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211 articles for “SEM (Scanning Electron Microscopy)”
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To explore the effect of polyethylene glycol additive on mechanical and gas permeation properties of polyvinyl alcohol membranes
Abstract: Polyvinyl alcohol (PVA) membranes were prepared by solution casting and blended with Polyethylene glycol (PEG) in de-ionized water which led to the formation of porous and flexible membranes. Extensive experimentation were performed, in order to find out that at what composition of PEG pores will be generated in the PVA membranes. The PVA polymer is a hard and crystalline thermoplastic so high concentrations of PEG were used, i.e. 40 wt%, …
Published in Journal of Polymer & Composites · Vol. 7, Issue 1, 2019 · pp. 27–33 Read article
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A Study on the Effect of Ionic Conductivity on Addition of Salt for Polymer Nanocomposite Gel Electrolyte for Solar Cell Applications
Abstract: AbstractDye sensitized solar cells (DSSC) have attracted greater attention in the recent years because of their relatively high energy conversion efficiency and low cost. In the DSSCs, the electrolytes play a vital role in the determination of the efficiency and long term stability. In this investigation, we report on the synthesis, characterization and conductivity study of polymer nanocomposite gel electrolyte. Cadmium oxide nanoparticles were added into polymer blend of poly …
Published in Journal of Polymer & Composites · Vol. 3, Issue 3, 2015 · pp. 8–15 Read article
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Thermo-Mechanical Properties of Unsaturated Polyester Reinforced with Coconut and Snail Shells
Abstract: AbstractParticulate-filled polymer composites are becoming quite attractive because of their low cost and wide applications. In this study, the effects of coconut shell (CS) and snail shell (SS) volume fractions (5–50 vol. %) on the thermal and mechanical properties of unsaturated polyester resin (UPR) composite are investigated. The results show that tensile strength, elongation at break, flexural strength, and hardness of the composite increase as filler concentration increases. However, impact …
Published in Journal of Polymer & Composites · Vol. 2, Issue 2, 2023 · pp. 44–56 Read article
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Investigation on Properties of Water and Methylene Chloride Blown Rigid Polyurethane Foam
Abstract: Physical properties are important parameters which influence the other properties and performance of rigid polyurethane foam (RPUF). Water and methylene chloride are the important ingredients of RPUF which act as blowing agents and influence the density, morphology and fire properties. RPUF samples were prepared from crude 4, 4’-diphenylmethane diisocyanate (CMDI), polyether polyol, triethylene diamine (TED), 1, 4-butane diol, polysiloxane ether, water and methylene chloride. RPUF with different densities were prepared …
Published in Journal of Polymer & Composites · Vol. 2, Issue 1, 2023 · pp. 46–54 Read article
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Experimental Studies to Record the Lithographically Fabricated Microstructures by Surface Profilometry and Scanning Electron Microscopy for Microfluidic Laboratory-on-a-Chip Systems
Abstract: In this research paper, the poly(methyl methacrylate) (PMMA) microfluidic laboratory-on-a-chip system is fabricated in the cleanroom laboratory by maskless lithography, hot embossing lithography and direct bonding technique. The microstructures of the lab-on-a-chip system are measured by surface stylus profilometer. Also, the images of microstructures of lab-on-a-chip system are captured by using scanning electron microscopy (SEM). This fabricated lab-on-a-chip system is useful in bioengineering applications.
Published in Journal of Polymer & Composites · Vol. 4, Issue 1, 2016 · pp. 27–36 Read article
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Effect of Softening Agents in the Thermal and Morphological Properties of Starch Based Bioplastics
Abstract: Plasticization of starch with 1,2,3-trihydroxy-propane (glycerol) as a softening agent (plasticiser) can replace the starch-starch bonds to starch-massive glycerol bonds, which offers stability, improved physicochemical and functional properties of starch. This study is an investigation on the thermal and morphological properties of bio plastic samples made of starch with varying plasticiser contents (8, 6.5, 5, 3.5 and 2 ml) and are evaluated by methods like thermogravimetric analysis (TGA), differential scanning …
Published in Journal of Polymer & Composites · Vol. 5, Issue 1, 2017 · pp. 15–24 Read article
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Analysis of Oxidation Behavior on T-22 Boiler steel at 800°C
Abstract: The behavior of boiler steel T-22 in a rich air environment has been studied under the condition of isothermal at 800°C for 50 cycles in a cyclic manner. The kinetics of oxidation was established for boiler steel T-22under cyclic conditions for 50 cycles by weight change technique per unit area. Each cycle heating the sample at 1 hour followed by cooling 20 minutes at ambient temperature. Detonation gun spray techniques …
Published in Journal of Polymer & Composites · Vol. 8, Issue 1, 2020 · pp. 18–25 Read article
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Enhancement of Dielectric Properties of PVDF Composites with MWCNT and GCNF Fillers
Abstract: The paper discusses the role of multiwalled carbon nanotube (MWCNT) and graphitized carbon nanofibre (GCNF) in Polyvinylidene fluoride (PVDF) composites prepared by melt mixing method. Analytical studies were carried out using X-ray diffraction analysis (XRD) and Fourier transform infrared spectroscopy (FTIR) for understanding the role of fillers. Formation of β phase crystalline structure with a relative increase in β phase content is observed and is maximum at 5 wt.% of …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 43–52 Read article
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Eco-friendly Materials of Polymer Composites Based on Water Hyacinth Fibers/Roving
Abstract: Overgrowth of water hyacinths will cause difficulties for water traffic in the Mekong Delta and affect the growth of other aquatic species. The water hyacinth as a raw material available in nature has been applied in production of the composite materials. The water hyacinth trees were treated in NaOH solution for 2-12 hours with concentration in the range 2.5-15.0%. The morphology of the water hyacinth before and after treatment was …
Published in Journal of Polymer & Composites · Vol. 8, Issue 3, 2020 · pp. 62–69 Read article
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Thermally Trigged Self-Healing Smart Shape Memory Polymer Composite
Abstract: Temperature-responsive self-actuating PU/MWCNTs composites were prepared with micro-compounder through in-situ polymerization. For making of 1CNTPU composite sample 1 part per hundred multiwall Carbone nanotubes (MWCNTs) were reinforced into the neat polyurethane (PU) base matrix. Surface characterizations for pure and composite have studying by using Atomic Force Microscope (AFM), high resolutions Scanning Electron Microscopy (SEM). Properties like shape recovery, storage modulus, loss modulus, tensile stress, degree of hardness, and flexural stress …
Published in Journal of Polymer & Composites · Vol. 9, Issue 3, 2021 · pp. 10–18 Read article
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Photoluminescent Reduced Graphene Oxide (rGO)–ZnO Nanocomposites Prepared Through one-pot Solvothermal Route
Abstract: In the present article, we report solvothermal synthesis of reduced graphene oxide (rGO)–ZnO nanocomposites through in situ exfoliations of graphite oxide with two different zinc-containing precursors viz. Zinc acetate dihydrate and zinc(II) acetylacetonate in water-diethylene glycol medium with hexamethylenetetramine as a reducing agent. The obtained rGO–ZnO nanocomposites were characterized by X-ray diffraction, and the ZnO lattice parameters were calculated. Raman spectroscopy indicated the presence of characteristic bands of graphene and …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 70–80 Read article
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Microstructure and Mechanical Characterization of AA390 and Si3N4 Metal Matrix Composite Using Severe Plastic Deformation
Abstract: Metal matrix composites (MMCs) have significant attention in recent years due to their potential for improved mechanical properties compared to conventional monolithic materials. This study focuses on the microstructure and mechanical characterization of a MMC comprising AA390 aluminum alloy reinforced with Si3N4 particles. The severe plastic deformation (SPD) process, Equal Channel Angular Pressing (ECAP), was employed to fabricate the composite with enhanced mechanical properties. The ECAP method was chosen as …
Published in Journal of Polymer & Composites · Vol. 12, Issue 1, 2024 · pp. 17–30 Read article
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Synthesis and Characterization of In2S3 Nanoflake Thin Film for Photosensor Applications
Abstract: Indium sulphide (In2S3) thin films in the form of nanoflakes are synthesized by using chemical vapour deposition method on glass substrate with the intension to test its photosensor applications. These as deposited nanoflake thin films are characterized for physicochemical properties using X-ray diffraction (XRD) pattern, energy dispersive X-ray (EDAX) analysis,scanning electron microscopy (SEM) while optoelectronic properties were studied using optical and electrical characteristics obtained through UV-Vis transmission spectroscopy and I-V …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 4, Issue 3, 2017 · pp. 21–26 Read article
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Corrosion Inhibition Effect of 1-(4-Methoxy-phenyl)-3-(5-phenyl-1,3,4-oxadiazol-2-yl) propan-1-one Inhibitor for Mild Steel in 1 M HCl Solution
Abstract: The environmental friendly 1-(4-Methoxy-phenyl)-3-(5-phenyl-1,3,4-oxadiazol-2-yl) propan-1-one (A1) inhibitor is synthesized and their corrosion inhibition for Mild Steel in a 1 M HCl solution was studied using weight loss methods, electrochemical measurements, and the surface morphology of mild steel with and without inhibitor were studied using scanning electron microscopy (SEM) analysis. As the concentration of the inhibitor was increased the inhibition efficacy of 1-(4-Methoxy-phenyl)-3-(5-phenyl-1, 3, 4-oxadiazol-2-yl) propan-1-one was also enhanced and on …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 8, Issue 2, 2021 · pp. 31–37 Read article
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Fabrication and Surface Modified Non-woven Calotropis gigantea Fiber Mat Reinforced Polypropylene Composites by Film Stacking Method
Abstract: Nowadays, there is a growing environmental consciousness and awareness about the need for sustainable development, which has led to growing interest in using natural fibers as reinforcement in polymer composites for synthetic fiber substitution. The current work deals with the effects of Calotropis gigantea fiber (CGF) content and chemical modification of CGF mats by treatment with sodium dodecyl sulfate (SDS) and SDS-pretreated benzoyl chloride on the fundamental properties of CGF-filled …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 9, Issue 1, 2022 · pp. 10–22 Read article
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A Study of the Effect of Sodium Hydroxide and Sodium Lauryl Sulfate Surface Treatments on Natural Fibers
Abstract: Due to its accessibility, environmental friendliness, renewability, CO2-neutrality, flexibility, low density, and low cost, natural fibre (NF) can have a significant impact on the area of fibre reinforced polymer composite (FRPC) as a reinforcing material. Banana fiber (BF)/calotropis gigantea fiber (CGF) could be a potential candidate for synthetic FRPC replacement. Plant derive banana and calotropis gigantea fibers are valuable NFs that are abundantly available in Bangladesh. The purpose of this …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 9, Issue 2, 2022 · pp. 1–11 Read article
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California Bearing Ratio and Young’s Modulus Behavior of Clinker Stabilized Fly Ash-Mine Overburden Mixes
Abstract: Fly ash is a major byproduct of coal combustion. Fly ash often causes disposal problems and environmental pollution. This paper presents detailed laboratory investigation carried out on clinker stabilized fly ash-mine overburden mixes to find out its suitability for sub-base of mine haul road pavements. Proctor compaction test, Unconfined Compressive Strength (UCS) test, California Bearing Ratio (CBR) Test, Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDX) were conducted …
Published in Recent Trends in Civil Engineering & Technology · Vol. 3, Issue 3, 2013 · pp. 1–10 Read article
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Enhancing Concrete Strength: Investigating the Impact of Glass Fines on Mechanical Properties
Abstract: The global emission of CO2 from cement industries poses a significant environmental challenge, being a primary contributor to environmental issues. Numerous researchers have explored alternative cementitious materials to formulate robust and long-lasting concrete. This study focuses on utilizing waste glass powder (GlP), derived from rejected soda-lime glass bottles collected from various sources, for experimental purposes. The laboratory experiments investigate the behavior of concrete incorporating glass as a partial substitute for …
Published in Recent Trends in Civil Engineering & Technology · Vol. 13, Issue 3, 2023 · pp. 15–23 Read article
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Characterization Techniques for Thin Film Coatings Based on SiO₂, TiO₂, and ZrO₂
Abstract: Thin film coatings made from silicon dioxide (SiO₂), titanium dioxide (TiO₂) and zirconium dioxide (ZrO₂) have attracted great interest owing to their excellent optical, electrical, mechanical and chemical properties. These oxide thin films are widely used in microelectronics, solar cells, sensors, biomedical devices, photocatalysis, anti-reflective coatings and protective layers. The structural, morphological, compositional, optical and mechanical properties of these coatings are closely related to their performance and reliability. Therefore, thorough …
Published in Journal of Materials & Metallurgical Engineering · Vol. 16, Issue 2, 2026 Read article
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Experimental Study on Microstructural Evolution and Tensile Properties of Robotic Pulse MIG Welded Steel
Abstract: Robotic pulse Metal Inert Gas (MIG) welding has emerged as an advanced joining technique capable of producing superior weld quality through precise control of welding parameters. The present study evaluates the influence of welding parameters on the microstructural evolution and tensile properties of steel weldments fabricated using robotic pulse MIG welding and compares the results with conventional pulse MIG welding. Microstructural characterization was carried out using Scanning Electron Microscopy (SEM) …
Published in Journal of Experimental & Applied Mechanics · Vol. 17, Issue 2, 2026 · pp. 40–52 Read article