Search
144 articles for “SEM and FTIR.”
-
Electron beam irradiation studies of polyethylene maleic anhydride on their Chemical and Thermal properties.
Abstract: The electron beam (e-beam) irradiation effects on polyethylene maleic anhydride (MANPE) are investigated by spectroscopic and thermal methods. The MANPE irradiated with electron beam to a radiation dose of 30, 60 and 90 K Gy and the resultant changes in their chemical structure and thermal properties have been investigated by Electron spin resonance (ESR), Fourier transform infrared spectroscopy (FTIR), differential scanning calorimetry (DSC), X-ray diffraction (XRD) and scanning electron microscopy …
Published in Journal of Polymer & Composites · Vol. 6, Issue 2, 2018 · pp. 17–30 Read article
-
Effect of Bismuth doping on Thiourea crystals : A NLO Material
Abstract: Single crystals of pure and thiourea-substituted bismuth were successfully grown using the slow evaporation solution growth technique at ambient temperature. The impact of thiourea doping on the crystal properties was thoroughly investigated. Solubility tests for the grown samples were conducted at various temperatures, providing crucial data on the dissolution characteristics. Structural characterization of these crystals was performed using single crystal X-ray diffraction (XRD), confirming their crystalline nature. Energy-dispersive X-ray spectroscopy …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 15, Issue 2, 2024 · pp. 10–16 Read article
-
Influence of B2O3 and Li2O on Physical, Thermal and Spectroscopic properties of Bi2O3-B2O3-CdO-Li2O glass system
Abstract: ABSTRACT Bismuth Borate based glasses with compositions BiBCL: 40Bi2O3-(40-X) B2O3-20CdO-XLi2O where x=5,10,15,20,25 mol% were prepared by conventional melt quenching technique. X-ray diffraction (XRD), differential thermal analysis (DTA), UV-VIS absorption spectroscopy, Fourier transform-infrared (FTIR), and Raman spectroscopies were used to analyse the synthesized samples. Through XRD and SEM studies, the synthesized glasses amorphous nature was confirmed. To evaluate the physical and structural characteristics of the glasses, calculations were made for the …
Published in Journal of Polymer & Composites · Vol. 11, Issue 1, 2023 · pp. 51–62 Read article
-
Gelatin-EiO2 (Ei = Si/Ti/Zr) Based Mesoporous Nano-hybrids: Synthesis and Characterization
Abstract: The hybrid materials are mostly prepared by combining the organic or bio-organic part to the inorganic building blocks and are used in many applications. Gelatin as one of the main component of hybrid materials is an attractive option. It is biodegradable; biocompatible; non-toxic; bio-adhesive and contains many active groups such as –NH2, –COOH, in the biopolymer backbone makes these hybrid materials important in various technological applications. The synthesis of a …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 3, 2024 · pp. 30–58 Read article
-
Au@Sio2@PVP-DCMD Membranes: A Breakthrough in Heavy Metal Removal and Antibacterial Defense
Abstract: This study investigates the development and characterization of multifunctional gold-doped silica (Au@SiO₂) membranes for water distillation and antibacterial applications. The manufacturing process integrated gold nanoparticles into silica matrices using sol-gel techniques. Structural analysis was conducted using SEM (showing uniform pore distribution with an average pore size of 40-50 nm), FTIR (confirming Si-O-Si and Si-Au-Si bonding peaks at 525 cm⁻¹ and 1310 cm⁻¹ respectively), EDX (revealing gold nanoparticle content of 1.5 …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 13–27 Read article
-
Synthesis and Characterization of Polyvinyl alcohol film incorporated with Tridax procumbens leaf extract
Abstract: Active film materials are prepared by incorporation of natural antimicrobial and antioxidant agents. These materials have attracted growing interest in wound dressing and food packaging process. In this study, active films were developed by incorporation of Tridax procumbens (T. procumbens) leaf extract into Polyvinyl Alcohol (PVA) matrix. T. procumbens leaves have been accounted for their biomedical and nutritional properties. The impact of T. procumbens leaf extract on the physical, mechanical …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 40–51 Read article
-
Synthesis and Characterization of Polymer Blend Electrolyte Based on Bio-degradable Polymers Doped with Ammonium Iodide
Abstract: A polymer blend of Polyvinylalchohol (PVA) and Polyvinylpyrrilodine (PVP) doped with ammonium iodide (NH4I) has been prepared by solution casting method to develop a new solid polymer electrolyte. The influence of NH4I on the structural, electrical characteristics of PVA/PVP blend was investigated utilizing XRD, FTIR and impedance spectroscopy techniques. Structural properties were studied by using the XRD technique and found that the pure polymer blend is in semi crystalline form, …
Published in Journal of Polymer & Composites · Vol. 10, Issue 2, 2022 · pp. 60–71 Read article
-
Green Synthesis of Gold Nanoparticles Using Piper Nigrum (Black Pepper) Aqueous Extract
Abstract: In the present study, we wish to report the green synthesis of gold nanoparticles using aqueous extract from fruit of black pepper. The extract with different concentrations was reduced with HAuCl4 aqueous solution at room temperature. The color change, pH change and UV-visible spectroscopic analysis reveal the surface plasmon resonance (SPR) of the final reaction product which confirms the reduction of Au3+ ion to gold nanoparticles. The FTIR spectra confirms …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 2, 2012 · pp. 48–57 Read article
-
Development and Characterization of Antimicrobial Polymer Composites for Food Packaging Applications
Abstract: The increasing demand for sustainable and antimicrobial food packaging materials has led to extensive research in polymer-based composites. This study focuses on developing a polyethylene terephthalate-ethylene vinyl acetate (PET-EVA) composite reinforced with metal oxide nanoparticles (MONs), including Cu₂O, ZnO, and MgO₂. These nanoparticles were selected for their antimicrobial properties and ability to enhance the functional characteristics of the composite. Structural, chemical, mechanical, and barrier properties were extensively evaluated to determine …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 86–93 Read article
-
Effect of concentration of Halloysite nanotubes on the Mechanical, Thermal and electrical properties of NBR/PP Elastomer nanocomposites
Abstract: Preparation of nanocomposites from immiscible polymer blends system has been investigated in this work. Natural clay named halloysite nanotubes are incorporated in the immiscible blend system using melt mixing process to prepare halloysite based nanocomposites comprising of PP/NBR blend system. FTIR studies have been carried out to establish the structure properties relationship. Nanocomposites are characterized by SEM for morphological studies. The thermal stability of nanocomposites has been evaluated by TGA …
Published in Journal of Polymer & Composites · Vol. 8, Issue 2, 2020 · pp. 62–67 Read article
-
Synthesis and Characterization of VO 2+ doped SrMg 2 (PO 4 ) 2 Nanopowder by Solid State Reaction technique suitable for White LED material
Abstract: VO2+ doped SrMg2(PO4)2 nanopowder was synthesized by using solid state reaction (SSR) technique. Various experimental techniques have been performed on prepared sample. XRD analysis has revealed that prepared nanopowder is in monoclinic phase. The average crystallite size, micro strain and dislocation density evaluated and make an analogy with W-H plot method. SEM micrographs shows that agglomerated stone like structure and EDS spectrum shows elemental compositions of synthesized sample. FTIR spectrum …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 95–110 Read article
-
Green synthesis of zinc oxide and copper oxide nanoparticles and their effect against wilt fungus, Fusarium udum.
Abstract: Nowadays nanoparticles (NPs) come out as powerful tools to enhance crop production and protection. Biosynthesis of NPs has a vital role and an alternate to chemical and physical methods because it is simple, easy, eco-friendly, and free from chemical hazards. Zinc oxide (ZnO) and copper oxide (CuO) NPs were synthesized from leaves extract of Lantana camara (L.) and Nerium oleander (L.) and characterized by using several techniques such as transmission …
Published in Research and Reviews : A Journal of Life Sciences · Vol. 13, Issue 3, 2023 · pp. 1–5 Read article
-
Solid acidity of MoO3 synthesized by solution combustion method and acetalization of formaldehyde using it
Abstract: MoO 3 nanoparticles were synthesized via solution combustion approach. Ammonium nitrate was used as oxidant and ammonium molybdate as fuel in combustion reaction. XRD, FTIR and Raman spectroscopy results showed that MoO 3 nanoparticles were successfully synthesized by the solution combustion reaction. The SEM analysis showed that synthesized MoO 3 nanoparticles have rod-like shape with width and thickness of 50-200nm and length of 0.2-1μm, respectively. The XRD pattern and morphology …
Published in Journal of Catalyst & Catalysis · Vol. 12, Issue 3, 2025 · pp. 01–09 Read article
-
Sonochemical Synthesis and Photo-Catalytic Study of Cd Doped Znse Nanoparticles
Abstract: Cd doped ZnSe nanoparticles have been successfully synthesized with sonochemical process by reacting high purity acetates and sodium selenosulphate at 343 K. The size of nanoparticles was calculated by using powder XRD. It shows the crystalline size ranging between 35.3 nm to 45.44 nm. XRD further shows that ZnSe nanocrystallites are polycrystalline in nature and belong to the hexagonal phase. SEM shows that the particles are spherical in shape. Effect …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 17, Issue 1, 2015 · pp. 32–41 Read article
-
Synthesis of Activated Carbon from Corn Cob and Factors Affecting its Adsorption and Desorption Efficiency of Cationic Brilliant Green Dye
Abstract: Extreme dye pollutants released from textile, leather, and pulp industries are becoming a major concern to the water. These pollutants are highly toxic to living things. The major objective of this study was to prepare low-cost and efficient activated carbon from corncob (CCAC) adsorbent through the H2SO4 activation method and characterize its suitability for removing brilliant green dye (BGD) from aqueous solution. The adsorption and desorption efficiency of the prepared …
Published in Journal of Water Pollution & Purification Research · Vol. 12, Issue 3, 2025 · pp. 27–44 Read article
-
Experimental Investigation for Strengthening the Nanocomposite Cementitious Materials with a Nanoscale Modification
Abstract: For the last few decades, researchers have widely used nanopolymer to control the mechanical properties of cementitious materials as a micro reinforcement. This paper examines and compares the mechanical and microstructure property of nanofiber cementitious material. Twenty-four sets of beam/cube cast with carbon nanofibers (CNFs) cementitious material where CNFs were used from 0.1%, 0.2%, and 0.3% of cement weight. The nanoparticles were scattered using a surfactant and an ultrasonic probe …
Published in Recent Trends in Civil Engineering & Technology · Vol. 12, Issue 2, 2022 · pp. 10–24 Read article
-
In-Situ Polymerized GO/PANI Composites: Structural Evolution, Optical Modulation, and NH₃ Sensing at Room Temperature
Abstract: Graphene oxide (GO)/polyaniline (PANI) composites with varying PANI contents (20, 40, and 60 wt%) were synthesized via in-situ oxidative polymerization and systematically investigated for their structural, morphological, optical, and gas-sensing properties. X-ray diffraction (XRD) confirmed a progressive increase in interlayer spacing and partial exfoliation of GO layers with increasing PANI content, indicating intercalation-assisted hybridization. Fourier transform infrared (FTIR) spectroscopy revealed the characteristic vibrational bands of both constituents and confirmed strong …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 509–525 Read article
-
Sonochemical Synthesis of SrBaFexMo2-xO6 (x=1.0, 1.1, 1.3 and 1.4) Double Perovskites: Characterization and Magnetic Properties
Abstract: This work investigates ultrasound assisted synthesis, characterization and magnetic properties of SrBaFexMo2-xO6 (x=1.0, 1.1, 1.3 and 1.4) double perovskites. X-ray diffraction (XRD) analysis confirmed proposed that samples are in single phase. It was found that lattice constants decrease with increase in composition x. Morphology of all samples was examined by Scanning Electron Microscopy (SEM) images. Energy Dispersive X-ray Spectroscopy (EDS) data confirmed purity and nonexistence of foreign elements in prepared …
Published in Research & Reviews : Journal of Physics · Vol. 7, Issue 2, 2018 · pp. 8–17 Read article
-
Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
-
Multifunctional Lignin-Modified Jute/Bio-Epoxy Composites with MWCNT-Based Piezoresistive Self-Sensing for Sustainable Housing Applications
Abstract: This study develops a multifunctional natural-fibre-reinforced polymer composite based on alkali-treated jute fabric, bio-based epoxy, kraft lignin and a small amount of multiwalled carbon nanotubes (MWCNTs), with particular emphasis on polymer-matrix modification, fibre–matrix interfacial behaviour and intrinsic damage sensing. Kraft lignin was incorporated at 0, 2, 4 and 6 wt.% to examine its influence on polymer-chain mobility, interfacial morphology, thermal stability and mechanical response, while 0.5 wt.% MWCNTs was introduced …
Published in Journal of Polymer & Composites · Vol. 14, Issue 5, 2026 Read article