF) on Polyethylene terephthalate (PET). This method reduces the processing cost and Zinc Oxide (ZnO) is cheaper and abundant in comparison to other semiconductors option. Material was …
Published in Journal of Polymer & Composites · Vol. 12, Issue 3, 2024 · pp. 56–66 Read article
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Properties of ZnO Thin Film deposited on Flexible Substrate using RF Sputtering
Abstract: Semiconductor materials demand is increased in recent years, due to new emerging technologies. There is need to find the alternate for silicon in electronics industry, as silicon is brittle in nature and has low efficiency, which makes it unsuitable for transparent and flexible device. Zinc oxide (ZnO) is emerging as popular choice of researchers due to its wide range of properties, abundancy and non-toxicity. This work explores the properties of …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 50–56 Read article
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SYNTHESIS AND CHARACTERIZATION OF Mn2+ DOPED LiPbX3(X = Cl, Br, I)
Abstract: In this paper the structural, electronic and optical properties of Mn doped Pb based cubic perovskites LiPbX3(X= Cl, Br and I) were studied by wet chemical method (sol gel method). For Mn doped LiPbX3(X= Cl, Br and I) NCs, MnCl2 and PbBr2 were added in molar feed ratio 1.35 mole% and nan crystal were examine with the help of TEM and their structure were confirmed by X-ray diffraction (XRD). Additionally, …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 48–54 Read article
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Enhanced Synthesis Methods and Comprehensive Material Response Analysis in Alloy-Infused Nanocomposites
Abstract: This study looks into the most advanced ways to make alloy-infused nanocomposites and how they react to different materials. It focuses on how these nanocomposites can be used to process and make plastics and composites. A lot of people are interested in alloy-infused nanocomposites because they have better mechanical, thermal, and electrical qualities than regular composites. The goal of this study is to improve the methods used for making nanocomposites …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 175–191 Read article
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Zn Doped CuO Nanoparticles for Increasing the Longevity of The Agricultural Products †
Abstract: Nanotechnology is an enabling technology at the service of mankind. Indeed, enhancing the long-term storage of agricultural products (post-harvest during transportation and storage) in general and apples and tomatoes, in particular, is a challenge. Zn-doped CuO is a proven nanomaterial with special ability to kill plant pathogens as well as a variety of microorganisms (bacteria, virus, and fungus). Much of the review is focused on the landmark papers published by …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 1, 2024 · pp. 14–29 Read article
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Characterization Of Senna Occidentalis (Link.) Seed Extract
Abstract: Senna occidentalis (L.) Link commonly known as "coffee senna" or majamfari/rai dore in Hausa is a plant with a long history of traditional and medicinal uses against diseases such as inflammation, pains, and diabetes. This study presents characterization of the bioactive compounds of the seed extracts. Physicochemical analysis of seed powder was carried out following standard procedures. Qualitative phyto-chemical contents were determined for the presence and absence of major metabolites. …
Published in Research & Reviews : Journal of Botany · Vol. 13, Issue 3, 2024 · pp. 13–22 Read article
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Innovative Porcelain Insulators: Prolonged Durability and Anti-Contamination Efficiency via Nano-TiO2 Photocatalyst Integration
Abstract: Porcelain has long been a critical material in high-voltage electrical insulation due to its exceptional mechanical, thermal, and dielectric properties. However, environmental contamination and material degradation over time pose significant challenges to its durability. This study investigates the integration of nano-sized titanium dioxide (TiO2) photocatalyst coatings on porcelain insulators to enhance their performance and prolong their operational lifespan. Local clay compositions were analyzed, and a comparative study of untreated and …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 2, 2024 · pp. 18–23 Read article
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Development of Biomass-Derived Composites From Commodity Plastics Via Pyrolysis For Enhanced Corrosion Protection of Metals
Abstract: Escalating environmental concerns and the depletion of fossil resources have spurred the need for sustainable and eco-friendly materials. By converting plastic waste into valuable carbonaceous materials via pyrolysis, both plastic pollution and resource scarcity can be addressed. The process involves the thermal decomposition of plastics in an inert atmosphere, producing a mixture of gases, liquids, and solid residues rich in carbon. These carbonaceous residues are then incorporated with biomass materials …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 59–70 Read article
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Structural and Optical Properties of Nanocomposites of Polyethylene Oxide Embedded with Nano-ZNO
Abstract: Polymer nanocomposites have attracted significant attention in recent years owing to their unique properties and potential applications in a variety of fields. In this study, PEO-ZnO nanocomposites were prepared with different wt.% (5, 10 and 15) nano-ZnO particles incorporated into PEO matrix by a solution casting method. Structural and Optical properties of PEO-ZnO nanocomposites were studied. X-ray diffraction (XRD) studies suggest the incorporation of ZnO NPs into PEO matrix. The …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 586–600 Read article
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Synthesis and Study of Photoluminescence properties of Sm3+ activated 7TiO2 + 3Al2O3 + (60-x)B2 O3 +xY+ 5LiCO3 +25SrCO3 Borate Glass for SSL Applications
Abstract: Melt quenching was used to successfully create the raddish orange light-emitting Sm3+activated 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 (X=0.001, 0.002, 0.005, 0.01 and 0.02, Y=Sm3+) borate glass. XRD examination confirmed the phase of the prepared Un-doped and Doped 7TiO2 + 3Al2O3+ (60-x) B2O3+xY+ 5LiCO3+25SrCO3 glass. Its PL characteristics under ultraviolet (UV) light (302-468 nm) were later studied. At 602 nm, the excitation was detected, and at 402 nm, the emission. …
Published in Journal of Polymer & Composites · Vol. 12, Issue 6, 2024 · pp. 55–60 Read article
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Sustainable Innovations in Green Nanotechnology for Nanoparticle Synthesis
Abstract: Green nanotechnology is an emerging field that focuses on the environmentally friendly production of nanoparticles through biological and sustainable processes. This approach has diverse applications across industries such as pharmaceuticals, energy, electronics, and bioengineering. Compared to conventional methods, biologically driven nanoparticle synthesis, particularly utilizing green chemistry principles, offers a safer, eco- friendly, non-toxic, and cost-effective alternative. Metal nanoparticles are commonly synthesized through top-down and bottom-up strategies using physical, chemical, and …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 1, 2025 · pp. 31–37 Read article
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Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article