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86 articles for “transmission electron microscope”
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Principles and Use of Analytical Transmission Electron Microscope
Abstract: At the beginning of the review the analytical Transmission Electron Microscope is introduced. Equipment, imaging, diffraction and use of analytical TEM are described. Electron path under magnetic lens is delineated, emphasizing the lens aberrations, diffraction, astigmatism and gun brightness. Selected area electron diffraction patterns of Al-Cu and Inconel super alloy are used to index crystallographic planes and to derive zone direction while basic sources of diffraction contrast are depicted using …
Published in Journal of Materials & Metallurgical Engineering · Vol. 9, Issue 3, 2019 · pp. 27–49 Read article
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Synthesis and Characterization of Amorphous Carbon Nanotube-Molybdenum Disulfide (ACNT-MoS2) Nanohybrids using Sodium Molybdate Dehydrate and L-Cysteine as Precursor
Abstract: The discovery of graphene makes the researcher interested towards the other two-dimensional material which has quite similar properties like graphene. Among them, MoS2 nanosheets haves extraordinary optoelectronic and physical properties. It has several applications in developing battery, sensor, optoelectronic device etc. On the other hand, amorphous carbon nanotube can be synthesized by using a low temperature chemical process. Due to the ease processing of amorphous carbon nanotube (ACNT), good optoelectronic …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 3, 2019 · pp. 41–47 Read article
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Synthesis of Homogenous Colloidal Silver Nanoparticles
Abstract: Normal 0 false false false EN-US X-NONE X-NONE MicrosoftInternetExplorer4 Silver nanoparticles have potential applications in various fields such as biology, medicine, electronics and optical components. Suitability for these applications depends on the size, shape and chemical composition of the nanoparticles. The method of synthesis plays an important role in determining many of these properties. In this study, the formation of silver nanoparticles has been studied via the chemical reduction of …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 2, 2011 · pp. 59–66 Read article
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HRTEM and Current-Voltage Study of ACNT-MoS2 Nanocomposite Prepared by Hydrothermal Method
Abstract: Recently amorphous carbon nanotube and their nanocomposites are most influenced research topic in the field of nanoscience and nanotechnology. Here in this paper, amorphous carbon nanotube-molybdenum disulfide nanocomposite has been prepared by hydrothermal method. Hexaammonium heptamolybdate tetrahydrate, thiourea and amorphous carbon nanotube were used as main material in that process. Amorphous carbon nanotube have been prepared separately by a low temperature chemical process. Finally the high resolution transmission electron microscope …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 3, 2019 · pp. 15–21 Read article
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Microstructural Design and Functional Properties of Polycrystalline Materials
Abstract: Polycrystalline materials, composed of an aggregate of crystallites or grains, are foundational to modern engineering applications due to their versatile functional properties. The microstructural design—encompassing grain size, shape, orientation, phase distribution, and grain boundary characteristics—plays a pivotal role in determining mechanical, thermal, electrical, and magnetic behavior. This abstract explores the intricate relationship between microstructure and functionality, emphasizing how tailored processing techniques such as thermomechanical treatments, sintering, and additive manufacturing can …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 16–20 Read article
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Synthesis, characterization, and antibacterial activity of silver nanoparticles with expired minocycline as reducing agent: proposed as a recycling technique.
Abstract: In this research, expired minocycline, a broad-spectrum tetracycline antibiotic, was employed as both a reducing and stabilizing agent for the eco-friendly synthesis of silver nanoparticles. This sustainable method avoids the use of toxic chemical reducing agents, providing a greener alternative for nanoparticle production. The synthesized silver nanoparticles were analyzed using several characterization techniques, such as UV-Vis’s spectroscopy, scanning electron microscopy, transmission electron microscopy, and Edex analysis, to assess their structural, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 1, 2026 · pp. 30–43 Read article
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Quantum dots: Properties, Synthesis and Applications
Abstract: AbstractSemiconductor nanocrystal or quantum dots are Nano particles composed of ten to few hundreds of atoms but confined in a very small region. These are zero dimensional materials and are gaining attention to the researchers because of their interesting optical, electronic and opto-electronic properties compared to bulk. Quantum mechanical confinement plays a key role in determining the peculiar behaviour compared to bulk. Various preparation methods such as chemical, colloidal synthesis, …
Published in Research & Reviews : Journal of Physics · Vol. 9, Issue 1, 2020 · pp. 1–4 Read article
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Processing and Characterization of Ni2MnSn FSMA
Abstract: Among Ferromagnetic Shape Memory alloys (FSMAs), Ni2MnSn Heusler alloys owing to occurrence of large magnetic field induced strain (> 10%) along with other interesting properties like premartensitic transition, high transformation temperature, large magnetocaloric effect and low stress of twin variant rearrangement. The prominent challenges facing the design and utilization of these specialized alloys are a limited range of operating temperatures, phase transformations that have high sensitivity to variations in composition, …
Published in Journal of Materials & Metallurgical Engineering · Vol. 2, Issue 1-3, 2012 · pp. 154–159 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article
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Biosynthesis, Characterization and Non-toxic Activity of Gold Nanoparticles using Geranium (Pelargonium graveolens L.) Leaf Extract
Abstract: Nanoparticles from various materials can be prepared by relatively simple methods. During the past few decades, a variety of different methods have been reported and reviewed for synthesizing gold colloids of monodisperse and uniform sized particles. In present investigation, a new method of one-pot biosynthesizing of gold nanoparticles (GNPs), using geranium leaves extract as a reductant and stabilizer is reported. GNPs were characterized by UV-visible spectroscopy; transmission electron microscopy, X-ray …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 16, Issue 3, 2014 · pp. 1–7 Read article
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Enhanced Synthesis Methods and Comprehensive Material Response Analysis in Alloy-Infused Nanocomposites
Abstract: This study looks into the most advanced ways to make alloy-infused nanocomposites and how they react to different materials. It focuses on how these nanocomposites can be used to process and make plastics and composites. A lot of people are interested in alloy-infused nanocomposites because they have better mechanical, thermal, and electrical qualities than regular composites. The goal of this study is to improve the methods used for making nanocomposites …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 175–191 Read article
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Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
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Synthesis of Magnetically Recoverable Nickel (II) Complex-Functionalized Fe3O4@ISNA (ISNA= Isonicotinic acid) Nanomaterials: Catalytic Studies on Nitrophenol Reduction and TD- DFT Studies
Abstract: In this study, we aimed to develop a novel, environmentally sustainable, and magnetically separable heterogeneous nanocatalyst, denoted as Fe3O4@ISNA@NiL (where L represents the ligand). The synthesis involved a two-step process, first, isonicotinic acid was chemically grafted onto the surface of iron oxide nanoparticles (Fe3O4) to introduce functional groups capable of further chemical modification. Subsequently, a nickel(II) Schiff base monomeric complex was anchored onto the modified surface, resulting in a nanocatalyst …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 88–96 Read article
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Synthesis of Magnetically Recoverable Nickel (II) Complex-Functionalized Fe 3 O 4 @ISNA (ISNA= Isonicotinic acid) Nanomaterials: Catalytic Studies on Nitrophenol Reduction and TD- DFT Studies
Abstract: In this study, we aimed to develop a novel, environmentally sustainable, and magnetically separable heterogeneous nanocatalyst, denoted as Fe 3 O 4 @ISNA@NiL (where L represents the ligand). The synthesis involved a two-step process, first, isonicotinic acid was chemically grafted onto the surface of iron oxide nanoparticles (Fe 3 O 4 ) to introduce functional groups capable of further chemical modification. Subsequently, a nickel(II) Schiff base monomeric complex was anchored …
Published in Journal of Polymer & Composites · Vol. 12, Issue 9, 2024 Read article
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Synthesis and Photoluminescence Dynamics of Europium (III) and Terbium (III) Co-doped of GdSrAl3O7 Color-Tunable Nanophosphors
Abstract: A series of Europium (III) and Terbium (III) co-doped GdSrAl3O7 color-tunable nanophosphors were synthesized by a simplistic, streamlined and self-propagating, urea-assisted solution combustion synthesis process. The structural and luminescence characteristics of synthesized Eu3+/Tb3+ co-doped Gadolinium Strontium Aluminate nanocrystalline phosphors were validated using powder X- ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X- ray analysis (EDAX), and photoluminescence spectra studies. The morphological studies revealed that …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1069–1082 Read article
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Sustainable Innovations in Green Nanotechnology for Nanoparticle Synthesis
Abstract: Green nanotechnology is an emerging field that focuses on the environmentally friendly production of nanoparticles through biological and sustainable processes. This approach has diverse applications across industries such as pharmaceuticals, energy, electronics, and bioengineering. Compared to conventional methods, biologically driven nanoparticle synthesis, particularly utilizing green chemistry principles, offers a safer, eco- friendly, non-toxic, and cost-effective alternative. Metal nanoparticles are commonly synthesized through top-down and bottom-up strategies using physical, chemical, and …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 1, 2025 · pp. 31–37 Read article
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Exploration of Copper Oxide PVA/PEG Paraffin Polymer Composites for Enhanced Thermal Performance of Nano-Enhanced Phase Change Materials and Their Environmental Impact
Abstract: This study investigates the synthesis, characterization, and application of copper oxide (CuO) nanoparticles integrated into polymer-based paraffin wax composites for advanced thermal management applications. CuO nanoparticles were synthesized using a wet chemical approach and characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and dynamic light scattering (DLS), confirming their crystalline structure, morphology, and nanoscale size distribution. The synthesized nanoparticles were incorporated into polymer-supported phase change …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 156–173 Read article
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Tailoring The Electrochemical Interface of Graphene–Gd₂O₃ Nanocomposites for Advanced Energy Storage
Abstract: Graphene–Gd₂O₃ nanocomposites were synthesized by incorporating varying concentrations of reduced graphene oxide (rGO) into Gd₂O₃ using a straightforward room-temperature solution method. The composites were analyzed using various distinct characterization techniques, including X-ray diffraction (XRD), Fourier-transform infrared (FTIR) spectroscopy, Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). Electrochemical measurements, particularly cyclic voltammetry (CV), demonstrated that the incorporation of graphene significantly enhanced the electrochemical performance …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 369–388 Read article
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Semiconducting Materials for Emerging Electronics and Technological Applications
Abstract: Semiconducting materials are important for emerging electronic and photovoltaic technologies because their structural, optical and electrical properties can be tailored for specific device applications. In this study, a TiO₂-based composite photoanode is considered as a polymer-assisted semiconducting thin-film system in which inorganic TiO₂ nanoparticles are processed with organic film-forming components to produce a porous layer for dye-sensitised solar cell application. Nanocrystalline TiO₂ nanoparticles were synthesised from titanium isopropoxide using a …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 36–50 Read article
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Crystalline Materials: From Crystal Growth and Defect Engineering to Advanced Functional Applications
Abstract: Crystalline materials form the foundation of numerous modern technologies owing to their highly ordered atomic structures and exceptional physical, chemical, electrical, optical, and mechanical properties. Their periodic crystal lattices provide superior structural stability and enable precise control of electronic, thermal, and optical behavior, making them indispensable in microelectronics, photonics, energy storage, catalysis, aerospace, environmental remediation, and biomedical engineering. Rapid advances in crystal growth techniques, nanotechnology, and computational materials science have …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 2, 2026 · pp. 23–31 Read article