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240 articles for “and XRD”
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Structural Modification of Sugarcane Bagasse using Alkaline, Acid, and Bleaching Pretreatments for Enhanced Yield of Poly (1→4)-β-D-glucopyranose (Cellulose) and Hemicellulose for Utilization as Biocomposites
Abstract: Sugarcane bagasse, a lignocellulosic byproduct generated in substantial quantities by the sugar industry, represents a promising feedstock for the sustainable production of enzymes and bio-based chemicals. Its high (1→4)-β-D-glucopyranose (cellulose) content, abundant availability, and low cost make it an ideal candidate for bioconversion processes. However, the inherent recalcitrance of bagasse, primarily due to its lignin-rich matrix, necessitates effective pretreatment strategies to enhance enzymatic digestibility. This study presents a comparative investigation …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 983–992 Read article
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Fabrication and Analysis of PBAT/Cyperus Rotundus Micro Crystalline Cellulose Biofilms for Food Packaging Applications
Abstract: Global plastic waste crisis has gained an increasing attention and many efforts have been made recently to develop biodegradable polymers as food packaging alternatives. Solution casting is used for fabrication and characterization of reinforced polybutylene adipate-co-terephthalate (PBAT) biofilm with Cyperus rotundus microcrystalline cellulose (CRC). PBAT-CRC biofilms with different CRC loadings (1%, and 2%) had been prepared and their structural, mechanical, thermal and morphological properties of fabricated biofilms were analyzed to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 591–599 Read article
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Design of a Geopolymer Based on Fly Ash and Metakaolin with a Solid, Liquid, and Powdered Alkaline Activator at High Temperatures
Abstract: In this work, the fresh and hardened properties of geopolymer concrete activated using solid, liquid, and powder alkaline activator systems, including fly ash and different amounts of metakaolin, are examined. Compressive and flexural strengths were assessed at 7 and 28 days in accordance with IS 516 (1959). Workability was evaluated using a slump test in accordance with IS 1199 (Part 2): 2018. At an ideal replacement level of 30%, the …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 712–726 Read article
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Polymeric Ion-Exchange Complexes of Carbomer for Taste Masking and Enhanced Drug Bioavailability: A Physicochemical and In Vivo Study
Abstract: Famotidine (FAM) was recognized as a crystalline powder that varies in color from white to pale yellow and possesses an extremely bitter flavor. This study aimed to conceal the unpleasant flavor of FAM through employing unconventional ion-exchange resins sourced from Carbomer polymer Evaluation (Carbopol 974P). We used FTIR, DSC, and XRD to look at the drug-resin combination in its hard form to learn more about its physical and chemical properties. …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 727–740 Read article
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Engineered Hybrid Nanoclay-Infused Nano-Polymers for Multifunctional Anti-Corrosive Coatings
Abstract: Polymer nanocomposites reinforced with layered nanofillers have emerged as an effective route to enhance structural stability in protective coating applications. Polymer–clay nanocomposites also provide a promising route to enhance mechanical robustness and environmental durability in coating systems. In this study, a hybrid epoxy–polyurethane (EPU) coating was reinforced using organo-modified montmorillonite (o-MMT) and layered double hydroxide intercalated with 2-mercaptobenzothiazole (LDH–MBT). Uniform dispersion and interfacial anchoring between the nanoclays and polymer chains …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 40–53 Read article
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Structure-Property-Process Relationships in BNNS-Modified PEEK Nanocomposites for High-Performance Applications
Abstract: This study reports the design and performance evaluation of boron nitride nanosheet (BNNS)-reinforced polyetheretherketone (PEEK) nanocomposites fabricated using melt compounding and high-temperature Fused Filament Fabrication (FFF). PEEK, a high-performance thermoplastic, was reinforced with BNNS at 0.5–5wt.% to enhance mechanical, thermal, and tribological functionalities for advanced engineering use. Composite filaments were extruded and printed using a modified Bambu Lab FFF printer. Mechanical testing revealed a peak tensile strength of 108 MPa …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 867–888 Read article
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Bioinspired Nanocomposite Bone Pins: Fabrication, Evaluation, and Suitability for Orthopedic Implant Applications
Abstract: Bone tissue engineering (BTE) requires scaffolds that mimic bone’s mineral–organic composition, offering mechanical strength, bioactivity, and degradation rates compatible with regeneration. Conventional metallic implants face corrosion and toxic ion release risks, while ceramics like hydroxyapatite (HAp) are bioactive but brittle. This study reports a multifunctional hybrid scaffold combining HAp for osteoconductivity; polycaprolactone (PCL) and collagen for flexibility and biocompatibility with sodium citrate for nanoparticle dispersion, ferrocene (Fc) for catalytic bioactivity; …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 526–540 Read article
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Tailoring The Electrochemical Interface of Graphene–Gd₂O₃ Nanocomposites for Advanced Energy Storage
Abstract: Graphene–Gd₂O₃ nanocomposites were synthesized by incorporating varying concentrations of reduced graphene oxide (rGO) into Gd₂O₃ using a straightforward room-temperature solution method. The composites were analyzed using various distinct characterization techniques, including X-ray diffraction (XRD), Fourier-transform infrared (FTIR) spectroscopy, Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). Electrochemical measurements, particularly cyclic voltammetry (CV), demonstrated that the incorporation of graphene significantly enhanced the electrochemical performance …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 369–388 Read article
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Activated Carbon Materials as Ideal Adsorbents for the Desulfurization of Fossil Fuels
Abstract: Removal of organosulfur compounds from diesel is of interest from scientific, social, economic, and environmental viewpoints. Production of clean fuel remains a primary goal of the petroleum refining industry. The reduction of sulfur content below stringent ppm levels in diesel fuels becomesincreasingly challenging due to the presence of sterically hindered sulfur compounds, such as 4,6- dialkyldibenzothiophenes, which are resistant to removal over conventional supported mixed sulfide hydrodesulfurization catalysts. Consequently, alternative …
Published in International Journal of Pollution: Prevention & Control · Vol. 4, Issue 1, 2026 · pp. 28–34 Read article
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Comparative Study of Structural, Optical, Morphological, and Magnetic Properties of BifeO3 Nanoparticles Synthesized Via Green and Chemical Methods
Abstract: BiFeO3 nanoparticles were synthesized via a green route using Strychnos nux-vomica leaf extract and a conventional chemical sol–gel method to study the effect of synthesis routes on their properties. XRD analysis confirmed phase-pure rhombohedral BiFeO3 for both samples. FTIR analysis was carried out to confirm the formation of the perovskite structure and to detect surface functional groups. FESEM analysis indicated a significant effect of phytochemicals in controlling particle growth and …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 1, 2026 · pp. 1–8 Read article
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Structure–Optical Property Correlation of Co-Doped TiO₂ and ZnO Nanofillers for Advanced Functional Composite Applications
Abstract: This study investigates the enhancement of the structural and optical properties of titanium dioxide (TiO₂) and zinc oxide (ZnO) nanoparticles through cobalt (Co) doping. Pristine TiO₂ and ZnO are widely studied metal oxides; however, their large band gaps and limited visible-light absorption restrict their performance in optoelectronic, photocatalytic, and environmental applications. Co doping is employed as an effective strategy to overcome these limitations by inducing band-gap narrowing, creating defect-related electronic …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1374–1394 Read article
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Nanostructured Catalysts for Sustainable CO2 Reduction: Advancing Green Chemistry and Polymer Composites
Abstract: This study provides a comprehensive analysis of advanced nanostructured catalysts designed to enhance the efficiency of artificial photosynthesis for sustainable fuel production. We systematically evaluated a range of nanomaterials—including metal oxides, plasmonic nanoparticles, and carbon-based composites—to determine their effectiveness in converting solar energy into storable chemical fuels. The catalysts were synthesized via sol-gel, hydrothermal, and green methods, and their properties were thoroughly characterized using XRD, SEM, TEM, UV-Vis spectroscopy, and …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 175–181 Read article
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Spin Coated Polyvinylidene Difluoride / Ionic Liquid Nanocomposite Thin Films with Enhanced Dielectric and Piezoelectric Properties
Abstract: This study introduces a novel approach to enhance the piezoelectric and dielectric properties of polyvinylidene difluoride (PVDF) by incorporating 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIM][BF₄]) ionic liquid via a spin-coating method— a processing route that has been rarely reported for PVDF/ionic liquid composites. Structural and morphological analyses using X-ray diffraction (XRD), Raman spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) confirm the successful integration of [BMIM][BF₄] into the PVDF matrix. The …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1190–1204 Read article
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Mn Doping–Induced Enhancement of Ethanol Gas Sensitivity in CuO/Cu₂O/Cu Composites
Abstract: A composite of CuO/Cu2O/Cu was synthesized by heating cupric acetate up to 600 °C for 2 hours in air. The properties of pure CuO films and CuO/Cu2O/Cu films were compared. Films were fabricated by the doctor blade method. Polyethylene glycol was used as a binder to prepare films. Mn was doped to composite to enhance the gas sensing properties. Compositions of Mn doped samples were confirmed using XRFS. According to …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 52–61 Read article
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Utilization of Treated Textile Dyeing Wastewater and GGBFS–Perlite Blends for Sustainable Cementitious Composite Development
Abstract: The increasing global demand for concrete critically intensifies the consumption of potable water, raising significant environmental concerns and depleting vital resources. Concurrently, the textile dyeing industry generates substantial volumes of wastewater, posing considerable disposal and pollution challenges. Our investigation explores a dual solution by utilizing treated textile dyeing wastewater as an alternative mixing water source, combined with ground granulated blast furnace slag (GGBFS) and perlite as supplementary cementitious materials (SCMs), …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 291–300 Read article
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High-Performance Carbon Nanotube-Reinforced Biodegradable Polymer Composites for Packaging
Abstract: The growing issues concerning the properties of petroleum-based plastics on the environment increased the demand for biodegradable alternatives and polylactic acid (PLA) is one of the most promising options available. However, its poor toughness, thermal resistance, and barrier properties limit broader applications in sustainable packaging. This study reports the fabrication and characterization of PLA-based nanocomposites reinforced with carbon nanotubes (CNTs) at varying loadings (0.1-2 wt.%). Structural analysis (FTIR, XRD) confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 183–194 Read article
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Development and Performance Evaluation of Polymer-Modified Geopolymer Composites Incorporating GGBS
Abstract: This research investigates the development and performance of geopolymer-based composite materials formulated using Ground Granulated Blast Furnace Slag (GGBS) as a reactive mineral component within an aluminosilicate polymer matrix. The study aims to create an eco-efficient and structurally sound inorganic polymer composite comparable to M35-grade concrete, produced entirely under ambient curing conditions. A series of mixes with varying GGBS replacement ratios (0–100%) was prepared, maintaining a constant binder content of …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1145–1165 Read article
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Comparative Study of Structural and Optical Properties of Bismuth Ferrite Nanoparticles for Photovoltaic Applications Synthesized via Different Sol-Gel Methods
Abstract: Pure multiferroic bismuth ferrite (BiFeO3) nanoparticles were successfully synthesized using an energy-efficient, low-temperature sol-gel method, comparing two distinct approaches: auto-combustion and non-auto-combustion. To ensure phase stability, the precursor solution's pH was strictly maintained between 1 and 2 using ammonia solution (NH4OH), while ethylene glycol (C2H6O2) was employed as a chelating agent for the Fe3+ and Bi3+ cations. All samples underwent a final annealing process at 500 °C to promote crystallization. …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 1, 2026 · pp. 83–94 Read article
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Water Chestnut Stem-Derived Biochar Supported AgNPs/AC-CTS-PVA Composite Gel for Wastewater Treatment and Potent Antibacterial Performance
Abstract: In the present study, green and efficient Ag-NPs functionalized activated carbon/chitosan-polyvinyl alcohol (AgNPs/AC-CTS-PVA) composite gel was successfully synthesized using water chestnut stem-derived biochar for wastewater treatment and antibacterial applications. The composite was characterized by FTIR, XRD, SEM-EDX, and TGA analyses, confirming the successful incorporation of crystalline Ag nanoparticles within the polymeric matrix and improved thermal stability. The material was tested regarding the removal of the dye of methylene blue (MB) …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1129–1144 Read article