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55 articles for “crystallite size”
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SnO2 Nanoparticles: Preparation, Characterization and Humidity Sensor Application
Abstract: The microwave-assisted synthesis method is used to prepare SnO2 nanoparticles for the application of humidity sensor, because of oxygen vacancy in the lattice. Microwave-assisted method is very simple, low cost and rapid heating method. Room temperature ionic liquids and tin source were used in the reaction as precursors. The obtained SnO2 nanoparticles were characterized by X-ray diffractometer, particle size analyser, Fourier transform infrared spectroscope, and thermo gravimetric-differential thermal analyser. The …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 6, Issue 2, 2016 · pp. 29–35 Read article
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A New Approach of Synthesis Fe-Substituted Bi-2223 Superconductors
Abstract: Generally, the Bismuth based high temperature superconductors are utilizing in three phases as Bi-2201, Bi-2212 and Bi-2223. These have different transition temperature according to superconducting phase. Here, we studied about Bi-2223 phase by using complex Bi2Sr2Can-1 (Cu1-xFex)3O10+δ where n = 3. In this complex, we has been doped iron in Coper (Cu) site (x = 0.07%). This sample was prepared by solid state reaction method. The planetary Ball mill was …
Published in Research & Reviews : Journal of Physics · Vol. 10, Issue 3, 2021 · pp. 22–29 Read article
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Study of Size Controllable Synthesis of Indium Tin Oxide Nanoparticles and Their Different Characterizations
Abstract: Nanocrystalline indium oxide powders were prepared by combustion synthesis. The changes of nanostructure caused by material processing were studied using X-ray powder diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and Brummer Emette teller analysis (BET). The stoichiometric composition of the starting indium tin oxide powder (cubic in traces) induced phase transitions to high temperature. We found that the phase transition to ITO was initiated at the …
Published in Research & Reviews : Journal of Physics · Vol. 1, Issue 2, 2012 · pp. 9–18 Read article
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Sonochemical Synthesis and Photo-Catalytic Study of Cd Doped Znse Nanoparticles
Abstract: Cd doped ZnSe nanoparticles have been successfully synthesized with sonochemical process by reacting high purity acetates and sodium selenosulphate at 343 K. The size of nanoparticles was calculated by using powder XRD. It shows the crystalline size ranging between 35.3 nm to 45.44 nm. XRD further shows that ZnSe nanocrystallites are polycrystalline in nature and belong to the hexagonal phase. SEM shows that the particles are spherical in shape. Effect …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 17, Issue 1, 2015 · pp. 32–41 Read article
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Optimization of gas sensitivity of CuO/carbon composites with carbon particles synthesized from acacia auriculiformis branches
Abstract: Carbon particles fabricated from the core of acacia tree branches were utilized to synthesize CuO/carbon composite films. The gas sensing properties of these films grown on glass substrates using the doctor blade method were measured in 1000 ppm of methanol vapor at the room temperature. All the films were annealed at 75 0C for 1 hour in air. The structure, the optical band gap and the surface morphology of the …
Published in International Journal of Membranes · Vol. 1, Issue 1, 2024 · pp. 22–30 Read article
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Synthesis and Characterization of VO 2+ doped SrMg 2 (PO 4 ) 2 Nanopowder by Solid State Reaction technique suitable for White LED material
Abstract: VO2+ doped SrMg2(PO4)2 nanopowder was synthesized by using solid state reaction (SSR) technique. Various experimental techniques have been performed on prepared sample. XRD analysis has revealed that prepared nanopowder is in monoclinic phase. The average crystallite size, micro strain and dislocation density evaluated and make an analogy with W-H plot method. SEM micrographs shows that agglomerated stone like structure and EDS spectrum shows elemental compositions of synthesized sample. FTIR spectrum …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 95–110 Read article
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Influence of Gd Doping in Structural, Morphological and Optical Properties of Zno Nanostructures Synthesised Via Sol-Gel Processes
Abstract: In this study, nanocrystalline Zn1-xGdx (x=0.0 and 0.03) samples were synthesised via the Sol-gel combustion process. An array of analytical techniques was employed to examine the prepared samples to determine their different physical features. For both pristine and Gd-doped samples, the crystal symmetry is hexagonal with the P63mc space group which is verified via the Rietveld refinement analysis of X-ray diffraction (XRD) data. The atoms' bond length Zn-O and bond …
Published in Journal of Polymer & Composites · Vol. 12, Issue 4, 2024 · pp. 219–225 Read article
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Raman Spectroscopy for The Determination of Relative Crystallinity of Carbon Fibers
Abstract: Analogous to X-ray diffraction technique, the light scattering technique discovered by Sir CV Raman has great potential in quantifying the crystallinity of new materials, like the highly crystalline pitch based carbon fibers (NX90 and NX100). For comparison the Raman spectra of polyacrylonitrile based carbon fibers (T700SC) were also recorded. From the Raman spectral analysis, it was found that the pitch based carbon fibers exhibit far far higher degree of crystallinity …
Published in International Journal of Crystalline Materials · Vol. 1, Issue 1, 2024 · pp. 30–38 Read article
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Synthesis and Characterization of Sustainable, Low-Cost, Biomass-Derived Carbon Films from Hevea Brasiliensis (Rubber) Wood for Environmentally Friendly Gas Sensors with Enhanced Selectivity and Sensitivity to Polar Vapors and Hazardous Gases
Abstract: Hevea brasiliensis (rubber) wood sawdust was utilized to fabricate carbon gas sensors for detecting 1000 ppm of ethanol, methanol, acetone, carbon dioxide, and ammonia gases. The carbon particles were prepared by phosphoric acid impregnation followed by thermal activation and then fabricated into films on conductive and non-conductive substrates using the doctor blade method. X-ray diffraction (XRD) analysis revealed distinct graphitic features with peaks at the (002) and (100) planes, indicating …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 12, Issue 1, 2025 · pp. 22–36 Read article
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Facile Synthesis and Characterization of Cd²⁺ Doped NiAl₂O₄ Nanoparticles for Advanced Polymer Composite Integration
Abstract: Ni1-xCdxAl2O4, where 0 ≤ x ≤ 0.5, was successfully synthesized using the chemical co-precipitation technique, a scalable and cost-effective route suitable for composite material applications. X-ray diffraction (XRD) analysis revealed a crystalline cubic spinel structure for the resulting nanoparticles, with determined crystallite sizes ranging from 36 to 12 nm for NiAl2O4 and Cd-doped NiAl2O4. The respective band gaps for the materials were found to be 3.51 and 4.18 eV. Infrared …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 59–72 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Combustion Synthesis and Comprehensive Characterization of Pure and Ni-Doped CuFe₂O₄ Nanoparticles for Functional Composite Applications
Abstract: The CuFe2-xNixO4 (x = 0, 0.1, 0.3, and 0.5) nanoparticles were synthesized using a combustion method and comprehensively characterized to understand their suitability for polymer-based composite applications. X-ray diffraction confirmed the formation of a single-phase spinel ferrite structure with crystallite sizes of 20–30 nm. Energy-dispersive X-ray spectroscopy verified the successful incorporation of Ni ions into the CuFe₂O₄ lattice, while FE-SEM analysis revealed uniformly dispersed nanoscale particles desirable for composite reinforcement. …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1–11 Read article
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Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material
Abstract: With the enlargement of flexibility and suitability in material industries, high-performance thermal management materials are demanded with high thermal conductivity and electrical insulation are growing. In recent years, graphene has received a numerous focus from science community due to its high thermal conductivity and electrical insulation. Fabrication of light weight graphene and its derivatives as graphene Oxide (GO) and reduced graphene oxide (rGO) via facile processing method is yet a …
Published in Journal of Polymer & Composites · Vol. 12, Issue 9, 2024 Read article
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Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material
Abstract: With the enlargement of flexibility and suitability in material industries, high-performance thermal management materials are demanded with high thermal conductivity and electrical insulation are growing. In recent years, graphene has received a numerous focus from science community due to its high thermal conductivity and electrical insulation. Fabrication of light weight graphene and its derivatives as graphene Oxide (GO) and reduced graphene oxide (rGO) via facile processing method is yet a …
Published in Journal of Polymer & Composites · Vol. 12, Issue 5, 2024 · pp. 25–36 Read article
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Structural, Optical, Surface, and Gas-Sensing Properties of rGO/Sn1–xZnxO₂ Nanocomposites
Abstract: rGO/Sn₁–ₓZnₓO₂ nanocomposites with x = 0.00–0.75 were synthesized by sol–gel auto-combustion followed by wet impregnation with reduced graphene oxide. The adopted synthesis route enabled homogeneous Zn incorporation into the SnO₂ matrix and uniform distribution of rGO, leading to improved structural integrity and interfacial contact between the two components. XRD confirmed a dominant tetragonal cassiterite SnO₂ structure, while FTIR, FESEM, EDS, UV–visible, and BET analyses verified oxide–rGO coupling, Zn-dependent structural modification, …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 · pp. 429–452 Read article
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Application of Polypyrrole/Lead Sulphide Nanocomposite in UV Light Assisted Photocatalysis and Gas Sensing
Abstract: The synthesis of ppy/lead sulphide nanocomposite was done using the co-precipitation method. The synthesized ppy/leadsulphide nanocomposite was characterized using Transmission Electron Microscopy (TEM), Selected Area Electron Diffraction (SAED), X-Ray Powder Defraction (XRD), Fourier Transformation Infra-Red Spectroscopy (FTIR), UV-Vis Spectroscopy techniques. The optical bandgap of the synthesized ppy/lead sulphide nanocomposite was observed to be 3.48 eV. The synthesized material is crystalline, with an average crystallite size of 2.51 nm. The photocatalytic …
Published in Journal of Polymer & Composites · Vol. 9, Issue 1, 2021 · pp. 13–27 Read article
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Synthesis and Characterization of In2S3 Nanoflake Thin Film for Photosensor Applications
Abstract: Indium sulphide (In2S3) thin films in the form of nanoflakes are synthesized by using chemical vapour deposition method on glass substrate with the intension to test its photosensor applications. These as deposited nanoflake thin films are characterized for physicochemical properties using X-ray diffraction (XRD) pattern, energy dispersive X-ray (EDAX) analysis,scanning electron microscopy (SEM) while optoelectronic properties were studied using optical and electrical characteristics obtained through UV-Vis transmission spectroscopy and I-V …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 4, Issue 3, 2017 · pp. 21–26 Read article
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Effect of Annealling on Optical Band Gap of Fe2O3 Thin Films on Amorphos Transparent Glass Substrate by Spray Pyrolysis Method
Abstract: The Fe 2 O 3 thin film has widely used photo-electrochemical cells. In this paper, the optical properties like band gap of thin films is depend on annealed temperature at 100 o C and 200 o C was discussed. The optical property of Fe 2 O 3 are studied by UV- Vis spectroscopy .The optical band gap decreased after increasing annealing temperature. The refractive index of Fe 2 O 3 …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 10, Issue 2, 2023 · pp. 25–29 Read article
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Crystallization Kinetics and Morphological Shifts in Polylactic Acid/Nanocellulose Blends Under Isothermal Melt Conditions
Abstract: The great potential of polylactic acid as a sustainable biopolymer for packaging, biomedical materials, and additive manufacturing, polylactic acid's slow crystallization kinetics during melt processing causes it to be poorly crystallized, thermally weak, and mechanically underperforming. Crystallization models of PLA/nanocellulose blends have been limited to isothermal melt crystallization kinetics and the resulting morphological changes. The phenomena discussed in this work are systematically explored by melt compounding of polylactic acid with …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article
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Fabrication, Interfacial Characterization, and Superparamagnetic Properties of Fe₃O₄@γ-Fe₂O₃ Core/Shell Nanoparticle-Reinforced Chitosan Biopolymer Composites
Abstract: Magnetite/maghemite core/shell nanoparticles were prepared by alkaline co-precipitation of Fe(II) and Fe(III) precursors followed by controlled thermal oxidation at 350 °C and subsequently incorporated into chitosan at 1, 3, and 5 wt% loadings by solution casting. The resulting films were evaluated by X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), high-resolution transmission electron microscopy (HR-TEM), vibrating-sample magnetometry (VSM), thermogravimetric analysis (TGA), and tensile testing. XRD showed the characteristic cubic spinel reflections …
Published in Journal of Polymer & Composites · Vol. 14, Issue 4, 2026 Read article