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240 articles for “and XRD”
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Synthesis and Characterization of Green Synthesized Iron Nano Particle (GInP) Using Eucalyptus globulus for Lead Removal
Abstract: The application of green synthesized iron nanoparticle for the removal of lead is researched in this study. The FT-IR and XRD results reveal that a nanoparticle with 80 nm size could be synthesized using Eucalyptus globulus leaf extract. The specific surface area of the nanoparticle was found to be 59 m2/g. The lead removal capability of the green synthesized iron nanoparticle (GInP) was investigated for lead concentration ranging from 50–250 …
Published in Journal of Materials & Metallurgical Engineering · Vol. 10, Issue 3, 2020 · pp. 20–25 Read article
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Enhancement of Electrical Conductivity of Laterite Derived Ferric Oxide to Facilitate As Anode Materials
Abstract: Laterite is a mineral abundant in ferric oxide and various impurities, including aluminum oxide and silicon dioxide. The extraction of ferric oxide from laterite is accomplished through a cost-effective leaching process employing HCl, NaOH, and Sodium dodecyl sulfate (SDS). Characterization using Xray diffraction (XRD) confirmed the synthesized particles to be α-Hematite nano particles, with an average particle size of 94.21 nm, predominantly falling within the range of 90 nm to …
Published in Journal of Materials & Metallurgical Engineering · Vol. 13, Issue 3, 2023 · pp. 1–11 Read article
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Characterisation of Plasma Sprayed CNT-Alumina Composite Coatings on Boiler Tube Steel
Abstract: In this research work, the 1.5, 2 and 4 wt.% CNTs-Al2O3 coatings were prepared and successfully deposited on T22 boiler tube steel using plasma spray process. Ni-Cr was also used as bond coat before applying CNTs-Al2O3 coatings. The coatings were subjected to metallography, XRD and SEM/EDAX analysis. The porosity of CNTs-Al2O3 mixed coatings on T22 boiler steel was found to be decreasing with increase in CNTs content. The CNTs were …
Published in Journal of Polymer & Composites · Vol. 5, Issue 3, 2017 · pp. 1–15 Read article
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Enhancement of anticorrosion performance on aluminium substrate by novel nanocomposites of PANI/Bi2O3.CO.ZnO/CNT
Abstract: PANI/Bi2O3.CO.ZnO nanocomposites were prepared in presence of bismuth cobalt oxide nanoparticles at 25oC using ammonium persulphate as an oxidant in an in situ polymerisation with aqueous solution of camphor sulphonic acid (SDBS). These nanocomposites were characterized by XRD, FTIR, TEM, UV and SEM. The performance of PANI, PANI/Bi2O3.CO.ZnO nanocomposites and PANI/Bi2O3.CO.ZnO/CNT nanocomposites as anticorrosion protective coating on Al in 0.5 M HNO3 was studied by using potentiodynamic polymerisation technique and …
Published in Journal of Polymer & Composites · Vol. 6, Issue 2, 2018 · pp. 31–41 Read article
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Chemical Synthesis, Spectral Characterization and Electrical Conductivity Behavior of Poly(2-Methoxyaniline-Co-2-Chloroaniline) and its CuO Nanocomposite and Polypropylene Glycol Blend
Abstract: AbstractCopolymerization of 2-chloro aniline and 2-methoxy aniline was achieved chemically by oxidative polymerization technique using ammonium persulphate as the oxidizing agent in acidic medium in the presence of sodium lauryl sulphate, an anionic surfactant. Copolymerization was also carried out in the absence of the surfactant to study the effect of surfactant on the thermal stability and electrical conductivity. The copolymer composite with CuO nano particles and blend with poly propylene …
Published in Journal of Polymer & Composites · Vol. 6, Issue 3, 2018 · pp. 1–13 Read article
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Synthesis and Experimental Evaluation of Graft Polymer Nanocomposite in Water Based Drilling Fluid System for Reactive Unconventional Reservoirs
Abstract: AbstractThis experimental work discusses the evaluation of polyacrylamide-grafted-gum arabic/carboxymethyl cellulose nanocomposite as a drilling mud additive for the drilling of reactive shale formations which may lead to wellbore instability. The synthesized nanocomposite was synthesized with free polymerization technique and it was characterized by XRD, FTIR, and FESEM. Then, it was preceded in the development of the WBDMS. Its effect on the rheological and filtration control properties of the formulated mud …
Published in Journal of Polymer & Composites · Vol. 5, Issue 2, 2017 · pp. 34–41 Read article
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Synthesis of Polyorthanisidine by Interfacial Polymerization
Abstract: AbstractPolyorthoanisidine has been synthesized by interfacial polymerization method. O-anisidine has been used as a monomer, hydrochloric acid is used as a dopant and ammonium persulphate as an oxidiser. The solvent used for the study is chloroform, isopropanol, hexane and xylene. The polyorthoanisidine obtained is characterized for particle size analysis. It is observed as with xylene as a solvent the least particle size has been observed with Z average value of …
Published in Journal of Polymer & Composites · Vol. 5, Issue 1, 2017 · pp. 1–6 Read article
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Electrical Conductivity and Antibacterial Studies on Chemically Synthesized Poly (2-Methyl Aniline-co-2-Chloro Aniline)-Blend-Polyurethane
Abstract: AbstractElectrically conducting copolymer blend, poly (2-methyl aniline-co-2-chloro aniline)-blend-polyurethane has been synthesized chemically by oxidative polymerization technique using 0.3 M ammonium persulphate (APS) as oxidant, 0.1 M of the anionic surfactant, sodium lauryl sulphate and 1 M HCl as dopant. The formation of the copolymer blend has been confirmed by comparison with the spectral data obtained for the copolymer which was synthesized under the same conditions and characterized. The copolymer blend …
Published in Journal of Polymer & Composites · Vol. 5, Issue 1, 2017 · pp. 7–14 Read article
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A Study on the Effect of Ionic Conductivity on Addition of Salt for Polymer Nanocomposite Gel Electrolyte for Solar Cell Applications
Abstract: AbstractDye sensitized solar cells (DSSC) have attracted greater attention in the recent years because of their relatively high energy conversion efficiency and low cost. In the DSSCs, the electrolytes play a vital role in the determination of the efficiency and long term stability. In this investigation, we report on the synthesis, characterization and conductivity study of polymer nanocomposite gel electrolyte. Cadmium oxide nanoparticles were added into polymer blend of poly …
Published in Journal of Polymer & Composites · Vol. 3, Issue 3, 2015 · pp. 8–15 Read article
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Conductive Organic Polymer Based Inorganic-Organic Hybrid Composite: Synthesis and Characterization
Abstract: Inorganic organic (IO) hybrids where inserted conducting organic polymer (COP) imprints their polymeric nature onto the hybrid material are one of the most promising candidates for solving many technological problems of modern technocratic society. The Inorganic-organic hybrid material of para toluidine (organic) & mercuric chloride (inorganic) was synthesized by using “instant-heating and slow-cooling” technique. Some light orange coloured plate-like crystals were obtained. XRD pattern of the grown crystal were analysed …
Published in Journal of Polymer & Composites · Vol. 8, Issue 1, 2020 · pp. 1–5 Read article
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Engineering Novel Blue Emissive Thiazolidinedione (TD) Poly Lactic Acid (PLA) Composite Thin Films for Bioplastic Scintillation
Abstract: In this article, we demonstrate luminescent properties of PLA blended with new 3-[2-(4-methylphenyl)-2-oxoethyl]-5-(thiophen-2-ylmethylidene)-1, 3-thiazolidine-2, 4-dione and 3-[2-(4-chlorophenyl)-2-oxoethyl]-5-(thiophen-2-ylmethylidene)-1, 3-thiazolidine-2, 4-dione (TD). This paper mainly aims at the preparation of intercalated thin films of PLA and TD. The formation of matrix-dopant composite films was confirmed by FTIR, SEM, TGA, DSC and XRD characterizations. This work really stands out from our previous work as TD has been better recognized as drug material in …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 10–23 Read article
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Enhancement of Dielectric Properties of PVDF Composites with MWCNT and GCNF Fillers
Abstract: The paper discusses the role of multiwalled carbon nanotube (MWCNT) and graphitized carbon nanofibre (GCNF) in Polyvinylidene fluoride (PVDF) composites prepared by melt mixing method. Analytical studies were carried out using X-ray diffraction analysis (XRD) and Fourier transform infrared spectroscopy (FTIR) for understanding the role of fillers. Formation of β phase crystalline structure with a relative increase in β phase content is observed and is maximum at 5 wt.% of …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 43–52 Read article
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Characteristics of Novel Geopolymer Composites Synthesized from Red Mud and Diatomaceous Earth in Autoclave Conditions without Using Alkaline Activators
Abstract: The geopolymer-based materials have been studied and developed since the last decades of the 20th century and applied in many fields of life. The production of geopolymer also has many different levels of technology from low to high technology which depends on quality and the applied fields of products. The geopolymer composites are also considered as friendly environmentally products related to low energy consumption production technology; reuse industrial wastes as …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 81–91 Read article
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Application of Polypyrrole/Lead Sulphide Nanocomposite in UV Light Assisted Photocatalysis and Gas Sensing
Abstract: The synthesis of ppy/lead sulphide nanocomposite was done using the co-precipitation method. The synthesized ppy/leadsulphide nanocomposite was characterized using Transmission Electron Microscopy (TEM), Selected Area Electron Diffraction (SAED), X-Ray Powder Defraction (XRD), Fourier Transformation Infra-Red Spectroscopy (FTIR), UV-Vis Spectroscopy techniques. The optical bandgap of the synthesized ppy/lead sulphide nanocomposite was observed to be 3.48 eV. The synthesized material is crystalline, with an average crystallite size of 2.51 nm. The photocatalytic …
Published in Journal of Polymer & Composites · Vol. 9, Issue 1, 2021 · pp. 13–27 Read article
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An Optimize Formulation to Synthesis of size Controlled Hydrophobic Starch Acetate Nanoparticles using Box-Behnken Design
Abstract: The best way to improve the overall performance of native starch is by chemical modification. In recent years, hydrophobically modified starch has attracted considerable attention for the design and manufacture of novel nanoparticulate drug delivery carriers. The purpose of this research was to synthesize hydrophobic starch nanoparticles (NPs) and to optimize process factors through the use of response surface methodology (RSM). The corn starch acetate (CSA) NPs was synthesized using …
Published in Journal of Polymer & Composites · Vol. 10, Issue 1, 2022 · pp. 32–54 Read article
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Synthesis of PANI/RGO/NiCrO Nanocomposite Material for Charge Storage Application
Abstract: PANI/RGO/NiCrO nanocomposite is synthesized by chemical oxidative polymerization of aniline and Nickel-Chromium Oxide (NiCrO). The prepared PANI/RGO/NiCrO nanocomposite exhibited high specific capacitance of 800 F/g at the scan rate of 5 mV/s, high power density of 1399.44 Wkg-1 and high energy density of 70 Whkg-1. The as-prepared polymer nanocomposites were characterized by X-ray diffraction (XRD) to study crystallinity, Fourier transform infrared spectroscopy (FTIR) to know the functional groups, Transmission electron …
Published in Journal of Polymer & Composites · Vol. 10, Issue 1, 2022 · pp. 89–99 Read article
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Influence of Bi2O3 on Physical, Optical and gamma radiation Properties of BaO-Bi2O3-B2O3-CuO and BaO-Bi2O3-B2O3-Fe2O3 glasses
Abstract: In this present work glasses with chemical composition 30BaO-XBi2O3-(69-X)B2O3-1CuO and 30BaO-XBi2O3-(69-X)B2O3-1Fe2O3 (X = 0, 5, 10, 15, 20 and 25 mole%) have been prepared and labeled as BBBC and BBBF series, respectively. Traditional quenching method was employed for making these samples. XRD diffractograms confirmed that the materials were amorphous. Physical, optical and structural properties were studied with the influence of Bi2O3 concentration. The density of both BBBC and BBBF series …
Published in Journal of Polymer & Composites · Vol. 10, Issue 1, 2022 · pp. 20–31 Read article
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Synthesis of Copper Nanoparticles using Alternanthera Sessilis Linn Leaf Aqueous Extract and their Characterization
Abstract: The current study describes the biogenesis of Cu NPs using an aqueous extract of the leaf of Alternanthera sessilisLinn. (A.S). recently, biological synthesis of nanoparticles has gained popularity due to the fact that it is eco-friendly, simple, cost-effective, non-hazardous, and extreme conditions. The aqueous extract of Alternanthera sessilisleaf contains enoughterpenoids, carbohydrates, and flavonoids to convert metal ions into metal and thus stabilize the resulting nanoparticles. The UV-visible spectrophotometer confirmed the …
Published in Journal of Polymer & Composites · Vol. 10, Issue 2, 2022 · pp. 14–28 Read article
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Effect of Curing Time on Physico-mechanical Properties on Dental Composite
Abstract: This study aim to investigate the influence of curing time on physical and mechanical properties of a dental composite cured by using LED light with intensity of 1500 mW/cm2 in the range of 440-480 nm. We prepared the glass ionomer powder by fusion of various inorganic components at high temperature and studied the influence of silica/alumina ratio keeping other inorganic salts such as Calcium fluoride (CaF2), Sodium Fluoride (NaF), Calcium …
Published in Journal of Polymer & Composites · Vol. 10, Issue 3, 2022 · pp. 36–47 Read article
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Thermal degradation analysis of banana fiber by Coats & Redfern methodThermal Degradation Analysis of Banana Fiber by Coats and Redfern Method
Abstract: Nowadays, natural fiber is more advantageous than synthetic fiber. Natural fibers are used as reinforcement material with combination of polymer matrix. These are of different types like banana fiber, bamboo fiber, sisal, hemp, and jute, etc. Banana fiber is one of them which is most common and easily available fiber in global scenario. It is biodegradable, renewable, and lower in cost. This fiber is higher in cellulosic content. Out of …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 28–32 Read article