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272 articles for “scanning electron microscopic”
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Revolutionizing Petrology and Mineralogy: The Study of AI and Advanced Sensor Technologies
Abstract: Petrology and mineralogy are fundamental to understanding Earth's intricate processes, from crustal evolution to economic resource formation. However, traditional methods, while precise, are often laborious, time-consuming, and occasionally subject to interpretive bias. This abstract explores the transformative potential of integrating cutting-edge Artificial Intelligence (AI) and advanced sensor technologies to revolutionize data acquisition, analysis, and interpretation in these critical geosciences. Advanced sensor technologies, including high-resolution spectral imaging (hyperspectral, Raman), automated X-ray …
Published in International Journal of Minerals · Vol. 2, Issue 2, 2025 · pp. 1–11 Read article
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Microstructure Analysis and Material Properties of Weld Slag as Fine Aggregate in Concrete
Abstract: To reduce the amount of river sand used, researchers and engineers have developed their own solutions. The well-known technique of submerged-arc welding can create high-quality welds in a variety of thicknesses for ferrous, stainless, and even some non-ferrous metals. The procedure involves an electric current flowing constantly between a welding wire and the work piece, creating an arc. In submerged arc welding, the shielding flux is transformed into slag during …
Published in Recent Trends in Civil Engineering & Technology · Vol. 15, Issue 2, 2025 · pp. 13–18 Read article
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Optimization of Direct Ink Writing Process Parameters for Liquid Silicone Rubber/TiO2 Composite Ink
Abstract: The purpose of this research is to develop and optimize the Liquid Silicone Rubber (LSR)/Titanium Dioxide (TiO₂) composite inks in Direct Ink Writing (DIW)-based 3D printing systems. The primary research objective was to use enhancement of mechanical, rheological, and dielectric characteristics of LSR using TiO₂ reinforcement but still retain extrusion stability and dimensional consistency. TiO₂ content (0, 5, 10, and 15 wt%) and catalyst and glycerol ratios were regulated and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 240–259 Read article
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Kinetics of Crystallization and Microstructural Evolution of Commercial Fluorophlogopite Machinable Glass- Ceramics in the System SrO∙4MgO∙Al2O3∙ 6SiO2∙2MgF2 with Varying in B2O3
Abstract: Glass materials based on fluorophlogopite stoichiometry with varying concentrations of B₂O₃ were synthesized using the melt-casting method, followed by heat treatment at different crystallization temperatures. The resulting glass and glass–ceramic samples were characterized using differential thermal analysis (DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier-transform infrared (FT-IR) spectroscopy. Kinetic analysis revealed that the activation energies required for the formation of glass–ceramics were 192.77 kJ mol⁻¹ and 210.47 kJ …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 3, 2025 · pp. 1–16 Read article
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Fabrication and Multi scale Characterization of Functionally Graded Composites Reinforced with Hybrid Ceramic–Metallic Phases
Abstract: Using composite materials as functionally graded composites (FGM) can improve its excellent material properties. In this work, magnesium peroxide, silicon carbide, and aluminum are used to create four-layer FGMs. The sintering process, which blends the particles of each material using a powder methodology, has been used to complete the fabrication process. Three factors, including sintering time, sintering temperature, and compacting pressure, are taken into account when fabricating FGM. The FGM …
Published in International Journal of Mechanical Dynamics and Systems Analysis · Vol. 3, Issue 2, 2025 · pp. 1–11 Read article
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Composite Behavior of Bagasse Ash Stabilized Expansive Soil with Sodium Benzophenone Under Curing Conditions
Abstract: The present investigation examines the development of a hybrid composite using Black Cotton (BC) soil, Bagasse Ash (BA), and Sodium Benzophenone (SBP) as performance-enhancing elements. Different ratios of BA, a silica-rich agro-industrial by-product, were added to improve pozzolanic reactivity and particle size distribution (0%, 6%, and 12%). SBP was added in the range of 0–0.6% as a compatibilizer in order to enhance interfacial adhesion, particle cohesivity and moisture-assisted deterioration resistance. …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 1134–1146 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Fabrication and Analysis of PBAT/Cyperus Rotundus Micro Crystalline Cellulose Biofilms for Food Packaging Applications
Abstract: Global plastic waste crisis has gained an increasing attention and many efforts have been made recently to develop biodegradable polymers as food packaging alternatives. Solution casting is used for fabrication and characterization of reinforced polybutylene adipate-co-terephthalate (PBAT) biofilm with Cyperus rotundus microcrystalline cellulose (CRC). PBAT-CRC biofilms with different CRC loadings (1%, and 2%) had been prepared and their structural, mechanical, thermal and morphological properties of fabricated biofilms were analyzed to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 591–599 Read article
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A Study on Tensile Characterization of Polypropylene Reinforced with Recycled Epoxy Particles
Abstract: Polypropylene is a thermo plastic, tensile properties of polypropylene are crucial in the real world applications as they determine structural integrity and durability. Epoxy is a thermosetting plastic finds applications in various fields like aerospace, automobile, food packing etc. A major concern is the disposal of epoxy composites after their service life, since most of the waste is sent to landfills, causing land pollution and soil infertility. In this experimental …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 221–237 Read article
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Polymer Electrolyte Films Doped with Nanofillers ZnO: Electrochemical and Optical Investigations
Abstract: The electrochemical and optical characteristics of polymer composite electrolyte films doped with zinc oxide (ZnO) nanofillers are thoroughly examined in this work. Because of its superior film-forming capacity, flexibility, and ionic transport properties, poly(vinyl alcohol) (PVA) mixed with potassium iodide (KI) is used as the host polymer electrolyte. To investigate their effects on ionic conductivity, dielectric behavior, and optical transmission, ZnO nanoparticles are synthesized and added to the PVA–KI matrix …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 320–332 Read article
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Mechanical Characterization of Kevlar 49 and Pina Fiber Hybrid Composites
Abstract: The pursuit of sustainable yet high-performance materials has accelerated research into hybrid composites that combine synthetic and natural fibers. This study investigates the fabrication and characterization of a Kevlar 49/Pina fiber hybrid composite using epoxy resin as the matrix. Kevlar 49, known for its exceptional tensile strength and energy absorption, was employed as the face sheet material, while Pina fiber, a biodegradable reinforcement extracted from pineapple leaves, was incorporated as …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 301–316 Read article
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Characterization of Polyurethane at Multiple Scales for Erosion Mechanisms Under Sand Particle Impact
Abstract: Thin polyurethane layers have been widely used as erosion-resistant coatings on helicopter rotor blades such as UH-60 Black Hawk and Eurocopter SA 315. Published research has mainly focused on empirical studies that relate the mechanical properties such as rebound resilience and hardness of polyurethane to solid particle erosion resistance. However, polyurethane possesses phase mixing at multiple scales and thus sand particle erosion resistance depends also on the microstructure and the …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 13, Issue 1, 2026 · pp. 1–13 Read article
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Grey Relational Analysis of Cuttlefish Bone Particles–Glass Fiber Reinforced Epoxy Composites
Abstract: This research examines the mechanical characteristics, water absorption performance, and thermal stability of epoxy composites reinforced with Cuttlefish Bone Particles (CFBP) and glass fibers. Composites were fabricated with varying CFBP contents (0%, 3%, 6%, 9%, and 12%) using an epoxy resin as the matrix material and glass fiber as the primary reinforcement. The experimental results revealed that the CFBP-0 composite (neat epoxy with glass fiber) exhibited the highest tensile strength, …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 239–246 Read article
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Mechanical and Thermal Performance of PETG Composites Reinforced with Short Carbon Fibers via Fused Filament Fabrication
Abstract: The study investigates the fabrication and characterization of polyethylene terephthalate glycol (PETG) composites reinforced with short carbon fibers (CF) using the fused filament fabrication (FFF) technique. Composite filaments with varying CF weight fractions (0, 5, 10, 15, and 20 wt%) were produced and evaluated for their mechanical, thermal, and morphological performance. The influence of CF reinforcement on tensile, flexural, and impact behavior was systematically examined, alongside thermal stability metrics including …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1219–1238 Read article
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Investigating The Influence of Sic Reinforcement on The Mechanical and Tribological Properties of PA12 Polymer Composites in SLS
Abstract: The study investigates the mechanical and tribological performance of neat PA12 polymer and SiC-reinforced PA12 polymer composites made via Selective Laser Sintering (SLS). To evaluate just how reinforcement has influence upon overall performance, we incorporated into the PA12 polymer matrix a constant amount of 5 wt.% of Silicon Carbide (SiC). Mechanical testing focused on both tensile and fatigue behavior and testers conducted it with a Servo-Hydraulic Multipurpose High-Capacity Fatigue Test …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 541–554 Read article
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Synthesis and Characterization of pH-Sensitive Poly (N-isopropylacrylamide-co-acrylic Acid) Hydrogels for Controlled Release of Doxorubicin
Abstract: pH-responsive polymeric hydrogels have attracted significant attention as intelligent biomaterials for site-specific and controlled drug delivery in cancer therapy due to their ability to respond to the acidic tumor microenvironment. In the present study, poly (N-isopropylacrylamide-co-acrylic acid) [P(NIPAM-co-AAc)] hydrogels were synthesized via free radical copolymerization and systematically characterized to evaluate their suitability for controlled delivery of doxorubicin, a widely used chemotherapeutic agent. The copolymer hydrogels were prepared using N-isopropylacrylamide and …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 449–458 Read article
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Material-Level Degradation of Magnetorheological Fluids Under Long-Term Cyclic Shear
Abstract: The long-term functional stability of magnetorheological fluids (MRF) remains a key limitation for their reliable use in adaptive systems and continuously operated magnetorheological devices. In this study, the intrinsic evolution of rheological properties in a commercial MRF (MRC-C1L) is systematically examined under prolonged cyclic loading, with the aim of isolating material-level degradation mechanisms independent of device-related effects. The fluid was subjected to 120,000 low-strain oscillatory shear cycles under a constant …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 101–112 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article
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Spin Coated Polyvinylidene Difluoride / Ionic Liquid Nanocomposite Thin Films with Enhanced Dielectric and Piezoelectric Properties
Abstract: This study introduces a novel approach to enhance the piezoelectric and dielectric properties of polyvinylidene difluoride (PVDF) by incorporating 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIM][BF₄]) ionic liquid via a spin-coating method— a processing route that has been rarely reported for PVDF/ionic liquid composites. Structural and morphological analyses using X-ray diffraction (XRD), Raman spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) confirm the successful integration of [BMIM][BF₄] into the PVDF matrix. The …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1190–1204 Read article