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620 articles for “Subtractive Synthesis”
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Synthesis, Characterization of New Imidazolidin-4-One Containing Azo Compound Derived from Acetylacetone as Antibacterial and Antioxidant Agents
Abstract: In the present study, new derivatives of imidazolidine-4-one was prepared. Which involved reactions to diazonium salt of o-methoxy aniline with acetylacetone in the presence of sodium hydroxide, and isolating the azo compound as a brown precipitate. The azo diketone reacts efficiently with aromatic amine derivatives to produce Schiff bases as a light yellow and dark brown precipitates, and from this Schiff bases three derivatives of imidazolidine-4-one was prepared by reacting …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 17, Issue 1, 2026 · pp. 94–114 Read article
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Green Synthesis and Functional Evaluation of Ag–Polypyrrole/TeO2 Nanocomposites for Advanced Electronic Applications
Abstract: Ag–PPy/TeO₂ nanocomposites with TeO₂ loadings ranging from 2% to 10% were synthesized using an in-situ chemical polymerization method. Green tea extract, rich in phytochemicals, acted as both a reducing and stabilizing agent to facilitate the formation of metal oxide nanoparticles. The structural and morphological characteristics of the nanocomposites were analyzed using FTIR, PXRD, and SEM techniques. FTIR confirmed the successful integration of Ag, TeO₂, and PPy functional groups. PXRD patterns …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 64–76 Read article
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Synthesis and Spectral Characterization of Complexes Tin(II) With 4-Nitrophenol
Abstract: Tin(II)4-nitrophenoxide complexes with the formulas SnCl(OC₆H₄NO₂-4) and Sn(OC₆H₄NO₂-4)₂ were prepared through the reaction of stannous chloride (SnCl₂) with 4-nitrophenol (HOC₆H₄NO₂-4) in 1:1 and 1:2 molar ratios, respectively. The reaction was performed in tetrahydrofuran (THF) with diethylamine serving as the base. The resulting compounds were characterized through elemental analysis, determination of molecular weight, molar conductance measurements, and spectroscopic methods including IR and ¹H NMR spectroscopy. Current investigations are directed toward assessing …
Published in International Journal of Advance in Molecular Engineering · Vol. 4, Issue 1, 2026 · pp. 22–26 Read article
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Synthesis of Glass Fiber Reinforced Polymer Composites Incorporating MWCNTS and Graphene: A Study on Dynamic Mechanical Behavior and Cole–Cole Representation
Abstract: Glass fiber reinforced polymer (GFRP) composites were fabricated using multi-walled carbon nanotubes (MWCNTs) and graphene as nanofillers through the hand lay-up technique. Two sets of composites were prepared by incorporating MWCNTs and graphene separately into the epoxy resin matrix at varying weight percentages (2%, 4%, 6%, 8%, and 10%). Mechanical and viscoelastic properties were evaluated following ASTM standards, and Dynamic Mechanical Analysis (DMA) was performed to study their mechanical and …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1411–1403 Read article
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Polymer Composite-Assisted Crystal Engineering for Drug Synthesis and Property Control through Solid Solutions and Co-Crystals
Abstract: The long-standing problem of low aqueous solubility, which affects about 90% of all new drug molecules under development, requires an immediate need for alternative approaches apart from the usual practice of crystallization. Polymer-composite-assisted crystal engineering is a novel technique for overcoming the aforementioned problem. This involves the addition of accepted pharmaceutical polymers, such as HPMC, PVP, PEG, and Eudragit copolymers in a single process, which can promote nucleation, stabilize the …
Published in Journal of Polymer & Composites · Vol. 14, Issue 3, 2026 · pp. 172–189 Read article
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Intelligent Electromagnetic Synthesis: An AI-Driven IoT Framework for Adaptive Antenna Design in Missile Navigation
Abstract: The rapid evolution of hypersonic and long-range tactical missile systems necessitates antenna architecture capable of maintaining robust communication links under extreme thermal, mechanical, and signal-jamming environments. Traditional antenna design methodologies often relying on iterative simulation cycles and static optimization are increasingly insufficient for the real-time requirements of modern aerospace navigation. This paper proposes an AI-driven, IoT- integrated framework that facilitates autonomous antenna design and performance optimization. By deploying a distributed …
Published in International Journal of Radio Frequency Innovations · Vol. 4, Issue 1, 2026 Read article
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Synthesis and Evaluation of MgO-Supported Activated Carbon for Carbon dioxide Capture
Abstract: Carbon dioxide (CO₂) capture has emerged as a critical strategy for mitigating greenhouse gas emissions and addressing global climate change. In this study, a series of MgO-supported activated carbon adsorbents containing 2, 4, 6, 8, and 10 wt% MgO were successfully synthesized using the impregnation method to evaluate their CO₂ adsorption performance. The structural, chemical, and surface properties of the prepared materials were characterized using powder X-ray diffraction (PXRD), Fourier-transform …
Published in Journal of Catalyst & Catalysis · Vol. 13, Issue 3, 2026 · pp. 53–57 Read article
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Novel 1,3,4-Thiadiazole Derivatives: Design, Synthesis, Characterization and Anticancer Evaluation – A Review
Abstract: Cancer remains one of the leading causes of mortality worldwide despite significant advances in diagnosis and treatment. The clinical usefulness of many anticancer drugs is often restricted by toxicity, poor selectivity, and the emergence of drug resistance. These limitations have encouraged the search for novel heterocyclic compounds with improved therapeutic efficacy and safety. Among these, the 1,3,4-thiadiazole scaffold has gained considerable attention because of its favorable physicochemical characteristics, metabolic stability, …
Published in Research & Reviews: A Journal of Drug Design & Discovery · Vol. 13, Issue 2, 2026 · pp. 42–49 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis Read article
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Synthesis, Characterization, and Biomedical Applications of a Silver Nanoparticle-Coated Chitosan–Fucoidan–Polymer Nanocomposite Loaded with Persea americana Leaf Extract
Abstract: Consuming a natural composite of Persea americana (Avocado) leaf extract and a chitosan and fucoidan form a biodegradable biopolymer matrix–polymer nanocomposite with biomedical applications, this study explored a potential therapeutic method. GC–MS and UV spectroscopy were used to describe the aqueous leaf extract, which was verified by phytochemical screening to contain flavonoids, tannins, phenols, terpenoids, and alkaloids. The chitosan–fucoidan biodegradable polymer matrix served as a biocompatible stabilizing and encapsulating carrier …
Published in Journal of Polymer & Composites · Vol. 14, Issue 5, 2026 · pp. 130–148 Read article
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Synthesis and Immobilization of N-doped Titanium Dioxide for Degradation of Amaranth Dye under Visible Light Irradiation from Light Emitting Diodes
Abstract: Titanium dioxide photocatalysis has a great potential as green and sustainable technology to treat pollutants present in water. In the present study, N-TiO2 (nitrogen doped titanium dioxide)photocatalyst was prepared by wet method using titanium tetra iso-propoxide and NH3. The calcination of the prepared photocatalyst was performed at different temperatures. The prepared catalyst was characterized by DRS, FE SEM and TEM. The N-TiO2 was immobilized on the surface of the quartz …
Published in Emerging Trends in Chemical Engineering · Vol. 3, Issue 2, 2016 · pp. 11–17 Read article
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Synthesis of Biodiesel with Methanol Recovery in Reactive Distillation
Abstract: In the present study, biodiesel was synthesized from waste vegetable oil, methanol and catalyst. The present work investigates the use of reactive distillation for continuous production and separation of biodiesel with recovery of excess methanol as top product of acceptable purity. In order to determine the best conditions for biodiesel production by reactive distillation, process parameters such as molar ratio of oil to alcohol, reaction temperature, catalyst concentration (0.5–1.5 wt …
Published in Emerging Trends in Chemical Engineering · Vol. 3, Issue 1, 2016 · pp. 26–31 Read article
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Application of Ultrasound for Synthesis of Biodiesel
Abstract: The aim of study is to synthesize a biodiesel from soybean oil using ultrasonic process. At present, biodiesel is produced in batch reactors in which the required energy is provided by heating by mechanical mixing. Alternatively, ultrasonic processing is an effective way to attain required mixing providing the necessary activation energy. Ultrasonic is a very desirable tool for producing biodiesel from vegetable oil and animal fats, because it lowers the …
Published in Emerging Trends in Chemical Engineering · Vol. 2, Issue 1, 2015 · pp. 1–8 Read article
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Synthesis of new heterocyclic compounds containing nitrogen, sulphur and study their biological activity
Abstract: Several substituted pyridines with brominated coumarin and with other substituents were achieved by condensing brominated coumarin IV with 4-methoxybenzaldehyde in basic solution forming α,β-unsaturated ketone II. Hantzsch reaction of this ketone with β-ketoester to provide precursor substituted pyridines. The Hantzsch reaction product was subjected to different reactions. The other targeted heterocyclic compound was obtained by reaction of α,β-unsaturated ketone II with hydrazine carbothioamide to give substituted pyrazole with brominated coumarin, …
Published in Emerging Trends in Chemical Engineering · Vol. 8, Issue 3, 2021 · pp. 8–16 Read article
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Use of Modified and Unmodified Calcium Oxide from Bio-resources as Heterogeneous Transesterification Catalyst for Biodiesel Synthesis: A Review
Abstract: Metal oxides have been widely used to catalyze various types of organic reaction, whatever supported or nonsupport metal oxide catalysts (supported with metal, mixed oxides and acids such as sulphoric acid). Calcium oxide is one of the most metal oxides used as heterogeneous catalysts; due to its favorable properties such as high activity, availability, low cost, and easily separated, as well as environmental friendly. Calcium oxide whether laboratory, prepared from …
Published in Emerging Trends in Chemical Engineering · Vol. 9, Issue 3, 2022 · pp. 30–34 Read article
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Synthesis and characterization of mesoporous silica supported Pt catalysts for Decalin dehydrogenation
Abstract: Hydrogen, potentially very attractive energy source as its combustion forms only water in addition to energy. Hydrogen is the cleanest source of fuel. Decalin consists of considerable high hydrogen contents of 7.3 wt% and 64.8 kg H2 /m3 is an excellent mobile storage source for hydrogen. In this work, SBA-15 and carbon modified SBA-15 supported 1wt% Pt catalysts were synthesized and characterized for vapour phase dehydrogenation of decalin. About 154 …
Published in Journal of Catalyst & Catalysis · Vol. 5, Issue 3, 2018 · pp. 12–21 Read article
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Synthesis of Isoamyl Acetate (Banana oil) Using Fly Ash Supported Nano Crystalline Solid Acid Catalyst
Abstract: A novel fly ash supported solid acid catalyst (HClO4/FA) has been synthesized by using F-type fly ash and HClO4 as precursor. The variation of surface and physicochemical properties of the fly ash by activation methods resulted in improved acidity and therefore, catalytic activity for acid catalyzed esterification reactions. The HClO4/FA catalyst was characterized by XRF, XRD, FT-IR, SEM and BET surface area. The catalytic performance of HClO4/FA catalyst was evaluated …
Published in Journal of Catalyst & Catalysis · Vol. 4, Issue 2, 2017 · pp. 1–8 Read article
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Basic Urea and Ammonia Synthesis
Abstract: AbstractIndian population has continued to grow at the rate of 1.2% per year. This population explosion demands for around 263 million tonne of food grain per annum. From the present level of production of some 241 million tonnes (2012–2013); it is clear that an adequate quantity of fertilizer has to be made available. Urea (NH2CONH2) and ammonia (NH3) are of great importance to the agriculture industry as nitrogen-rich fertilizer. This …
Published in Journal of Catalyst & Catalysis · Vol. 3, Issue 2, 2016 · pp. 7–13 Read article
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Effect of catalyst and methanol on synthesis of methyl esters from used cooking oil
Abstract: Due to depletion in the fossil fuels and the increase of energy usage, the rapid depletion of fossil fuel is accelerated. Therefore, using renewable energy is a key solution to the problem of fossil fuel depletion. There are several resources of renewable energy like geothermal energy, solar energy, and biofuels. Biodiesel is a fatty acid alkyl ester made from renewable resources such as used cooking oil. The attractiveness of biodiesel …
Published in Journal of Catalyst & Catalysis · Vol. 8, Issue 1, 2021 · pp. 42–51 Read article
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Saccharomyces exiguus Single Cell Protein Synthesis in Ethanol
Abstract: At present, foods of animal and vegetable origin have two fundamental aspects of resolving the nutritional value for human and animal consumption. As well as the cost of agricultural production with the necessary inputs in a sustainability scheme. Consequently, there are other strategies for the generation of nutritional quality protein for consumption, such as the so-called protein of unicellular origin “single cell protein” (SCP), Saccharomyces exiguus is a precise example …
Published in Journal of Catalyst & Catalysis · Vol. 10, Issue 1, 2023 · pp. 22–27 Read article