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145 articles for “scanning electron microscopy”
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Synthesis of Magnetically Recoverable Nickel (II) Complex-Functionalized Fe3O4@ISNA (ISNA= Isonicotinic acid) Nanomaterials: Catalytic Studies on Nitrophenol Reduction and TD- DFT Studies
Abstract: In this study, we aimed to develop a novel, environmentally sustainable, and magnetically separable heterogeneous nanocatalyst, denoted as Fe3O4@ISNA@NiL (where L represents the ligand). The synthesis involved a two-step process, first, isonicotinic acid was chemically grafted onto the surface of iron oxide nanoparticles (Fe3O4) to introduce functional groups capable of further chemical modification. Subsequently, a nickel(II) Schiff base monomeric complex was anchored onto the modified surface, resulting in a nanocatalyst …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 88–96 Read article
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Synthesis of Magnetically Recoverable Nickel (II) Complex-Functionalized Fe 3 O 4 @ISNA (ISNA= Isonicotinic acid) Nanomaterials: Catalytic Studies on Nitrophenol Reduction and TD- DFT Studies
Abstract: In this study, we aimed to develop a novel, environmentally sustainable, and magnetically separable heterogeneous nanocatalyst, denoted as Fe 3 O 4 @ISNA@NiL (where L represents the ligand). The synthesis involved a two-step process, first, isonicotinic acid was chemically grafted onto the surface of iron oxide nanoparticles (Fe 3 O 4 ) to introduce functional groups capable of further chemical modification. Subsequently, a nickel(II) Schiff base monomeric complex was anchored …
Published in Journal of Polymer & Composites Read article
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Synthesis and Photoluminescence Dynamics of Europium (III) and Terbium (III) Co-doped of GdSrAl3O7 Color-Tunable Nanophosphors
Abstract: A series of Europium (III) and Terbium (III) co-doped GdSrAl3O7 color-tunable nanophosphors were synthesized by a simplistic, streamlined and self-propagating, urea-assisted solution combustion synthesis process. The structural and luminescence characteristics of synthesized Eu3+/Tb3+ co-doped Gadolinium Strontium Aluminate nanocrystalline phosphors were validated using powder X- ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X- ray analysis (EDAX), and photoluminescence spectra studies. The morphological studies revealed that …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1069–1082 Read article
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Integrative Machine Learning Approaches for Predicting the Rheological Behaviour of Soft Magnetorheological Elastomers
Abstract: Magnetorheological Elastomers (MREs) are advanced composite materials known for their ability to alter mechanical properties under external magnetic fields, making them highly valuable in adaptive damping systems, vibration control, and smart devices. The accurate prediction of rheological behavior in soft MREs remains a significant challenge due to the complex interplay between material composition and magnetic fields. To address this challenge, this study employs a multi-pronged approach that integrates traditional material …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 1083–1096 Read article
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Composite Gel-Fibers and Solid-State-Processed Tapes Based on Disentangled Ultra-High Molecular Weight Polyethylene and Electrically Conductive Carbon Black: a Comparative Study
Abstract: In this study, oriented nanocomposite gel-spun fibers and solid-state-processed tapes were manufactured and analyzed. The fibers and tapes were produced using a specific type of nascent disentangled ultra-high molecular weight polyethylene (UHMWPE) reactor powder. As the filler, commercially available electrically conductive carbon black (CB) was used. The ultra-high filler content values up to 75 wt.% were achieved for the UHMWPE/CB gel-spun fibers, while the degree of filling was limited (up …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 151–165 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts: Properties and Applications
Abstract: The main study and the development of CeO2 and Cu-doped CeO2 nanocrystals containing transition- metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu-doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. The structural properties of Ce1-xCuxO2 nanocrystals were examined by investigating the influence of cerium dioxide and Cu dopant ions. The CeO2 single-phase cubic system was successfully incorporated with Cu …
Published in Journal of Catalyst & Catalysis · Vol. 11, Issue 3, 2024 · pp. 29–38 Read article
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Sustainable Innovations in Green Nanotechnology for Nanoparticle Synthesis
Abstract: Green nanotechnology is an emerging field that focuses on the environmentally friendly production of nanoparticles through biological and sustainable processes. This approach has diverse applications across industries such as pharmaceuticals, energy, electronics, and bioengineering. Compared to conventional methods, biologically driven nanoparticle synthesis, particularly utilizing green chemistry principles, offers a safer, eco- friendly, non-toxic, and cost-effective alternative. Metal nanoparticles are commonly synthesized through top-down and bottom-up strategies using physical, chemical, and …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 3, Issue 1, 2025 · pp. 31–37 Read article
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Improving the Mechanical and Interfacial Properties of Bhendi Fiber via Chemical Surface Treatments
Abstract: Because of its primary benefits—moderate strength and stiffness, low cost, and being a renewable, degradable, and ecologically friendly material—natural fibers are believed to have potential use as reinforcing agents in polymer composite materials. Due to their inherent hydrophilicity, they have a tendency to retain moisture, which can impair or soften the fibers' adhesion to the surrounding matrix. This can have an impact on the performance of composite materials used in …
Published in International Journal of Advance in Molecular Engineering · Vol. 3, Issue 1, 2025 · pp. 22–32 Read article
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Enhancing The Mechanical Performance of Al6061/Graphite Composites Reinforced with Sic and Aluminium Oxide Processed by Stir Casting
Abstract: The study investigates the mechanical properties of aluminum alloy Al6061 reinforced with varying proportions of silicon carbide (SiC) (0 wt%, 4 wt%, 5 wt%, and 6 wt%) and aluminum oxide (Al₂O₃) (0 wt%, 4 wt%, 3 wt%, and 2 wt%), with a constant addition of 1 wt% graphite. The composites were fabricated using the stir casting process, an efficient and economical method for uniformly distributing ceramic reinforcements within the metal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 66–74 Read article
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Green Synthesis of Cobalt Oxide Nanoparticles Using Delonix regia Leaf
Abstract: Green synthesis of nanoparticles offers a sustainable and eco-friendly alternative to conventional methods. This study explores the biosynthesis of cobalt oxide nanoparticles (Co3O4 NPs) using Delonix regia leaf extract as a reducing and stabilizing agent. The synthesized Co3O4 NPs were characterized by UV-visible spectroscopy, Fourier transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM), confirming their uniform spherical morphology with an average size of …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 30–38 Read article
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A Comparative Study of Oven, Spouted Bed, and Convective Tunnel Drying Methods of Mango for Oil Production
Abstract: Mango seeds, with a high moisture content exceeding 70% (wet basis) require effective drying methods to ensure their preservation and to enhance the quality of derivative products like mango seed oil. Proper drying is essential to inhibit enzymatic activity and microbial growth, which extends the shelf life of these seeds. This study investigates multiple drying techniques, including conventional oven drying, spouted bed drying, and convective tunnel drying, to determine their …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 1, 2025 · pp. 15–19 Read article
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Experimental Investigation and Surface Morphology Study on Areca Fiber Composite Material
Abstract: Composites manufactured from areca fibers had their characteristics assessed in recent research. Shape and size were determined by cutting the stem. It takes six months to dry the fibers once they are taken from the tree stem. Because pectin, cellulose, hemicellulose, and lignin make up the bulk of it. It has great regeneration capacity and is a resource material made of wood fibers. The untreated and chemically treated fibers are …
Published in Journal of Polymer & Composites · Vol. 13, Issue 1, 2025 · pp. 459–468 Read article
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Synthesis and Characterization of Sustainable, Low-Cost, Biomass-Derived Carbon Films from Hevea Brasiliensis (Rubber) Wood for Environmentally Friendly Gas Sensors with Enhanced Selectivity and Sensitivity to Polar Vapors and Hazardous Gases
Abstract: Hevea brasiliensis (rubber) wood sawdust was utilized to fabricate carbon gas sensors for detecting 1000 ppm of ethanol, methanol, acetone, carbon dioxide, and ammonia gases. The carbon particles were prepared by phosphoric acid impregnation followed by thermal activation and then fabricated into films on conductive and non-conductive substrates using the doctor blade method. X-ray diffraction (XRD) analysis revealed distinct graphitic features with peaks at the (002) and (100) planes, indicating …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 1, 2025 · pp. 22–36 Read article
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Synthesis and Characterization of Forsterite Incorporated HDPE Composites for Microwave Substrate Application
Abstract: High Density Polyethylene (HDPE) combined with dispersed forsterite (Mg₂SiO₄) powder was utilized to fabricate polymer matrix composites (PMCs) aimed at high-frequency microwave substrate applications. Forsterite powders were synthesized using the mixed oxide method, and their phase purity was confirmed by X-ray diffraction (XRD) analysis. The dispersion and morphology of the ceramic filler within the HDPE matrix were examined through Scanning Electron Microscopy (SEM), ensuring a homogeneous distribution essential for optimal …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 109–120 Read article
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Wettability and Physiothermal Analysis of Silver-Reinforced Eggshell-Derived Hydroxyapatite Based Biocomposite
Abstract: Hydroxyapatite (HAp), a biocompatible ceramic material, has garnered significant interest in medical applications due to its natural bone type replica. The current study investigates the physical, wettability, and thermal properties of a novel HAp derived from eggshell waste and reinforced with silver nanoparticles at 0.0, 0.1, 0.2 and 0.5 weight % concentration using chemical precipitation method and termed as HAP0.0Ag, HAP0.1Ag, HAP0.2Ag and HAP0.5Ag respectively. As observed, the Fourier transform …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 300–314 Read article
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Development of Robot Arm Fingers with Polymer Soft Materials
Abstract: Lightweight soft material applications have attracted attention to Basalt Fiber Reinforced Polymer (BFRP) laminates because of their impressive mechanical characteristics. The impact response and stress-strain behavior of epoxy resin laminates armored with basalt fiber and banana fiber are investigated during this project using computational and experimental approaches. The hand lay-up method was employed to create laminates with a thickness of 3 mm, dimensions of 300x300 mm², and a layout of …
Published in Journal of Polymer & Composites · Vol. 13, Issue 2, 2025 · pp. 432–439 Read article
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Exploring the Luminescent Behavior of Dysprosium-Doped Halo-sulphate Compounds
Abstract: In essence, this study aims toward understanding the photo-luminescent properties of Dy³⁺ halogenated sulfates, viz., synthesis, characterization, and luminescent behavior of the materials. Dysprosium ions are introduced into the halo-sulfate matrices to investigate their suitability for solid-state lighting applications. The aim of the study is to explain the mechanisms of the photo luminescence of Dy³⁺ and study the influence of the doping concentration on luminescence efficiency and the thermal stability …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 3, 2025 · pp. 01–06 Read article
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Acalypha Indica Root Fibre in Polymer Composite: Mechanical Characterization
Abstract: The mechanical characteristics of Acalypha Indica root fibre reinforced epoxy resin composites, including tensile strength, tensile modulus, percentage of elongation, flexural strength, and impact strength, were studied. Composites were fabricated using epoxy glue and randomly oriented fibres of 3 mm length in varying weight ratios of 10%, 20%, 30%, and 40%. The hand layup method was followed by compression moulding to construct the composites. The study aimed to determine the …
Published in Journal of Polymer & Composites · Vol. 13, Issue 3, 2025 · pp. 512–522 Read article
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Development and Characterization of Antimicrobial Polymer Composites for Food Packaging Applications
Abstract: The increasing demand for sustainable and antimicrobial food packaging materials has led to extensive research in polymer-based composites. This study focuses on developing a polyethylene terephthalate-ethylene vinyl acetate (PET-EVA) composite reinforced with metal oxide nanoparticles (MONs), including Cu₂O, ZnO, and MgO₂. These nanoparticles were selected for their antimicrobial properties and ability to enhance the functional characteristics of the composite. Structural, chemical, mechanical, and barrier properties were extensively evaluated to determine …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 86–93 Read article
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Mechanical Property Assessment of Hybrid Composite Laminates Composed of Jute Glass Fibers in Combination with Flax, Hemp, Sisal and Kenaf Fibers Using the Hand Layup Technique
Abstract: The present work compares the properties of various hybrid composite laminates manufactured using the hand layup technique and addresses their production process, based on glass fiber as the exterior layer and natural fibers (flax, hemp, kenaf, jute, and sisal) as interior layers, in an epoxy resin. Five stacking sequences A-GJJJJG, B-GFJJFG, C-GHJJHG, D-GKJJKG, and E-GJSSJG were used to prepare the test specimens. According to ASTM guidelines, experiments were performed to …
Published in Journal of Polymer & Composites · Vol. 13, Issue 4, 2025 · pp. 103–113 Read article