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117 articles for “scanning electron spectroscopy (SEM)”
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Enhancement of Dielectric Properties of PVDF Composites with MWCNT and GCNF Fillers
Abstract: The paper discusses the role of multiwalled carbon nanotube (MWCNT) and graphitized carbon nanofibre (GCNF) in Polyvinylidene fluoride (PVDF) composites prepared by melt mixing method. Analytical studies were carried out using X-ray diffraction analysis (XRD) and Fourier transform infrared spectroscopy (FTIR) for understanding the role of fillers. Formation of β phase crystalline structure with a relative increase in β phase content is observed and is maximum at 5 wt.% of …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 43–52 Read article
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To explore the effect of polyethylene glycol additive on mechanical and gas permeation properties of polyvinyl alcohol membranes
Abstract: Polyvinyl alcohol (PVA) membranes were prepared by solution casting and blended with Polyethylene glycol (PEG) in de-ionized water which led to the formation of porous and flexible membranes. Extensive experimentation were performed, in order to find out that at what composition of PEG pores will be generated in the PVA membranes. The PVA polymer is a hard and crystalline thermoplastic so high concentrations of PEG were used, i.e. 40 wt%, …
Published in Journal of Polymer & Composites · Vol. 7, Issue 1, 2019 · pp. 27–33 Read article
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Synthesis and Photoluminescence Dynamics of Europium (III) and Terbium (III) Co-doped of GdSrAl3O7 Color-Tunable Nanophosphors
Abstract: A series of Europium (III) and Terbium (III) co-doped GdSrAl3O7 color-tunable nanophosphors were synthesized by a simplistic, streamlined and self-propagating, urea-assisted solution combustion synthesis process. The structural and luminescence characteristics of synthesized Eu3+/Tb3+ co-doped Gadolinium Strontium Aluminate nanocrystalline phosphors were validated using powder X- ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X- ray analysis (EDAX), and photoluminescence spectra studies. The morphological studies revealed that …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1069–1082 Read article
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Synthesis and Characterization of Co-Doped ZnO Nanoparticles by Electrochemical Method: Photodegradation Kinetics of Bromophenol Blue Dye, Textile Effluent and Study of Antibacterial Activity
Abstract: ZnO nanoparticles doped with cobalt were synthesized by electrochemical method. The crystal structure and surface morphology were characterized by X-Ray diffraction and Scanning electron microscopy. The optical properties were studied by UV-Vis spectroscopy and from this the band gap energy was found to be 3.17 eV. The XRD data revealed that the crystalline size to be ~21.23 nm. The functional group test was done by FTIR-spectroscopy. SEM results showed the …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 1, 2015 · pp. 1–13 Read article
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Studies in Effect of Methyl Methacrylate to Butylacrylate Ratio on the Properties of TiO2/poly(methyl methacrylate-co-butylacrylate) Core–Shell Composite Nanoparticles Prepared by Microemulsion Polymerization
Abstract: AbstractTitanium dioxide, as a core, was coupled with the poly(methyl methacrylate-co-butyl acrylate) using amino propyltriethoxy silane as a coupling agent. A two-stage semi-continuous microemulsion polymerization method was used for the synthesis of these core–shell nanoparticles. Ratio of methyl methacrylate to butyl acrylate was varied in the shell of the nanoparticles and the prepared core–shell composite nanoparticles were characterized by Fourier transform infrared spectroscopy, X-ray diffractometer, differential scanning calorimetry, scanning electron …
Published in Journal of Polymer & Composites · Vol. 1, Issue 3, 2013 · pp. 32–39 Read article
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Exploration of Copper Oxide PVA/PEG Paraffin Polymer Composites for Enhanced Thermal Performance of Nano-Enhanced Phase Change Materials and Their Environmental Impact
Abstract: This study investigates the synthesis, characterization, and application of copper oxide (CuO) nanoparticles integrated into polymer-based paraffin wax composites for advanced thermal management applications. CuO nanoparticles were synthesized using a wet chemical approach and characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and dynamic light scattering (DLS), confirming their crystalline structure, morphology, and nanoscale size distribution. The synthesized nanoparticles were incorporated into polymer-supported phase change …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 156–173 Read article
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Characteristics of Novel Geopolymer Composites Synthesized from Red Mud and Diatomaceous Earth in Autoclave Conditions without Using Alkaline Activators
Abstract: The geopolymer-based materials have been studied and developed since the last decades of the 20th century and applied in many fields of life. The production of geopolymer also has many different levels of technology from low to high technology which depends on quality and the applied fields of products. The geopolymer composites are also considered as friendly environmentally products related to low energy consumption production technology; reuse industrial wastes as …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 81–91 Read article
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Effect of Electrochemically Synthesized Zno/CoO Nanocomposites on Optical, Electrical and Viscosity Properties of Polyvinyl Alcohol Films
Abstract: AbstractZnO/CoO nanocomposites doped poly vinyl alcohol films were prepared by casting method using water as a solvent. X-ray diffraction, IR spectroscopy UV-visible spectroscopy, and scanning electron microscopy techniques were used to characterize the synthesized nanocomposite films. Study of the structural changes and complexation of nanoparticles with polymer matrix were performed using X-ray and IR techniques. Optical characterization studies revealed a blue shift in the absorption edge with increasing nanoparticle concentration …
Published in Journal of Polymer & Composites · Vol. 4, Issue 2, 2016 · pp. 52–62 Read article
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Properties of ZnO Thin Film deposited on Flexible Substrate using RF Sputtering
Abstract: Semiconductor materials demand is increased in recent years, due to new emerging technologies. There is need to find the alternate for silicon in electronics industry, as silicon is brittle in nature and has low efficiency, which makes it unsuitable for transparent and flexible device. Zinc oxide (ZnO) is emerging as popular choice of researchers due to its wide range of properties, abundancy and non-toxicity. This work explores the properties of …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 50–56 Read article
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Bioscouring And Anionization of Waste Cotton Fabric for Efficient Removal of Malachite Green Dye
Abstract: Adsorption is an efficient method for dye removal but the high cost of adsorbents limits its use, emphasizing the need for sustainable, low-cost alternatives. This study explores the usage of modified cotton fabric for the treatment of malachite green (cationic dye) from wastewater. Cellulase extracted from Raphanus sativus and Daucus carota were evaluated for bioscouring potential which was confirmed by scanning electron microscopy. Further, cotton fabric was chemically modified using …
Published in Journal of Water Pollution & Purification Research · Vol. 13, Issue 1, 2026 · pp. 53–68 Read article
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Hybrid Polymer Nanocomposites with Enhanced Dielectric and Optical Properties for Wireless Communication Systems
Abstract: The incorporation of nanofillers into polymer matrices offers a promising approach to enhancing the multifunctional properties of composite materials. This study examines the effect of nanofiller concentration on the dielectric performance, mechanical strength, thermal stability, optical absorbance, and electromagnetic interference (EMI) shielding effectiveness of polyvinylidene fluoride (PVDF)-based nanocomposites. Titanium dioxide (TiO₂) and zinc oxide (ZnO) nanofillers were incorporated at varying concentrations to assess their influence on material properties. EMI shielding …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 518–549 Read article
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Recent Advances in Crystalline Materials
Abstract: Crystalline materials are solids in which atoms, ions, or molecules are arranged in a highly ordered, repeating three-dimensional lattice. This well-defined structure gives rise to unique physical, chemical, electrical, optical, thermal, and mechanical properties, making crystalline materials essential for numerous scientific and industrial applications. Advances in materials science, crystal engineering, and nanotechnology have enabled precise control over crystal size, morphology, composition, and defect structures through innovative synthesis techniques. These developments …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 2, 2026 · pp. 14–21 Read article
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Amorphous Carbon Nanotube (ACNT), Two-dimensional Molybdenum Disulfide Nanosheets (MoS2) and Amorphous Carbon Nanotube-MoS2 Nanohybrids: A Brief Theoretical and Practical Analysis
Abstract: Recently, carbon nanotube and MoS2 nanosheets have been showing great interest in the field of nanoscience and nanotechnology for its exceptional physical, optical and electronic properties. The synthesis procedure of crystalline carbon nanotube is immensely tough for which researchers are focused on amorphous carbon nanotube. Single layer MoS2 with direct band gap shows better semiconductor behavior such as photoluminescence, makes them more acceptable in optoelectronic applications in comparison with graphene, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 3, 2019 · pp. 1–13 Read article
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Structural Investigation on Synthesized Ag Doped ZnO-MWCNT and its applications
Abstract: Metal doped multiwalled carbon nanotube with metal oxide has unique properties which provide the remarkable studies in the field many applications. Zinc oxide nanoparticles (ZnO NPs) is a semiconducting material with a large excitation binding energy of 60 meV and wide energy band gap of 3.367 eV. The doping of silver naoparticle with ZnO/MWCNT composite materials offer values and makes it as advanced multifunctional materials. Silver nanoparticles are a highly …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 8, Issue 2, 2018 · pp. 49–59 Read article
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Preparation and characterization of High-performance ZnO/PVB Nanocomposite films for UV-shielding and Optoelectronics
Abstract: Zinc oxide nanoparticles can be incorporated into polymer matrices to create materials for various high-performance engineering applications. In this study, zinc oxide nanoparticles were reinforced at different loadings (0.5, 1.0, 0.5, 1.0, 1.5, and 2.0 wt.%) in polyvinyl butyral matrix to synthesize nanocomposite films using the solution casting method. The impact of zinc oxide nanofiller on the morphology and ultraviolet-shielding performance of polyvinyl butyral nanocomposite films was evaluated using various …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 27, Issue 3, 2025 · pp. 35–53 Read article
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Catalyst-Driven Degradation and Failure Analysis of Intergranular Cracking in 316H Studded Pipes under Refinery Heat Recovery Conditions
Abstract: A failure analysis investigation was carried out on a high-temperature studded pipe used in a convection module for heat recovery in an oil and gas refinery application after leakage was detected during pre-commissioning hydrotesting. The investigated pipe was manufactured from AISI 316H austenitic stainless steel, and carbon steel studs had been joined to its outer surface by high-frequency resistance welding. Two leaks were reported in the pipe under investigation, and …
Published in Journal of Catalyst & Catalysis · Vol. 13, Issue 1, 2026 Read article