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149 articles for “Crystals and Sizes”
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Study of Size Controllable Synthesis of Indium Tin Oxide Nanoparticles and Their Different Characterizations
Abstract: Nanocrystalline indium oxide powders were prepared by combustion synthesis. The changes of nanostructure caused by material processing were studied using X-ray powder diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and Brummer Emette teller analysis (BET). The stoichiometric composition of the starting indium tin oxide powder (cubic in traces) induced phase transitions to high temperature. We found that the phase transition to ITO was initiated at the …
Published in Research & Reviews : Journal of Physics · Vol. 1, Issue 2, 2012 · pp. 9–18 Read article
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Fabrication and Characterization of Copper Nanowires: An Overview
Abstract: Copper (Cu) is one of the most important metals in modern electronic technology. Keeping in view its role in nanoelectronics, we have fabricated copper nanowires of diameters 100 and 200 nm using Anodic Alumina and polymer membranes as templates. Template-based growth of copper nanowires has been realized using conventional electro deposition technique in an electrochemical cell designed in our laboratory. Fabrication of copper nanowires is one of the most important …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 1, Issue 1, 2011 · pp. 1–16 Read article
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A Comparative Study of Zinc Oxide Nano Particles Synthesized by Hydrothermal, Sol-gel and Thermal Decomposition
Abstract: In the proposed work, Zinc oxide nano particles (ZnO NP's) are synthesized using three different methods: Hydrothermal, Sol-gel and Thermal decomposition. The samples are characterized using X- ray diffraction (XRD), UV visible spectroscopy (UV-Vis), Fourier Transform Infrared Spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD pattern exhibit single-phase polycrystalline nature of all the samples exhibiting the most intense peak at (101). The diffraction peaks are located at 31.80, 34.46, …
Published in Journal of Polymer & Composites · Vol. 11, Issue 7, 2023 · pp. 39–45 Read article
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Optimization of gas sensitivity of CuO/carbon composites with carbon particles synthesized from acacia auriculiformis branches
Abstract: Carbon particles fabricated from the core of acacia tree branches were utilized to synthesize CuO/carbon composite films. The gas sensing properties of these films grown on glass substrates using the doctor blade method were measured in 1000 ppm of methanol vapor at the room temperature. All the films were annealed at 75 0C for 1 hour in air. The structure, the optical band gap and the surface morphology of the …
Published in International Journal of Membranes · Vol. 1, Issue 1, 2024 · pp. 22–30 Read article
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Influence of Gd Doping in Structural, Morphological and Optical Properties of Zno Nanostructures Synthesised Via Sol-Gel Processes
Abstract: In this study, nanocrystalline Zn1-xGdx (x=0.0 and 0.03) samples were synthesised via the Sol-gel combustion process. An array of analytical techniques was employed to examine the prepared samples to determine their different physical features. For both pristine and Gd-doped samples, the crystal symmetry is hexagonal with the P63mc space group which is verified via the Rietveld refinement analysis of X-ray diffraction (XRD) data. The atoms' bond length Zn-O and bond …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 219–225 Read article
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Enhancement of Gas Sensitivity of Composites of Carbon Derived from Rubber Tree and SnO2 to Detect Ethanol Vapor at Room Temperature
Abstract: Films of composites of activated carbon powder prepared from saw dust derived from core of rubber tree (Hevea Brasiliensis) and tin oxide (SnO2) were fabricated using the doctor blade method. Carbon powder was activated using phosphoric acid at 500°C for 45 minutes. The weight ratio carbon/SnO2 varied from 0 to 12% in steps of 2. The structural, optical and morphological properties of films were investigated using XRD patterns, UV-visible spectrums …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 2, 2025 · pp. 31–44 Read article
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Facile Synthesis and Characterization of Cd²⁺ Doped NiAl₂O₄ Nanoparticles for Advanced Polymer Composite Integration
Abstract: Ni1-xCdxAl2O4, where 0 ≤ x ≤ 0.5, was successfully synthesized using the chemical co-precipitation technique, a scalable and cost-effective route suitable for composite material applications. X-ray diffraction (XRD) analysis revealed a crystalline cubic spinel structure for the resulting nanoparticles, with determined crystallite sizes ranging from 36 to 12 nm for NiAl2O4 and Cd-doped NiAl2O4. The respective band gaps for the materials were found to be 3.51 and 4.18 eV. Infrared …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 59–72 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Combustion Synthesis and Comprehensive Characterization of Pure and Ni-Doped CuFe₂O₄ Nanoparticles for Functional Composite Applications
Abstract: The CuFe2-xNixO4 (x = 0, 0.1, 0.3, and 0.5) nanoparticles were synthesized using a combustion method and comprehensively characterized to understand their suitability for polymer-based composite applications. X-ray diffraction confirmed the formation of a single-phase spinel ferrite structure with crystallite sizes of 20–30 nm. Energy-dispersive X-ray spectroscopy verified the successful incorporation of Ni ions into the CuFe₂O₄ lattice, while FE-SEM analysis revealed uniformly dispersed nanoscale particles desirable for composite reinforcement. …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1–11 Read article
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Synthesis, characterizations, and challenges of magnetic Zn x Fe 2-x O 3 nanoparticles
Abstract: Diluted magnetic semiconductors comprising magnetic nanoparticles are a driving force in a variety of applications, including biomedicine, bioelectronics, photocatalytic activities, and nanosensors. However, the functionality of these nanomaterials can be influenced by several factors, such as synthesis route, characterization procedures, source, crystal size, and morphology. In this research, emphasis is devoted to synthesizing and characterizing magnetic nanoparticles. Most importantly, it is focused on biological methods, Co-precipitation methods, hydrothermal Gravity methods, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 28, Issue 2, 2025 · pp. 1–16 Read article
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Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material
Abstract: With the enlargement of flexibility and suitability in material industries, high-performance thermal management materials are demanded with high thermal conductivity and electrical insulation are growing. In recent years, graphene has received a numerous focus from science community due to its high thermal conductivity and electrical insulation. Fabrication of light weight graphene and its derivatives as graphene Oxide (GO) and reduced graphene oxide (rGO) via facile processing method is yet a …
Published in Journal of Polymer & Composites Read article
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Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material
Abstract: With the enlargement of flexibility and suitability in material industries, high-performance thermal management materials are demanded with high thermal conductivity and electrical insulation are growing. In recent years, graphene has received a numerous focus from science community due to its high thermal conductivity and electrical insulation. Fabrication of light weight graphene and its derivatives as graphene Oxide (GO) and reduced graphene oxide (rGO) via facile processing method is yet a …
Published in Journal of Polymer & Composites · Vol. 12, Issue 5, 2024 · pp. 25–36 Read article
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Structural, Optical, Surface, and Gas-Sensing Properties of rGO/Sn1–xZnxO₂ Nanocomposites
Abstract: rGO/Sn₁–ₓZnₓO₂ nanocomposites with x = 0.00–0.75 were synthesized by sol–gel auto-combustion followed by wet impregnation with reduced graphene oxide. The adopted synthesis route enabled homogeneous Zn incorporation into the SnO₂ matrix and uniform distribution of rGO, leading to improved structural integrity and interfacial contact between the two components. XRD confirmed a dominant tetragonal cassiterite SnO₂ structure, while FTIR, FESEM, EDS, UV–visible, and BET analyses verified oxide–rGO coupling, Zn-dependent structural modification, …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 429–452 Read article
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Application of Polypyrrole/Lead Sulphide Nanocomposite in UV Light Assisted Photocatalysis and Gas Sensing
Abstract: The synthesis of ppy/lead sulphide nanocomposite was done using the co-precipitation method. The synthesized ppy/leadsulphide nanocomposite was characterized using Transmission Electron Microscopy (TEM), Selected Area Electron Diffraction (SAED), X-Ray Powder Defraction (XRD), Fourier Transformation Infra-Red Spectroscopy (FTIR), UV-Vis Spectroscopy techniques. The optical bandgap of the synthesized ppy/lead sulphide nanocomposite was observed to be 3.48 eV. The synthesized material is crystalline, with an average crystallite size of 2.51 nm. The photocatalytic …
Published in Journal of Polymer & Composites · Vol. 9, Issue 1, 2021 · pp. 13–27 Read article
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Performance Improvement of Nano Field Effect Transistor Based on Zinc Oxide Semiconducting Materials – a Critical Analysis
Abstract: New semiconductor materials and new shapes for contemporary nanostructured semiconductor devices, like nanowires, have been researched as a result of advancements in transistor technology. Because of their unique electrical, photonic, and sensing capabilities, nanowires (NWs) constructed of various semiconductor material systems (gallium arsenide, zinc oxide, etc.) have been the subject of intense research over the past 20 years. Due to its distinctive properties, including high electron mobility, high crystalline quality, …
Published in Journal of Polymer & Composites · Vol. 12, Issue 2, 2024 · pp. 99–107 Read article
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Synthesis and Characterization of In2S3 Nanoflake Thin Film for Photosensor Applications
Abstract: Indium sulphide (In2S3) thin films in the form of nanoflakes are synthesized by using chemical vapour deposition method on glass substrate with the intension to test its photosensor applications. These as deposited nanoflake thin films are characterized for physicochemical properties using X-ray diffraction (XRD) pattern, energy dispersive X-ray (EDAX) analysis,scanning electron microscopy (SEM) while optoelectronic properties were studied using optical and electrical characteristics obtained through UV-Vis transmission spectroscopy and I-V …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 4, Issue 3, 2017 · pp. 21–26 Read article
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Effect of Annealling on Optical Band Gap of Fe2O3 Thin Films on Amorphos Transparent Glass Substrate by Spray Pyrolysis Method
Abstract: The Fe 2 O 3 thin film has widely used photo-electrochemical cells. In this paper, the optical properties like band gap of thin films is depend on annealed temperature at 100 o C and 200 o C was discussed. The optical property of Fe 2 O 3 are studied by UV- Vis spectroscopy .The optical band gap decreased after increasing annealing temperature. The refractive index of Fe 2 O 3 …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 2, 2023 · pp. 25–29 Read article
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Fabrication, Interfacial Characterization, and Superparamagnetic Properties of Fe₃O₄@γ-Fe₂O₃ Core/Shell Nanoparticle-Reinforced Chitosan Biopolymer Composites
Abstract: Magnetite/maghemite core/shell nanoparticles were prepared by alkaline co-precipitation of Fe(II) and Fe(III) precursors followed by controlled thermal oxidation at 350 °C and subsequently incorporated into chitosan at 1, 3, and 5 wt% loadings by solution casting. The resulting films were evaluated by X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), high-resolution transmission electron microscopy (HR-TEM), vibrating-sample magnetometry (VSM), thermogravimetric analysis (TGA), and tensile testing. XRD showed the characteristic cubic spinel reflections …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article
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Impact of Sol–Gel Processing on Dielectric and Energy Storage Properties of BaTiO3 Nanoceramics
Abstract: Barium titanate (BaTiO3) is a widely studied ferroelectric material because of its high dielectric permittivity and strong potential for electrostatic energy storage applications. In this study, BaTiO3 nanoceramics were synthesized using a controlled sol–gel processing route to investigate the influence of synthesis conditions on their dielectric relaxation and energy storage performance. The synthesized powders were calcined and subsequently sintered at temperatures ranging from 1100°C to 1300°C. Structural analysis using X-ray …
Published in Research & Reviews : Journal of Physics · Vol. 15, Issue 2, 2026 · pp. 11–25 Read article
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Role of Solvent on the Synthesis Structure of Zinc Oxide Nanoparticles
Abstract: Zinc oxide nanoparticles are synthesized by simple precipitation method in two different solvents, i.e., in distilled water and methanol. The zinc chloride and sodium hydroxide pellets are used as reactant precursors in both cases. The authors have analyzed the effect of solvents on crystal size and structure of zinc oxide nanoparticles. The samples were characterized by X-ray Diffraction (XRD) and UV-Vis spectroscopic techniques. The high absorption peak for zinc oxide …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 17, Issue 1, 2015 · pp. 42–45 Read article