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66 articles for “X-ray powder diffraction”
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An Overview on Powder X-Ray Diffraction and Its Current Applications
Abstract: AbstractIndustries and research centres are continuously developing novel materials with light weight, higher strength and which can retain their properties at environmental temperatures. The cited properties mainly depend upon micro-structure and chemical composition of materials. Many research works focused to characterize the materials by different experiment techniques. Among them powder x-ray diffraction (XRD) is a most prominent, non-destructive technique used for investigation, characterization, and quality control of crystalline materials. Numerous …
Published in Research & Reviews : Journal of Physics · Vol. 4, Issue 3, 2015 · pp. 6–10 Read article
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Synthesis and Characterization of Terbium Doped Strontium Aluminate Nanophosphor
Abstract: Luminescence investigations of Tb activated strontium aluminate phosphors prepared using the sol-gel method are described. The phosphor has been characterized by powder X-ray diffraction scanning electron microscope. Optical properties were studied by photoluminescence spectra. Photoluminescence studies of the prepared phosphors showed prominent IR emission, apart from near-band edge emission and green emission. Keywords: SrAl4O7, nanomaterial, sol-gel, photoluminescence, X-ray powder diffraction Cite this Article Jisha VT, Suresh G. Synthesis and Characterization …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 6, Issue 2, 2016 · pp. 25–28 Read article
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Sol–Gel Synthesis of SrAl4O7 and Defect-Related Luminescence Properties
Abstract: Single phase of monoclinic SrAl4O7 is synthesized by sol–gel process at a markedly lower temperature as compared to conventional solid-state reaction. The sol–gel derived samples were characterized by thermal gravimetric analysis (TGA), X-ray powder diffraction (XRD) analysis, scanning electron microscope (SEM) and spectrofluorometer. The XRD analysis shows that the strontium aluminate has the monoclinic (α-SrA2) structure. It was demonstrated that the PL emission was obtained at 395 nm, 510 nm …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 2, 2015 · pp. 16–19 Read article
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Novel Poly (Methyl Cellulose-G-Acrylamide)/Sodium Alginate Based Zeolite 4A Filled Mixed Matrix Membranes for The Separation of Water-Isopropyl Alcohol Mixtures by Pervaporation
Abstract: The Filled blend matrix membranes of (Methyl Cellulose-g-Acryl amide)/Sodium Alginate {(MC-g-AAm)/NaAlg} prepared via solution casting method by in situ incorporation with 4A zeolite particles in 5, 10 and 15 mass % with respect to the weight of (MC-g-AAm)/NaAlg membrane. Several analytical tools such as scanning electron microscope (SEM), atomic force microscope (AFM), Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and thermo-gravimetric analysis (TGA) were …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 131–152 Read article
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Exploring the Dual Functionality of Polypyrrole/Cobalt Sulphide Nanocomposite in Photocatalysis and Gas Sensing
Abstract: Cobalt sulphide nanomaterial was synthesized using the co-precipitation method, and chemical polymerization of polypyrrole (ppy) was performed in the presence of the synthesized cobalt sulphide nanomaterial for the preparation of nanocomposite. The synthesized ppy/cobalt sulphide nanocomposite was characterized by transmission electron microscopy (TEM), selected area electron diffraction (SAED), X-ray powder diffraction (XRD), Fourier transformation infrared spectroscopy, and UV-visible spectroscopy. The TEM micrograph revealed that the generated cobalt sulphide nanoparticles were …
Published in Journal of Polymer & Composites · Vol. 11, Issue 3, 2023 · pp. 72–85 Read article
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Characterization of Tabletting Properties of Mango Gum
Abstract: The aim of the study is to elucidate the physical, thermal, sorption, and functional properties of a mango gum obtained from the stem of Mangifera indica were characterized viz. elemental analysis, Fourier transmittance infrared, particle size analysis, thermogravimetric analysis, differential scanning colorimetry, scanning electron microscopy, and X-ray powder diffraction. Mango gum had a glass transition temperature (Tg) and melting peak of 90 and 318.795°C, respectively. This material showed a 14.59% …
Published in Research & Reviews: A Journal of Drug Formulation, Development and Production · Vol. 1, Issue 2, 2014 · pp. 22–30 Read article
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Biosynthesis, Characterization and Non-toxic Activity of Gold Nanoparticles using Geranium (Pelargonium graveolens L.) Leaf Extract
Abstract: Nanoparticles from various materials can be prepared by relatively simple methods. During the past few decades, a variety of different methods have been reported and reviewed for synthesizing gold colloids of monodisperse and uniform sized particles. In present investigation, a new method of one-pot biosynthesizing of gold nanoparticles (GNPs), using geranium leaves extract as a reductant and stabilizer is reported. GNPs were characterized by UV-visible spectroscopy; transmission electron microscopy, X-ray …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 16, Issue 3, 2014 · pp. 1–7 Read article
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Microstructure Analysis and Material Properties of Weld Slag as Fine Aggregate in Concrete
Abstract: To reduce the amount of river sand used, researchers and engineers have developed their own solutions. The well-known technique of submerged-arc welding can create high-quality welds in a variety of thicknesses for ferrous, stainless, and even some non-ferrous metals. The procedure involves an electric current flowing constantly between a welding wire and the work piece, creating an arc. In submerged arc welding, the shielding flux is transformed into slag during …
Published in Recent Trends in Civil Engineering & Technology · Vol. 15, Issue 2, 2025 · pp. 13–18 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis · Vol. 11, Issue 4, 2024 Read article
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Preparation and Characterization of Microwave-assisted Candesartan Cilexetil Solid Dispersions
Abstract: The aim of the present study was to enhance the solubility & dissolution rate of a poorly soluble, BCS class II drug candesartan cilexetil (CC), using its solid dispersions (SDs) with polyethylene glycol (PEG) 6000 & hydroxypropyl methylcellulose (HPMC) E5. Solid dispersions were prepared by melting, solvent evaporation & microwave method. The dispersions were evaluated for various in vitro parameters such as solubility study, dissolution study, fourier transform infrared spectroscopy …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 4, Issue 3, 2013 · pp. 9–19 Read article
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Biosynthesis, Characterization and Antibacterial Studies of Silver Nanoparticles from Tamil Nadu Major Crop Anacardium occidentale
Abstract: Recent studies have shown that Silver Nanoparticles have physical, optical and catalytic properties. Present work involves the eco-friendly and reproducible synthesis of Silver Nanoparticles from the Anacardium occidentale leaves extract. The synthesized silver Nanoparticle from 1 mM AgNO3 solution through the leaf extract were characterizing was monitored using Ultraviolet-visible (UV-vis) spectrophotometer, Scanning electron microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDX), X-ray powder diffraction (XRD) and Fourier transform infra-red spectroscopy (FT-IR).Scanning …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 20, Issue 3, 2018 · pp. 13–22 Read article
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Study of Size Controllable Synthesis of Indium Tin Oxide Nanoparticles and Their Different Characterizations
Abstract: Nanocrystalline indium oxide powders were prepared by combustion synthesis. The changes of nanostructure caused by material processing were studied using X-ray powder diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and Brummer Emette teller analysis (BET). The stoichiometric composition of the starting indium tin oxide powder (cubic in traces) induced phase transitions to high temperature. We found that the phase transition to ITO was initiated at the …
Published in Research & Reviews : Journal of Physics · Vol. 1, Issue 2, 2012 · pp. 9–18 Read article
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Bismuth's Doping Effect on Organic Non linear Optical Materials
Abstract: Using the method of slow evaporation solution growth, single crystals of pure and bismuth-doped urea were produced. Many interesting results on several properties of Bismuth fluoride impurity added to Urea single crystals have been observed and studied. The different morphology of bismuth doped urea crystals was noticed. By using FTIR analysis, the functional group's existence has been approximated. The generated crystals' lattice properties were examined using the single crystal X-ray …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 3, 2023 · pp. 17–24 Read article
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Synthesis and Characterization of Mn Doped ZnO Nanoparticles by Chemical Precipitation Method
Abstract: Normal 0 false false false EN-IN X-NONE X-NONE Nanosized Mn doped ZnO semiconductor (where Mn 0.5%–2.5%) has been synthesized via a chemical precipitation method using zinc acetate hydrate, MnCl2 in alcoholic medium and utilizing polyvinyl pyrolidone (PVP) as capping agent. A differential thermal analysis (DTA) and a thermo-gravimetric analysis (TGA) where used determine the thermal properties of ZnO:Mn. The structural characteristics were examined using X-ray diffraction (XRD).scanning electron microscopy (SEM) …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 3, Issue 2, 2012 · pp. 45–55 Read article
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The Effect of L-Valine on the Growth and Characterization of Lithium Sulphate Monohydrate Single Crystals
Abstract: Pure and amino acid doped good quality single crystals of Lithium Sulphate Monohydrate (LSM) were grown by slow evaporation solution growth technique at room temperature using water as solvent. The effect of amino acid (L-valine) dopant on the growth and characterization of LSM single crystal was investigated. Single-crystal X-ray diffractometer was utilized to find the unit cell parameters for pure and L-valine doped LSM crystals. The powder X-ray diffraction pattern …
Published in Research & Reviews : Journal of Physics · Vol. 8, Issue 1, 2019 · pp. 92–103 Read article
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Exploring the Impact of Lattice Strain on the Debye-Waller Factor in Iron Nanoparticles: A Comprehensive Analysis
Abstract: This study systematically investigates the influence of lattice strain and particle size in iron powder produced through milling, employing X-ray powder diffraction. The determination of lattice strain (ε) and the Debye-Waller factor (B) is accomplished by analyzing Bragg reflection half-widths and integrated intensities. Significantly, the Debye-Waller factor exhibited a notable increase with lattice strain. By establishing a correlation between stress and the influential Debye-Waller factor, we derived a precise relationship …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 215–224 Read article
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Preparation and Charactrization of lead free piezoelectric ceramic/PVA polymer composites
Abstract: Sodium potassium niobate (Na0.5K0.5 NbO3 ) ceramic was prepared through conventional solid state reaction using AR grade NaNO3, KNO3 and Nb2O5 in stochiometric ratio. Poly vinyl alcohol (PVA) polymer - sodium potassium niobate composite films were prepared by solution casting method by changing the blend ratio of PVA / Na0.5K0.5NbO3. The prepared samples in the form of films were characterized by powder X-ray diffraction. The XRD studies revealed the presence …
Published in Journal of Polymer & Composites · Vol. 6, Issue 1, 2018 · pp. 1–8 Read article
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Modified Solution Combustion Approach for Probing of Structural and Dielectric Properties of Sm3+ Doped GdAlO3 Nanoparticles
Abstract: A modified solution combustion approach was used in the preparation of nanosized Gd1xSmxAlO3 (x=1, 3, 5, 7, 9 mol%) using mixture of ODH and novel fuel E. tirucalli plant latex as fuels with corresponding metal nitrates. The structural morphology of synthesized and calcined powders are revealed using various analytical techniques such as Powder X-ray diffraction (PXRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR) and …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 10, Issue 1, 2020 · pp. 16–25 Read article
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Dissolution Enhancement in Nano/Micro-Sized Dispersions of Piroxicam with the Novel Polymer Soluplus® and Polyvinyl Pyrrolidone
Abstract: Piroxicam, a Non-Steroidal Anti-Inflammatory Drug (NSAID), belongs to the class II of the biopharmaceutical classification system (BCS) and thus exhibits poor bioavailability. In an effort to tackle this issue, we report here the comparative properties of the solid dispersions of piroxicam made from a novel graft copolymer of polyvinyl caprolactam-polyvinyl acetate-polyethylene glycol (Soluplus) and the linear polymer polyvinyl pyrrolidone (K 25), both the dispersions synthesized identically using solvent evaporation method. …
Published in Research and Reviews: A Journal of Pharmaceutical Science · Vol. 3, Issue 1, 2012 · pp. 10–19 Read article
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Nanocrystalline Silver: Synthesis by High-Energy Ball Milling, X-ray Debye Temperature Analysis, and Diverse Applications
Abstract: This research paper presents a comprehensive investigation into transforming micro-sized silver (Ag) powder into nanostructured Ag powder by applying high-energy ball milling. The ball milling process was executed over a total duration of 20 hours, with periodic sampling every 4 hours to monitor the evolving characteristics of the material. The particle size, lattice strain, Debye-Waller factor, and root mean square amplitudes of vibration were calculated by using X-ray powder diffraction …
Published in Journal of Polymer & Composites · Vol. 11, Issue 12, 2023 · pp. 140–148 Read article