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620 articles for “Subtractive Synthesis”
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Synthesis and antibacterial studies of some bivalent transition metal ions Zn (II), Cu (II) and Ni (II) complexes of Schiff’s base derived from some substituted aromatic aldehydes.
Abstract: In this study, Schiff bases were synthesised through the condensation of aromatic aldehydes with primary amines and subsequently complexed with Ni(II),Zn(II) and Cu(II) ions. The formation of the metal complexes was confirmed by FTIR spectroscopy, which identified the key functional groups involved in coordination. The biological activity of the prepared compounds were studied with the help of selected bacteria like E. coli , Pseudomonas. and B. sereus.. The results obtained …
Published in Journal of Modern Chemistry & Chemical Technology · Vol. 16, Issue 2, 2025 · pp. 96–104 Read article
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Role of the Surgical-Ward Nurse in Identifying, Escalating, and Managing Postoperative Anastomotic Leak in Colorectal Patients: A Narrative Synthesis in an Australian Nursing Perspective
Abstract: Purpose: Postoperative colorectal anastomotic leak (AL) is one of the most feared complications after colorectal surgery because of its association with sepsis, reoperation, mortality, prolonged hospital stay, delayed adjuvant therapy, and permanent stoma formation. This narrative practice review outlines the frontline role of surgical-ward nurses in the early identification, escalation, and interim management of AL within the Australian acute-care context. Methods: A narrative synthesis of contemporary consensus statements, systematic reviews, …
Published in Research and Reviews : Journal of Surgery · Vol. 15, Issue 1, 2026 · pp. 7–12 Read article
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Catalytic Performance of Fe Modified Zeolite Beta for Synthesis of Xylene
Abstract: The catalytic performance of metal exchanged zeolite for the synthesis of xylene was determined in the present investigation. The experiments were carried out for alkylation of toluene with methanol over Fe modified zeolite beta for the production of xylene in a plug flow reactor. Modification of zeolite beta with Fe brings significant increase in the activity of catalyst and selectivity of the product xylene. A time on stream study showed …
Published in Journal of Catalyst & Catalysis · Vol. 4, Issue 2, 2017 · pp. 27–34 Read article
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Synthesis of Biodiesel from Biowaste/Vegetable Oil by Using Heterogeneous Nano-Catalyst
Abstract: This paper presents preparation of heterogeneous nanocatalyst (NaOH/ZnO-Li2CO3) for biodiesel synthesis from biowaste/vegetable oil by transesterification. Transesterification is an important reaction that produces fatty acid methyl esters which are excellent substitutes for diesel fuel. Biodiesel production by using nanocatalyst is one of important approaches in the biofuel research. The optimization of transesterification reaction is affected by the catalyst type, reaction temperature, reaction time, methanol to biowaste/oil ratio. The analysis of …
Published in Journal of Catalyst & Catalysis · Vol. 4, Issue 1, 2017 · pp. 11–23 Read article
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Identification of Some Imported Lubricating Oil Additives Used in Libya and Synthesis of the Most Consumed Ones from the Local Raw Materials
Abstract: This paper presents the identified six additives imported under trade names used in the lubricating oil blending factory of A-Zawia-Libya. Their structures have been completely confirmed by examining their physical properties and using modern analytical techniques such as nuclear magnetic resonance spectroscopy (NMR), infra-red (IR), atomic absorption (AAS) and gas chromatography (GC). The synthesis of most important and more consumed additives in lubricating oils in Libyan oil industry from local …
Published in Journal of Catalyst & Catalysis · Vol. 3, Issue 3, 2016 · pp. 10–17 Read article
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Synthesis of Copper Oxide Nanoparticles using Ultrasound for the Treatment of Textile Organic Dyes (Reactive Black 5 and Basic Blue 3)
Abstract: This paper describes the ultrasound assisted synthesis of copper oxide (CuO) nanoparticles using copper nitrate trihydrate and ammonium carbonate as reactants. The resultant product, copper carbonate was calcined at 400°C which was chosen based on the thermogravimetric analysis of copper carbonate precipitate. The final product CuO nanoparticles characterized by X-Ray diffraction (XRD), scanning electron microscope (SEM), energy-dispersive X-ray spectroscopy (EDAX), particle size analyzer (PSA) and Brunner-Emmet-Teller surface area analyzer (BET) …
Published in Journal of Catalyst & Catalysis · Vol. 2, Issue 3, 2015 · pp. 16–22 Read article
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Synthesis of Zeolite Y-Encapsulated Copper(II) Complexes with Aminobenzonitriles and Carbonitriles by Flexible Ligand Method
Abstract: Zeolite Y encapsulated copper(II) sulphate complexes with 2-, 3- and 4- aminobenzonitrile and carbonitrile have been prepared by flexible ligand synthesis method. Complexes are characterized by magnetic susceptibility, infra-red and electronic spectral techniques. The data clearly suggests the presence of metal complexes in zeolite matrix.
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 1, 2014 · pp. 41–52 Read article
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Synthesis, Structural Studies and Catalytic activity of Copper(II) Complex Supported by N, N′-bis (2-Hydroxy-3-Methoxybenzaldehyde) 4-Methylbenzene-1, 2-Diamine
Abstract: A novel robust method for synthesis of 3-MOBdMBn-Cu complex, supported by -ONNO-tetradentate Schiff-base ligand is presented. This copper complex is prepared by the reactions of metal solution with one molar equivalent of 3-MOBdMBn (N, N’-bis (2-hydroxy-3-methoxybenzaldehyde) 4-Methylbenzene-1, 2-diamine) Schiff-base ligand in methanol under nitrogen atmosphere. In contrast to other catalysts, the main advantage of this catalyst system was that the cost of the catalyst was remarkably low and it can …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 1, 2014 · pp. 53–60 Read article
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Ceria and Modified Ceria: A Reusable Catalyst for the Green Synthesis of 2,3-diphenyl Quinoxaline at Room Temperature
Abstract: Simple, highly versatile and efficient synthesis of 2,3-diphenylquinoxalines is achieved from benzil and o-phenylene diamine using ceria and modified ceria as the catalyst. Modification of ceria is done using different weight percentage of zirconia. The catalysts are characterized by XRD, FT-IR, BET surface area, TGA and EDX-SEM. The advantages of this method are short reaction times, milder conditions and easy work-up. The product could be separated from the heterogeneous catalyst …
Published in Journal of Catalyst & Catalysis · Vol. 1, Issue 3, 2014 · pp. 1–11 Read article
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Synthesis of Biodiesel fuel additive from Glycerol using Cationic ion exchange resin- A review
Abstract: With the alarming increasing of oil consumption and the number of automotives being instilled, there has been immense research taking place to find a sustainable fuel to replace the current fossil fuels and also not render the current automotives obsolete. The current favorable solution to this is Biodiesel which can be generated either from oil seeds or waste vegetable oils. The selectivity of this process is 90% and the byproduct …
Published in Journal of Catalyst & Catalysis · Vol. 6, Issue 3, 2019 · pp. 1–8 Read article
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Synthesis of a Re-Usable HCl Treated Graphite Catalyst for Biodiesel Production from Pongamia Pinnata Oil and DMC
Abstract: AbstractThe aim of this research was to investigate the biodiesel from Pongamia pinnata oil with HCl treated graphite catalyst via transesterification. New biodiesel formation process was designed using P. pinnata oil and HCl treated graphite catalyst. Graphite powder was treated with HCl and HCl treated graphite was used as a catalyst. 95% biodiesel yield was obtained with operating conditions, including P. pinnata oil to dimethyl carbonate ratio (1:3), catalyst concentration …
Published in Journal of Energy, Environment & Carbon Credits · Vol. 8, Issue 2, 2018 · pp. 30–37 Read article
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Synthesis and Characterization of Nickel doped Barium Niobate Ba (Ni0.5Nb0.5)O3 (BNN) Nanomaterial
Abstract: AbstractFerroelectric materials are of great interest for researchers worldwide, because of their unique physical properties and wide range of applications. The composite nanomaterial Ba(NiNb)0.5O3 (BNN) was synthesized by conventional solid state reaction method. The structural characterization was done by x-ray diffraction (XRD). The research was carried out to investigate structural properties of BNN nanomaterial as a function of sintering duration. BNN was sintered at 10000C and different samples were prepared …
Published in Journal of Microelectronics and Solid State Devices · Vol. 5, Issue 2, 2018 · pp. 29–33 Read article
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Chemical Synthesis, Spectral Characterization and Electrical Conductivity Behavior of Poly(2-Methoxyaniline-Co-2-Chloroaniline) and its CuO Nanocomposite and Polypropylene Glycol Blend
Abstract: AbstractCopolymerization of 2-chloro aniline and 2-methoxy aniline was achieved chemically by oxidative polymerization technique using ammonium persulphate as the oxidizing agent in acidic medium in the presence of sodium lauryl sulphate, an anionic surfactant. Copolymerization was also carried out in the absence of the surfactant to study the effect of surfactant on the thermal stability and electrical conductivity. The copolymer composite with CuO nano particles and blend with poly propylene …
Published in Journal of Polymer & Composites · Vol. 6, Issue 3, 2018 · pp. 1–13 Read article
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Synthesis and Experimental Evaluation of Graft Polymer Nanocomposite in Water Based Drilling Fluid System for Reactive Unconventional Reservoirs
Abstract: AbstractThis experimental work discusses the evaluation of polyacrylamide-grafted-gum arabic/carboxymethyl cellulose nanocomposite as a drilling mud additive for the drilling of reactive shale formations which may lead to wellbore instability. The synthesized nanocomposite was synthesized with free polymerization technique and it was characterized by XRD, FTIR, and FESEM. Then, it was preceded in the development of the WBDMS. Its effect on the rheological and filtration control properties of the formulated mud …
Published in Journal of Polymer & Composites · Vol. 5, Issue 2, 2017 · pp. 34–41 Read article
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Synthesis of Polyorthanisidine by Interfacial Polymerization
Abstract: AbstractPolyorthoanisidine has been synthesized by interfacial polymerization method. O-anisidine has been used as a monomer, hydrochloric acid is used as a dopant and ammonium persulphate as an oxidiser. The solvent used for the study is chloroform, isopropanol, hexane and xylene. The polyorthoanisidine obtained is characterized for particle size analysis. It is observed as with xylene as a solvent the least particle size has been observed with Z average value of …
Published in Journal of Polymer & Composites · Vol. 5, Issue 1, 2017 · pp. 1–6 Read article
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Synthesis of Poly(Methyl Methacrylate) Latex Using Batch Emulsion Polymerization Reactor: Experimental and Simulation Study
Abstract: AbstractThe rationale for the present study was to develop Poly(methyl methacrylate) polymer latex, using free radical emulsion polymerization mechanism, in which water acted as the continuous aqueous phase, methyl methacrylate monomer as the dispersed phase, potassium persulfate (KPS) as an initiator and sodium dodecyl sulfate (SDS) as the stabilizing agent. PMMA is a versatile thermoplastic resin, used widely because of its excellent performance in optical and medical field. The characterization …
Published in Journal of Polymer & Composites · Vol. 4, Issue 1, 2016 · pp. 37–44 Read article
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Synthesis and Characterization of Emulsion Paint Binder from a Copolymer Composite of Dimethylol Urea/Polystyrene
Abstract: AbstractIn our desire to reduce formaldehyde emission from urea formaldehyde resin (UF), dimethylol urea (DMU) was synthesized. Liquid polystyrene (PS) obtained from waste PS material was copolymerized by blending with the DMU at varying concentrations (10–70%). Infrared spectra infers a reactive blending between DMU and PS, while some physical property tests carried out reveals reduction in moisture uptake, rigidity and further reduction in formaldehyde emission among the favorable changes in …
Published in Journal of Polymer & Composites · Vol. 3, Issue 2, 2015 · pp. 11–21 Read article
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Synthesis and Characterization of Ether Containing Tetraglycidyl Epoxy Reinforced with Amine Functionalized Graphene Oxide (F-Go) and It’s Nanocomposites
Abstract: AbstractTGDDE matrix material along with functionalized graphene oxide (F-GO) as reinforcement was used to develop a unique skeletally modified tetra functional epoxy nanocomposites. Amine functionalization of graphene oxide nanoparticles (F-GO) on its surface was achieved by grafting 3-aminopropyltriethoxysilane (APTES) as coupling agent. The FT-IR spectrum revealed that the silane coupling agent was covalently bonded to the surface of graphene oxide nanoparticles, offering better dispersibility and compatibility with TGDDE epoxy matrix. …
Published in Journal of Polymer & Composites · Vol. 3, Issue 2, 2015 · pp. 39–51 Read article
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Synthesis and Characterization of Certain Biodegradable Chitosan/Lactic Acid-based Polyester Blend Films
Abstract: AbstractBiodegradable blend films based on chitosan with poly(ethylene glycol lactate-co-ethylene glycol terephthalate), PEGLT and poly(butylene lactate-co-butylene succinate), PBLSA, were prepared by solution-mixing and film-casting method. The main objective of this investigation was the study and characterization of chitosan/lactic acid-based polyester blends which are useful as bio-packaging material for potential food applications. The first part of the investigation was related to the synthesis and characterization of polyesters, PEGLT and PBLSA by …
Published in Journal of Polymer & Composites · Vol. 1, Issue 2, 2013 · pp. 35–45 Read article
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Utilization of Bentonite Clay Coupled with Potash for the Synthesis of Octadec-9-Enoic Acid Methyl Esters of Pongamia Pinnatatriglycerides
Abstract: Due to the ever increasing human population worldwide, especially in the developing countries across the world; renewable energy sources are in the primary focus of the scientists and researchers. In addition, the depletion of the reserves of the fossil fuels along with the increased consumption of the available reserves has led to wide spread global unrest. Complementing the above, there are significant environmental problems namely global warming due to increased …
Published in Journal of Polymer & Composites · Vol. 10, Issue 2, 2022 · pp. 72–78 Read article