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145 articles for “scanning electron microscopy”
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Fabrication and Analysis of PBAT/Cyperus Rotundus Micro Crystalline Cellulose Biofilms for Food Packaging Applications
Abstract: Global plastic waste crisis has gained an increasing attention and many efforts have been made recently to develop biodegradable polymers as food packaging alternatives. Solution casting is used for fabrication and characterization of reinforced polybutylene adipate-co-terephthalate (PBAT) biofilm with Cyperus rotundus microcrystalline cellulose (CRC). PBAT-CRC biofilms with different CRC loadings (1%, and 2%) had been prepared and their structural, mechanical, thermal and morphological properties of fabricated biofilms were analyzed to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 591–599 Read article
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A Study on Tensile Characterization of Polypropylene Reinforced with Recycled Epoxy Particles
Abstract: Polypropylene is a thermo plastic, tensile properties of polypropylene are crucial in the real world applications as they determine structural integrity and durability. Epoxy is a thermosetting plastic finds applications in various fields like aerospace, automobile, food packing etc. A major concern is the disposal of epoxy composites after their service life, since most of the waste is sent to landfills, causing land pollution and soil infertility. In this experimental …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 221–237 Read article
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Polymer Electrolyte Films Doped with Nanofillers ZnO: Electrochemical and Optical Investigations
Abstract: The electrochemical and optical characteristics of polymer composite electrolyte films doped with zinc oxide (ZnO) nanofillers are thoroughly examined in this work. Because of its superior film-forming capacity, flexibility, and ionic transport properties, poly(vinyl alcohol) (PVA) mixed with potassium iodide (KI) is used as the host polymer electrolyte. To investigate their effects on ionic conductivity, dielectric behavior, and optical transmission, ZnO nanoparticles are synthesized and added to the PVA–KI matrix …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 320–332 Read article
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Mechanical Characterization of Kevlar 49 and Pina Fiber Hybrid Composites
Abstract: The pursuit of sustainable yet high-performance materials has accelerated research into hybrid composites that combine synthetic and natural fibers. This study investigates the fabrication and characterization of a Kevlar 49/Pina fiber hybrid composite using epoxy resin as the matrix. Kevlar 49, known for its exceptional tensile strength and energy absorption, was employed as the face sheet material, while Pina fiber, a biodegradable reinforcement extracted from pineapple leaves, was incorporated as …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 301–316 Read article
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Characterization of Polyurethane at Multiple Scales for Erosion Mechanisms Under Sand Particle Impact
Abstract: Thin polyurethane layers have been widely used as erosion-resistant coatings on helicopter rotor blades such as UH-60 Black Hawk and Eurocopter SA 315. Published research has mainly focused on empirical studies that relate the mechanical properties such as rebound resilience and hardness of polyurethane to solid particle erosion resistance. However, polyurethane possesses phase mixing at multiple scales and thus sand particle erosion resistance depends also on the microstructure and the …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 13, Issue 1, 2026 · pp. 1–13 Read article
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Evaluating Fiber Volume Fraction and Defects in Fiber Reinforced Polymer Composites for T Joint applications
Abstract: Fiber-reinforced polymer (FRP) composites have been integral to industries such as aviation, aerospace, shipbuilding, and automotive due to their strength, durability, lightweight, and corrosion resistance. This study examines the production and microstructural analysis of polymer composites using FRP and manual lamination methods. While manual lamination is quick and economical, it relies on operator skill, resulting in low mechanical properties. Microstructure analysis via 3D optical and scanning electron microscopes revealed that …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1222–1235 Read article
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Grey Relational Analysis of Cuttlefish Bone Particles–Glass Fiber Reinforced Epoxy Composites
Abstract: This research examines the mechanical characteristics, water absorption performance, and thermal stability of epoxy composites reinforced with Cuttlefish Bone Particles (CFBP) and glass fibers. Composites were fabricated with varying CFBP contents (0%, 3%, 6%, 9%, and 12%) using an epoxy resin as the matrix material and glass fiber as the primary reinforcement. The experimental results revealed that the CFBP-0 composite (neat epoxy with glass fiber) exhibited the highest tensile strength, …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 239–246 Read article
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Mechanical and Thermal Performance of PETG Composites Reinforced with Short Carbon Fibers via Fused Filament Fabrication
Abstract: The study investigates the fabrication and characterization of polyethylene terephthalate glycol (PETG) composites reinforced with short carbon fibers (CF) using the fused filament fabrication (FFF) technique. Composite filaments with varying CF weight fractions (0, 5, 10, 15, and 20 wt%) were produced and evaluated for their mechanical, thermal, and morphological performance. The influence of CF reinforcement on tensile, flexural, and impact behavior was systematically examined, alongside thermal stability metrics including …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1219–1238 Read article
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Investigating The Influence of Sic Reinforcement on The Mechanical and Tribological Properties of PA12 Polymer Composites in SLS
Abstract: The study investigates the mechanical and tribological performance of neat PA12 polymer and SiC-reinforced PA12 polymer composites made via Selective Laser Sintering (SLS). To evaluate just how reinforcement has influence upon overall performance, we incorporated into the PA12 polymer matrix a constant amount of 5 wt.% of Silicon Carbide (SiC). Mechanical testing focused on both tensile and fatigue behavior and testers conducted it with a Servo-Hydraulic Multipurpose High-Capacity Fatigue Test …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 541–554 Read article
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Synthesis and Characterization of pH-Sensitive Poly (N-isopropylacrylamide-co-acrylic Acid) Hydrogels for Controlled Release of Doxorubicin
Abstract: pH-responsive polymeric hydrogels have attracted significant attention as intelligent biomaterials for site-specific and controlled drug delivery in cancer therapy due to their ability to respond to the acidic tumor microenvironment. In the present study, poly (N-isopropylacrylamide-co-acrylic acid) [P(NIPAM-co-AAc)] hydrogels were synthesized via free radical copolymerization and systematically characterized to evaluate their suitability for controlled delivery of doxorubicin, a widely used chemotherapeutic agent. The copolymer hydrogels were prepared using N-isopropylacrylamide and …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 449–458 Read article
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Material-Level Degradation of Magnetorheological Fluids Under Long-Term Cyclic Shear
Abstract: The long-term functional stability of magnetorheological fluids (MRF) remains a key limitation for their reliable use in adaptive systems and continuously operated magnetorheological devices. In this study, the intrinsic evolution of rheological properties in a commercial MRF (MRC-C1L) is systematically examined under prolonged cyclic loading, with the aim of isolating material-level degradation mechanisms independent of device-related effects. The fluid was subjected to 120,000 low-strain oscillatory shear cycles under a constant …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 101–112 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article
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Spin Coated Polyvinylidene Difluoride / Ionic Liquid Nanocomposite Thin Films with Enhanced Dielectric and Piezoelectric Properties
Abstract: This study introduces a novel approach to enhance the piezoelectric and dielectric properties of polyvinylidene difluoride (PVDF) by incorporating 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIM][BF₄]) ionic liquid via a spin-coating method— a processing route that has been rarely reported for PVDF/ionic liquid composites. Structural and morphological analyses using X-ray diffraction (XRD), Raman spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) confirm the successful integration of [BMIM][BF₄] into the PVDF matrix. The …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1190–1204 Read article
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Performance Enhancement of COC-Modified LLDPE Films: Optimization of Stiffness, Tear Resistance, and Barrier through Plasma Surface Modification
Abstract: This study explores the development of high-performance packaging materials by blending commodity Linear Low-Density Polyethylene (LLDPE) with engineering cyclic olefin copolymer (COC) as a performance modifier. To leverage the processability of LLDPE alongside the structural rigidity of COC, blends were prepared at various weight ratios (95/05, 90/10, 85/15, and 80/20) using twin-screw melt extrusion, followed by the production of films and sheets via blown film extrusion and compression molding. The …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 128–143 Read article
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Synthesis, characterization, and antibacterial activity of silver nanoparticles with expired minocycline as reducing agent: proposed as a recycling technique
Abstract: In this research, expired minocycline, a broad-spectrum tetracycline antibiotic, was employed as both a reducing and stabilizing agent for the eco-friendly synthesis of silver nanoparticles. This sustainable method avoids the use of toxic chemical reducing agents, providing a greener alternative for nanoparticle production. The synthesized silver nanoparticles were analyzed using several characterization techniques, such as UV-Vis’s spectroscopy, scanning electron microscopy, transmission electron microscopy, and Edex analysis, to assess their structural, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 16, Issue 1, 2026 · pp. 30–43 Read article
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A Review on Effect of Cryogenic Treatment on Wear Resistant Bearing Materials for Automotive Application
Abstract: Cryogenic processing has come as a successful supplementary process to common heat treatment, especially in improving the wear-resistant performance of materials employed in in-vehicle applications. This sub-zero processing is normally performed following quenching and before tempering, during which materials are subjected to extremely low temperatures, typically around -196°C, for prolonged periods of 24 hours. Cryogenic treatment, which involves subjecting materials to extremely low temperatures, has demonstrated promising results in changing …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1–11 Read article
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Utilization of Treated Textile Dyeing Wastewater and GGBFS–Perlite Blends for Sustainable Cementitious Composite Development
Abstract: The increasing global demand for concrete critically intensifies the consumption of potable water, raising significant environmental concerns and depleting vital resources. Concurrently, the textile dyeing industry generates substantial volumes of wastewater, posing considerable disposal and pollution challenges. Our investigation explores a dual solution by utilizing treated textile dyeing wastewater as an alternative mixing water source, combined with ground granulated blast furnace slag (GGBFS) and perlite as supplementary cementitious materials (SCMs), …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 291–300 Read article
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Gamma Irradiation Effects on Structural and Optical Properties of PVA/Al₂O₃/TiC Polymer Nanocomposites for Optoelectronic Applications
Abstract: PVA/TiC/Al2O3 nanocomposite (PTA) films were successfully prepared via the solution casting method. The impact of high-dose gamma (γ) irradiation (30 kGy) on the structural and optical properties of PVA/TiC/Al2O3 nanocomposites was systematically explored using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV–Visible spectroscopy. XRD analysis confirmed the semi-crystalline nature of the nanocomposites, which was found to decrease upon incorporation of Al₂O₃ nanoparticles and exposure to …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 717–729 Read article
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Thermal and Microstructural Evaluation of Natural-Glass Fiber Hybrid Composites: Sustainable Alternatives to Synthetic Materials
Abstract: The scope of engineering requirements for composite materials, which mix features from several elements engaged in engineering applications to enable greater performance, cannot be adequately understood in this way. The most recent of these materials are hybrid composites, which combine synthetic and natural fibers, particularly glass fibers, and are anticipated to create new, promising materials in terms of their ties to cost, performance, and consistency. From the perspective of their …
Published in Journal of Polymer & Composites · Vol. 14, Issue 2, 2026 · pp. 1275–1285 Read article