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32 articles for “field-emission scanning electron microscope”
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Synthesis and Characterization of Amorphous Carbon Nanotube-Molybdenum Disulfide (ACNT-MoS2) Nanohybrids using Sodium Molybdate Dehydrate and L-Cysteine as Precursor
Abstract: The discovery of graphene makes the researcher interested towards the other two-dimensional material which has quite similar properties like graphene. Among them, MoS2 nanosheets haves extraordinary optoelectronic and physical properties. It has several applications in developing battery, sensor, optoelectronic device etc. On the other hand, amorphous carbon nanotube can be synthesized by using a low temperature chemical process. Due to the ease processing of amorphous carbon nanotube (ACNT), good optoelectronic …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 3, 2019 · pp. 41–47 Read article
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Efficient Green Synthesis of TiO2 Nanoparticles Using Murraya koenigii Leaf Extract
Abstract: Green synthesis of nanoparticles by plant extract is at present under exploitation due to eco-friendly, non-toxic and inexpensive process. Titanium dioxide (TiO2) nanoparticles were synthesized by ultrasound assisted sol-gel precipitation method using titanium tetra-isopropoxide as a precursor and Murraya koenigii leaf extract as a reducing and stabilizing agent. The leaf extract was prepared under various solvent media such as ethanol and distilled water under controlled ultrasonication. Due to effective ultrasound, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 6, Issue 1, 2016 · pp. 29–38 Read article
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Performance Evaluation of Green Walnut Husk Waste Extract for Inhibiting Aluminium 8088 Corrosion in Acidic Solution
Abstract: The cumulative call for environmental and supportable corrosion inhibitors has obsessed curiosity in exploiting plant-based agronomic surplus resources. Presented research work discovers the corrosion inhibition probable of green walnut husk extract(GWH)—a normal and plentiful agro-waste—on Aluminium 8088 alloy in an acidic medium. Aluminium 8088, however identified for its corrosion resistance, is vulnerable to squalor in highly acidic settings, affectation trials in several industrial claims. GWH extract act as an ecologically …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 45–59 Read article
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Development and Comparative Study of Aluminium- Copper Metal Based Composite Through Different Routes
Abstract: The aim of this study is to develop aluminium-copper composite through powder metallurgy technique. Powder metallurgy is an art or technology which can produce exact dimension of final roducts utilizing less energy. Copper oxide (CuO) was used as the source of copper, which was extracted through a reduction process using dextrose. The reaction was thoroughly examined and reported. Commercially available aluminium powder served as source of the aluminium. Aluminium- copper …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 19–32 Read article
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Fabrication and Characterization of Copper Nanowires: An Overview
Abstract: Copper (Cu) is one of the most important metals in modern electronic technology. Keeping in view its role in nanoelectronics, we have fabricated copper nanowires of diameters 100 and 200 nm using Anodic Alumina and polymer membranes as templates. Template-based growth of copper nanowires has been realized using conventional electro deposition technique in an electrochemical cell designed in our laboratory. Fabrication of copper nanowires is one of the most important …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 1, 2011 Read article
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Synthesis of Metallic Copper Nanoflowers, Nanocrystals and Nanorods using Electrodeposition and Hydrothermal Techniques
Abstract: Copper nanoflowers and nanocrystals have been fabricated using two different techniques; electro-deposition of copper in polymer and anodic alumina templates (AAT) and Cetyltrimethyl-ammonium Bromide (CTAB)-assisted hydrothermal method. Nanorods of copper are produced by electrodeposition in 100 nm AAT. Scanning Electron Microscope (SEM) micrographs record some interesting morphologies of metallic copper nanoflowers and nanocrystals. Field Emission Scanning Electron Microscope (FESEM) has been used to determine morphology and chemical composition of polycrystalline …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 1, 2012 Read article
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Amorphous Carbon Nanotube (ACNT), Two-dimensional Molybdenum Disulfide Nanosheets (MoS2) and Amorphous Carbon Nanotube-MoS2 Nanohybrids: A Brief Theoretical and Practical Analysis
Abstract: Recently, carbon nanotube and MoS2 nanosheets have been showing great interest in the field of nanoscience and nanotechnology for its exceptional physical, optical and electronic properties. The synthesis procedure of crystalline carbon nanotube is immensely tough for which researchers are focused on amorphous carbon nanotube. Single layer MoS2 with direct band gap shows better semiconductor behavior such as photoluminescence, makes them more acceptable in optoelectronic applications in comparison with graphene, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 3, 2019 · pp. 1–13 Read article
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A New Approach of Synthesis Fe-Substituted Bi-2223 Superconductors
Abstract: Generally, the Bismuth based high temperature superconductors are utilizing in three phases as Bi-2201, Bi-2212 and Bi-2223. These have different transition temperature according to superconducting phase. Here, we studied about Bi-2223 phase by using complex Bi2Sr2Can-1 (Cu1-xFex)3O10+δ where n = 3. In this complex, we has been doped iron in Coper (Cu) site (x = 0.07%). This sample was prepared by solid state reaction method. The planetary Ball mill was …
Published in Research & Reviews : Journal of Physics · Vol. 10, Issue 3, 2021 · pp. 22–29 Read article
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Influence of Crystallization Time by Hydrothermal Synthesis of Ag NPs-Zeolite Composite
Abstract: The nanocomposites Ag NPs-zeolite involve zeolite loaded with silver nanoparticles and have been prepared by an easy one-pot hydrothermal autoclave method. Three samples of silver-bearing zeolite were prepared for 8 hours, 6 hours, and 4 hours, respectively, inside an autoclave at 100°C. A range of characterization procedures were used to examine the samples, such as x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV-visible spectroscopy, and zeta potential. Results …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 80–90 Read article
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Hydrothermal modification of carbon fiber fabrics by ZnO nanorods for mechanical strengthening of CFRP laminates
Abstract: Hexagonal ZnO nanorods were produced on plain woven carbon fiber using a two-step seed-assisted hydrothermal procedure. By varying the process parameters such as molar concentrations, number of seeding cycles, and growth duration at a controlled growth temperature of 90 °C, it is feasible to produce ZnO nanostructures with a range of morphologies, including nanowires, hexagonal nanorods, and nanoflowers. The developed morphologies were examined using field emission scanning electron microscopy and …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 127–139 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts: Properties and Applications
Abstract: The main study and the development of CeO2 and Cu-doped CeO2 nanocrystals containing transition- metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu-doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. The structural properties of Ce1-xCuxO2 nanocrystals were examined by investigating the influence of cerium dioxide and Cu dopant ions. The CeO2 single-phase cubic system was successfully incorporated with Cu …
Published in Journal of Catalyst & Catalysis · Vol. 11, Issue 3, 2024 · pp. 29–38 Read article
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Process Parameters Optimization of Fiber Laser Cladded SS316 Surface Using RSM Analysis
Abstract: This paper presents the laser cladding experiments on the surface of SS316 to study the variations in process parameters, such as scanning speed (100-250 mm/min), laser power (50-250 W), and % volume of B4C (5- 25%) + SS316 powder on the mechanical, metallurgical and tribological performance of the modified surface. A central composite design (CCD) was used to develop the response surface methodology (RSM) to design the experiments and for …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 186–201 Read article
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Enhancing Delamination Resistance in CFRP Composites through surface Functionalization of Woven carbon Fiber by CuO Nanostructures
Abstract: In order to produce a nanostructured interphase that improves the interfacial interaction with an epoxy resin matrix, copper oxide (CuO) nanostructures were hydrothermally formed onto woven carbon fibers (WCF). Hexagonal CuO nanorods were created using a two-step, seed-assisted solvothermal technique on plain woven carbon fiber. This study investigates the effects of surface modification of carbon fibers by the formation of CuO nanostructures using a hydrothermal technique on the mechanical properties …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 589–602 Read article
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Green Fabrication of Glutaraldehyde-Crosslinked Chitosan/PVA Biocomposite for Heavy Metal Removal from Wastewater
Abstract: Chitosan (CS) and Polyvinyl alcohol (PVA) are polymers that possess biodegradable, biocompatible, and non-toxic properties, making them suitable for wastewater treatment applications. The primary objective of this research is to chemically modify chitosan in a novel manner to enhance its ability to remove hexavalent chromium Cr(VI) from aqueous solutions. In this study, a composite material was synthesized by crosslinking PVA and CS with glutaraldehyde (GA), resulting in the formation of …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 59–83 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Comparative Study of Structural and Optical Properties of Bismuth Ferrite Nanoparticles for Photovoltaic Applications Synthesized via Different Sol-Gel Methods
Abstract: Pure multiferroic bismuth ferrite (BiFeO3) nanoparticles were successfully synthesized using an energy-efficient, low-temperature sol-gel method, comparing two distinct approaches: auto-combustion and non-auto-combustion. To ensure phase stability, the precursor solution's pH was strictly maintained between 1 and 2 using ammonia solution (NH4OH), while ethylene glycol (C2H6O2) was employed as a chelating agent for the Fe3+ and Bi3+ cations. All samples underwent a final annealing process at 500 °C to promote crystallization. …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 83–94 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis Read article
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Synthesis, Characterization and Drug Delivery Application of Poly (Acid Fuchsin) Based Triblock Copolymer
Abstract: Synthesis, characterization and its drug delivery application of Poly (acid fuchsin) (PAF) was done under inert atmosphere. The (M0/I0) was maintained at 100. In order to increase the molecular weight and processability, it was block copolymerized with ε-caprolactone (CL) and tetrahydrofuran (THF) separately. The conductivity value of PAF was found to be decreased after the chemical conjugation with poly(ε-caprolctone) (PCL) and poly(tetrahydrofuran) (PTHF) blocks. Thus obtained triblock copolymer was subjected …
Published in Journal of Catalyst & Catalysis · Vol. 3, Issue 2, 2016 · pp. 33–43 Read article
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Nanostructured Cr-WS2 Solid Lubricant Coating for Space Applications
Abstract: Abstract Tungsten disulphide (WS2) is one of the widely used intrinsic low friction materials, which is commonly used in the form of coating. WS2 offers very low coefficient of friction only in non humid conditions. Presence of humidity destroys this property and restricts its utility. Modifying the structure of WS2 by adding certain metals helps in overcoming this limitation and in addition improves the mechanical properties. Further, deposition technique and …
Published in Journal of Instrumentation Technology & Innovations · Vol. 9, Issue 1, 2019 · pp. 12–18 Read article
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Improving Photocatalytic and Antibacterial Properties of Zein/Polyvinyl Alcohol Polymer Composite Film by Dispersing TiO2 Nano Particles
Abstract: Zein/polyvinyl alcohol/nano-TiO2 composite film was effectively blended using a solution casting method. Mechanical, photocatalytic, and antibacterial properties of the composite film were evaluated. The breaking elongation of the composite film increased up to the maximum loading of 0.4% of nano-TiO2. The humidity and moisture content relationship was estimated with standard modified models of Halsey, Oswin, Chung Pfost, and Henderson. It was found that the Halsey model was the most suitable …
Published in Journal of Polymer & Composites · Vol. 8, Issue 2, 2020 · pp. 110–127 Read article