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211 articles for “SEM (Scanning Electron Microscopy)”
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Studies on the preparation and characterization of TiO2 thin film
Abstract: Titanium dioxide thin film was deposited on the class substrate by using Ti(C10H14O5), and characterized by using X-Ray diffractometer (XRD) and scanning electron microscopy (SEM), SEM analysis was discussed for 350º C. FTIR analysis gives the vibrational modes of vibrations of the material. The diffraction plane is (101) and crystal size was as 50 nm. The morphological studies of the sample inferred that the size was nearly in micrometer due …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 8, Issue 3, 2018 · pp. 58–64 Read article
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Study of CdS/AZO/FTO, CdS/FTO and CdS Thin Films Deposited by Modified Double Layer Thermal Evaporation
Abstract: The CdS/AZO/FTO, CdS/FTO and CdS thin films were deposited by a modified double-layer vacuum evaporation technique. The 90 nm of double-layer CdS thin films were prepared with the bottom layer 50 nm thick and the upper one was 40 nm thick and respective substrate temperatures were 100oC and 70oC. The physical properties of thus prepared films were characterized using X-ray diffraction (XRD), UV-VIS-NIR spectrophotometer, Hall Effect Measurement System and Scanning …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 2, 2019 · pp. 56–63 Read article
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Substrates Effects on CdTe Thin Films Using Double Layer Thermal Evaporation
Abstract: The CdTe thin films are successfully deposited by a thermal evaporation method. In the CdTe/CdS/FTO glass and CdTe/CdS/AZO/FTO glass structures, modified double-layer thermal evaporation technique is applied for the preparation of CdTe thin films. The XRD analysis of CdTe thin films showed that the films are polycrystalline with a cubic structure. The scanning electron microscopy (SEM) image showed the homogeneous and uniform surface structure of the films. High conductivity of …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 9, Issue 2, 2019 · pp. 64–70 Read article
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Modified Solution Combustion Approach for Probing of Structural and Dielectric Properties of Sm3+ Doped GdAlO3 Nanoparticles
Abstract: A modified solution combustion approach was used in the preparation of nanosized Gd1xSmxAlO3 (x=1, 3, 5, 7, 9 mol%) using mixture of ODH and novel fuel E. tirucalli plant latex as fuels with corresponding metal nitrates. The structural morphology of synthesized and calcined powders are revealed using various analytical techniques such as Powder X-ray diffraction (PXRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR) and …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 10, Issue 1, 2020 · pp. 16–25 Read article
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Analytical Study on Humidity Sensing of Nanostructured Tin Oxide
Abstract: Nanocrystalline tin oxide powder was prepared by a mechanochemical method. The synthesised powder was characterised using X-ray diffraction (XRD) and scanning electron microscopy (SEM). XRD shows the crystalline nature of the synthesised material. The crystallite size was estimated using Debye–Scherrer equation and its minimum value was 9 nm. Surface morphologies of the sensing pellets were investigated using SEM. Pellets as well as thick films were used as sensing elements for …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 10, Issue 3, 2020 · pp. 1–7 Read article
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Synthesis and Characterization of europium doped barium magnesium aluminate (BaMgAl 10 O 17 :Eu 2+ ) and lanthanum yttrium phosphate (LaYPO 4 :Eu 2+ ) nanophosphors
Abstract: Over a decade after adapting the definition and long-term vision for nanotechnology, the programs around the world have achieved remarkable results regarding scientific discoveries that span better understanding of the smallest living structures and functions of matter at the nanoscale. The current scenario of emerging field of luminescent material (phosphor) has a great interest in optoelectronics and solid-state lighting applications for industrial purpose. In the present work, we have reported, …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 23, Issue 2, 2021 · pp. 20–39 Read article
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Development of PLLA-based Bio Inks Applicable in the Medical Field
Abstract: Some synthetic polymers, such as Poly (L-lactic acid) (PLLA), are interesting to use in 3D bioprinting because they can have adaptable and resilient mechanical properties that also facilitate bioprinting processes. PLLA is a biocompatible polymer which makes it very interesting for medical applications, it is an aliphatic polyester obtained from α-hydroxy acids in different ways: ring-opening polymerization, and direct polycondensation. The use of one path over the other depends on …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 24, Issue 2, 2022 · pp. 38–46 Read article
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Isolation, Identification and Characterization of Bdellovibrio sp. from Soil and its Antibiotic Potential against Selected Bacterial Pathogens
Abstract: Bdellovibrio and Like Organisms (BALOs) are the world's smallest Gram-negative, highly motile delta-proteobacterial predators generally found in diverse environmental niches such as soil, seawater, sewage, bio films, freshwater, gastro intestinal tract of animals and in association with plant roots. These small bacteria attack gram negative bacterial strains attaching to the outer membrane and consuming the prey extracellularly (epibiotic predation) or penetrating their periplasm (periplasmic predation). Bdellovibrio exovorus MPR11 (Accession No. …
Published in Research and Reviews : A Journal of Life Sciences · Vol. 9, Issue 1, 2019 · pp. 119–130 Read article
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Sonochemical Synthesis of SrBaFexMo2-xO6 (x=1.0, 1.1, 1.3 and 1.4) Double Perovskites: Characterization and Magnetic Properties
Abstract: This work investigates ultrasound assisted synthesis, characterization and magnetic properties of SrBaFexMo2-xO6 (x=1.0, 1.1, 1.3 and 1.4) double perovskites. X-ray diffraction (XRD) analysis confirmed proposed that samples are in single phase. It was found that lattice constants decrease with increase in composition x. Morphology of all samples was examined by Scanning Electron Microscopy (SEM) images. Energy Dispersive X-ray Spectroscopy (EDS) data confirmed purity and nonexistence of foreign elements in prepared …
Published in Research & Reviews : Journal of Physics · Vol. 7, Issue 2, 2018 · pp. 8–17 Read article
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Study of Calcium Oxide Nanoparticles Synthesized by Solvothermal Method
Abstract: Calcium oxide (CaO) nanoparticles have been synthesized by simple solvothermal method using a domestic microwave oven. The reaction of calcium acetate with urea in ethylene glycol and by adding different mole% of manganese acetate as dopant was studied. The structural and optical properties of the proposed nanoparticles were investigated. The structural properties were characterized by powder X-ray diffraction (PXRD) and scanning electron microscopy (SEM) analysis. The average particle size of …
Published in Research & Reviews : Journal of Physics · Vol. 8, Issue 3, 2019 · pp. 14–19 Read article
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Rapid Biosynthesis of Silver Nanoparticles of Flower-like Morphology from the Root Extract of Saussurea lappa
Abstract: With the emergence of nanomedicine, nanobiotechnology, and nanopharmacotherapeutics, there has been a rising demand of nanomaterials. Silver nanoparticles (AgNPs) finds immense applications for drug delivery, biomedical sciences, catalysis, etc. Numerous industries are at present synthesizing therapeutic AgNPs to meet the global demand. By using chemical methods, which are very cost-effective to produce these materials, are quite hazardous, environment polluting, produce harmful byproducts, and have several other alarming aspects. The extract …
Published in Research & Reviews: A Journal of Pharmacognosy · Vol. 5, Issue 1, 2018 · pp. 20–24 Read article
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Monophase Solution for Enhancing Solubility and Dissolution of Ezetimibe by Spray Dried Microparticle
Abstract: The aim of the present study was to improve the solubility and dissolution rate of Ezetimibe by preparing crystals by spray drying technique using Isopropyl alcohol (IPA) and water as solvent system. Ezetimibe crystals were produced by spray drying using IPA as solvent to enhance solubility and dissolution rate. The prepared crystals were evaluated for solubility and in vitro dissolution. The prepared formulations were characterized by differential scanning calorimetry (DSC), …
Published in Trends in Drug Delivery · Vol. 1, Issue 3, 2014 · pp. 30–36 Read article
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Crystal Defects and Their Characterization in Modern Materials Science
Abstract: The physical and chemical properties of crystalline solids are fundamentally dictated by deviations from structural perfection, known as crystal defects. From the point-scale vacancies that drive diffusion to the planar boundaries that determine mechanical strength, defects serve as the primary "tuning knobs" in material design. This review provides a comprehensive examination of point, line, and planar defects, exploring their formation energetics and their role in plastic deformation via crystallographic slip. …
Published in International Journal of Crystalline Materials · Vol. 3, Issue 1, 2026 · pp. 15–19 Read article
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Effects of Plasticizers on Structures of Chemical Functional Groups, Morphologies, Water Vapor Permeability, and Thermal Properties of HPMC/BW Biopolymer Films
Abstract: Food preservation is one of the fields that many researchers are interested in, especially in the epidemic period like COVID-19 today. The better food or agricultural products are preserved for a long time, the more it ensures social stability for state management related to food security for people. This paper introduces one kind of biopolymer films with investigation on effect of plasticizers to its characteristics. In order to produce biopolymers, …
Published in Journal of Polymer & Composites · Vol. 9, Issue 2, 2021 · pp. 10–20 Read article
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Effect of Hafnium on Nickel-Titanium based Thin Film Coating by DC/RF Magnetron Sputtering Technique
Abstract: Ni-Ti-Hf films as shape memory alloys were successfully prepared by magnetron sputtering technique using individual Ti, Ni and Hf targets. The hafnium content was varied from 6% to 30% and the required film composition was achieved by adjusting the power ratio to the targets. The as-deposited films were amorphous; a post deposition annealing was performed at 700 °C to crystallize the Ni-Ti-Hf films. Structural, compositional and phase-transformation studies were carried …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 2, Issue 3, 2012 · pp. 10–17 Read article
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Synthesis and Characterization of Amorphous Carbon Nanotube-Molybdenum Disulfide (ACNT-MoS2) Nanohybrids using Sodium Molybdate Dehydrate and L-Cysteine as Precursor
Abstract: The discovery of graphene makes the researcher interested towards the other two-dimensional material which has quite similar properties like graphene. Among them, MoS2 nanosheets haves extraordinary optoelectronic and physical properties. It has several applications in developing battery, sensor, optoelectronic device etc. On the other hand, amorphous carbon nanotube can be synthesized by using a low temperature chemical process. Due to the ease processing of amorphous carbon nanotube (ACNT), good optoelectronic …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 21, Issue 3, 2019 · pp. 41–47 Read article
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Biosynthesis of Zinc Oxide Nanoparticles and Their Revolutionary Impacts on Agroindustry: Review
Abstract: Nanotechnology is a new approach of science which provides alternative tool in many fields including agriculture. This comprehensive review focuses on the biosynthesis and characterization of zinc oxide nanoparticles (ZnO NPs), highlighting their vast potential in agroindustry applications. Unlike traditional physical and chemical methods, which are often costly, time-consuming, and involve hazardous materials, this review explores the promising biological synthesis routes, offering a more sustainable and eco-friendly alternative for producing …
Published in Nano Trends – A Journal of Nano Technology & Its Applications · Vol. 26, Issue 2, 2024 · pp. 33–50 Read article
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Multifunctional and Photocatalytic Properties of DyFeO₃/Dy₃Fe₅O₁₂ Biphasic Nanoparticles
Abstract: Rare-earth orthoferrites constitute a class of compounds that exhibit remarkable magnetic, optical, and electronic properties across a wide temperature range. In the present study, a dysprosium-based orthoferrite containing dual phases of DyFeO₃ perovskite and Dy₃Fe₅O₁₂ garnet was successfully synthesized via the co-precipitation technique. X-ray diffraction (XRD) analysis was employed to investigate the structural configuration of the synthesized material. The diffraction pattern confirmed the formation of a biphasic composite comprising orthorhombic …
Published in International Journal of Crystalline Materials · Vol. 2, Issue 2, 2025 · pp. 41–54 Read article
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article