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214 articles for “SEM (Scanning Electron Microscopy)”
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Aluminium-Doped Zinc Ferrite Nanoparticles Synthesized by Combustion Method for Polymer Composite Applications
Abstract: ZnFe₂₋xAlₓO₄ (x = 0 and 0.5) nanoparticles were synthesized via a combustion method owing to its simplicity, cost efficiency, and ability to produce highly crystalline nanomaterials. Powder X-ray diffraction (XRD) analysis confirmed the formation of a single-phase cubic spinel structure without detectable secondary phases, indicating high phase purity. The average crystallite size was estimated to be in the range of 14–20 nm, confirming the nanocrystalline nature of the samples. Field-emission …
Published in Journal of Polymer & Composites · Vol. 13, Issue 6, 2025 · pp. 272–282 Read article
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Facile Synthesis of SnO2/g-C3N4 nanocomposite for the photocatalytic degradation of Methylene Blue dye under visible light irradiation
Abstract: This work reports the nanoscale samples of pure tin dioxide (SnO₂), graphitic carbon nitride (g-C₃N₄), and their composite (SnO₂/g-C₃N₄) were successfully synthesized using the co-precipitation technique. The synthesized materials were extensively analyzed using multiple characterization techniques such as Powder X-ray Diffraction (PXRD), High-Resolution Scanning Electron Microscopy (HR-SEM), Energy-Dispersive X-ray Spectroscopy (EDAX), Fourier Transform Infrared Spectroscopy (FTIR), UV-Visible Spectroscopy, and High-Resolution Transmission Electron Microscopy (HR-TEM). Results from PXRD and EDAX confirmed …
Published in Journal of Polymer & Composites · Vol. 14, Issue 1, 2026 · pp. 1835–1845 Read article
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Synthesis and Structural Characterization of Nanocrystalline CeO2 and Ce0.95Cu0.05O2 Solid Solution Catalysts Properties and its Applications
Abstract: The Main study and the development of CeO2 and Cu doped CeO2 nanocrystals containing transition-metal species are of crucial importance for understanding the preparation and fabrication of CeO2 and Cu doped CeO2 nanoparticles by solution combustion technique to taken glycine as fuel. Here, we have investigated the effect of Cerium dioxide and Cu dopant ions on the structural properties of Ce1-xCuxO2 nanocrystals (NCs) synthesized via co-precipitation technique. XRD results confirmed …
Published in Journal of Catalyst & Catalysis · Vol. 11, Issue 4, 2024 Read article
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Efficient Green Synthesis of TiO2 Nanoparticles Using Murraya koenigii Leaf Extract
Abstract: Green synthesis of nanoparticles by plant extract is at present under exploitation due to eco-friendly, non-toxic and inexpensive process. Titanium dioxide (TiO2) nanoparticles were synthesized by ultrasound assisted sol-gel precipitation method using titanium tetra-isopropoxide as a precursor and Murraya koenigii leaf extract as a reducing and stabilizing agent. The leaf extract was prepared under various solvent media such as ethanol and distilled water under controlled ultrasonication. Due to effective ultrasound, …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 6, Issue 1, 2016 · pp. 29–38 Read article
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Exploring the Mechanical Characterization and Microstructural Properties of the Varying Weight % of Nano Boron Carbide (nB4C) Reinforced Al2024 composites using the Vacuum-Assisted Stir Casting Method
Abstract: In this investigation the stir casting technique is utilized to fabricate Al2024-B4C nano composites. The nanoB4C particles used in the reinforcement material have a particle size of 50 nm and variable weight percentages. In Al2024 composites, boron carbide reinforcement is included at weight percentages ranging from 0% to 3%, with a 1% interval between each percentage addition. Following the casting process, the samples were prepared for microstructural and mechanical evaluation …
Published in Journal of Polymer & Composites · Vol. 13, Issue 5, 2025 · pp. 394–404 Read article
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Comparative studies of Oxidation and hot corrosion behaviors of uncoated and detonation gun sprayed Cr3C2-25NiCr coating on SA-213 boiler steel at 8000C
Abstract: Fe-based alloys suffer oxidation and hot corrosion when the surfaces were in contact with air (oxidation) as well as the salty atmosphere (Hot corrosion) at elevated temperatures. In these atmospheric conditions, non-protective oxide Fe2O3 was formed on the surface of alloys. Oxidation and hot corrosion have been recognized as a major problem in the applications of the diesel engine, boilers, gas turbines, and chemical power plant etc. Detonation-gun sprayed Cr3C2-25NiCr …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 6, Issue 1, 2019 · pp. 17–22 Read article
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Surface Structure of Hydroxyl Apatite from Fluorosis Enamel
Abstract: Fluorosis is a condition due to ingestion of excessive amounts of Fluor that can cause the change in teeth structure and strength. Currently, a poor explanation was available to describe the surface structure of crystal hydroxylapatite that contributes to influence the macro characteristic of fluorosis enamel. The objective of this research is to describe the surface structure of crystal hydroxylapatite (HA) in fluorosis enamel. Scanning Electron Microscopy/ Energy Disperse X-Ray …
Published in Research and Reviews: A Journal of Dentistry · Vol. 2, Issue 1-3, 2011 · pp. 60–68 Read article
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Synthesis and Applications of Copper- Doped Pyridine Precipitate
Abstract: A metal organic nonlinear optical single crystal, copper doped pyridine material, was created at room temperature using the slow evaporation solution growth technique (SEST). The developed material's crystalline nature was revealed by a powder X-ray diffraction (XRD) analysis. Single crystal XRD study shows that the material synthesized possesses monoclinic system of cell parameters, a = 11.44 Å, b = 7.92 Å, C = 11.74 Å and alpha and gamma is …
Published in Journal of Materials & Metallurgical Engineering · Vol. 15, Issue 1, 2025 · pp. 51–60 Read article
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Molebdate as Corrosion Inhibitor for Aluminium 356 In Acidic and Saline Media
Abstract: Corrosion processes are the cause of significant losses in industry. Organic, inorganic, and mixed material inhibitors have all been used to resist corrosion for a long time, but the environmental toxicity of organic corrosion inhibitors has driven a quest for inorganic corrosion inhibitors. The effect of molybdate as a new corrosion inhibitor on the corrosion of aluminium 356 in acidic and saline conditions was investigated using electrochemical and weight loss …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 9, Issue 1, 2022 · pp. 39–47 Read article
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Microstructural and Mechanical characterization of Brass and Bronze alloys
Abstract: Brass, a copper and zinc alloy, is renowned for its malleability and resistance to corrosion, which makes it perfect for musical instruments and plumbing. Aluminium bronze, containing copper and aluminium, offers superior strength and wear resistance, commonly used in marine and industrial applications for its durability and corrosion resistance. This study aimed to compare the micro and macro structural characteristics of brass and aluminium bronze alloys. The microstructures of these …
Published in Journal of Materials & Metallurgical Engineering · Vol. 14, Issue 2, 2024 · pp. 28–37 Read article
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Light and Scanning Electron Microscopic Studies on Utricularia gibba L.––Lentibulariaceae
Abstract: Utricularia gibba L. belongs to family Lentibulariaceae, was studied using Light and Scanning Electron Microscopy to perform a comparative morphological analysis of the study species and conclude the evolutionary relationships of the section Utricularia.Keywords: Utricularia, LM, SEM, Pollen, Seed, phylogenyCite this ArticleRajasekar C, Samydurai P, Kanivalan I et al. Light and Scanning Electron Microscopic Studies on Utricularia gibba L.––Lentibulariaceae. Research & Reviews: Journal of Botany. 2017; 6(3): 7–10p.
Published in Research & Reviews : Journal of Botany · Vol. 6, Issue 3, 2017 · pp. 7–10 Read article
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Influence of SiO2 Nanoparticles on the Structural, Morphological, and Optical Properties of CsPbBr3 Quantum Dots
Abstract: This work mainly investigates the structural and optical property differences between CsPbBr3/SiO2 quantum dots (QDs) and CsPbBr3 QDs thin films deposited on fluorine-doped tin oxide (FTO) glass. X-ray diffraction of CsPbBr3/SiO2 QD thin film showed a polycrystalline cubic nanostructure with (200) as a dominant phase and did not show any peak of SiO2. Scanning and transmission electron microscopy images show that it is very small spherical or semi-spherical particles with …
Published in Journal of Polymer & Composites · Vol. 11, Issue 2, 2023 · pp. 62–69 Read article
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Comparative Study of Geopolymer Paste Prepared from Different Activators
Abstract: The present paper explores the comparative study of the geopolymer paste resulting from different alkali activations. In this experimental study, four series of geopolymer pastes differing in the alkali activation were manufactured by activating low calcium fly ash. These activators were subjected to a certain temperature of 35 °C for duration of 24 h. After casting of the specimens, activated by those activators, they were subjected to 85 °C for …
Published in Recent Trends in Civil Engineering & Technology · Vol. 2, Issue 1-3, 2012 · pp. 9–18 Read article
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Inhibitory Potentials of Datura Metel to Prevent Mild Corrosion
Abstract: The resistance of mild steel to corrosion was evaluated by immersing it in well water and determining the weight it lost after being allowed to return to room temperature after the submersion. The effectiveness of mild steel's ability to withstand corrosion was evaluated using this approach. A reduction in total body mass has an influence that is connected to and helps play a role in the prevention of rusting from …
Published in Journal of Polymer & Composites · Vol. 10, Issue 4, 2022 Read article
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Recent Advances in Crystal Defect Engineering of Semiconductor Photocatalysts for Sustainable Environmental and Energy Applications
Abstract: Semiconductor photocatalysis has emerged as one of the most promising green technologies for addressing environmental pollution and global energy challenges through solar energy utilization. Nevertheless, the practical application of conventional semiconductor photocatalysts is often limited by their narrow visible-light absorption, rapid recombination of photogenerated electron–hole pairs, insufficient active sites, and poor charge-transfer efficiency. Defect engineering has recently attracted significant attention as an effective strategy to overcome these limitations by deliberately …
Published in International Journal of Photochemistry and Photochemical Research · Vol. 4, Issue 2, 2026 Read article
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Structural and Dielectric Properties Hexaferrite/Poly (Vinyl Alcohol) Composites
Abstract: Magnetic barium cobalt hexaferrite particles-PVA composites with of different mass ratio: 9:1, 8:2, 7:3, 6:4 and 5:5 were prepared. Structural properties of the composites were characterized by Infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscope (SEM). The effect of the concentration of Ba2Co2Fe28O46 hexaferrites on structural and dielectric properties of magnetic-PVA composites were investigated. FTIR result revealed that composite samples show absorption peaks of both ferrites and PVA. …
Published in Research & Reviews : Journal of Physics · Vol. 2, Issue 3, 2013 · pp. 10–19 Read article
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Preparation and Characterization of Aluminium Doped ZnO Thin Films by Spin Coating Technique
Abstract: In this work, the preparation of Al-doped ZnO (AZO) thin films by the sol-gel spin-coating method is reported. The structural properties and surface morphologies of film prepared at RT were characterized by X-ray diffraction (XRD) and field emission scanning electron microscope (FE-SEM). The XRD and SEM results disclosed that the crystallization quality and grain size of as-prepared films were highly influenced by Al doping. Laser Raman Spectrometer results indicated that …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 7, Issue 2, 2020 · pp. 16–22 Read article
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Synthesis, Characterization and Deformation Studies of Blast Furnace Slag Particles Reinforced Aa2024 Composite
Abstract: The main objective is to explore the use of blast furnace slag as a reinforcing material. This work provides results of aluminum metal matrix composites reinforced with granulated slag (GS). The Composite is prepared by taking AA 2024 and GS with stir casting process. Optical microscope and scanning electron microscopy were employed to track the reactions between the aluminum matrix and the granulated slag during the sintering treatment. The hardness …
Published in Journal of Thin Films, Coating Science Technology & Application · Vol. 3, Issue 3, 2016 · pp. 31–43 Read article
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Synthesis and characterization of mixed SnO2-ZnO Nano composites material to study the kinetics of catalytic reduction of Aromatic Nitro compounds
Abstract: A straightforward and cost-effective method was employed to synthesize zinc oxide (ZnO) nanostructures supported on tin oxide (SnO₂) for catalytic applications. This hybrid nanocomposite, formed by integrating ZnO with SnO₂, exhibited impressive catalytic activity in the reduction of various nitro compounds. The synergistic interaction between ZnO and SnO₂ significantly enhanced the surface area and active sites of the catalyst, thereby improving its overall efficiency. The resulting SnO₂-ZnO nanocomposite not only …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 15, Issue 3, 2025 · pp. 8–14 Read article
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Synthesis and Characterization of Co-Doped ZnO Nanoparticles by Electrochemical Method: Photodegradation Kinetics of Bromophenol Blue Dye, Textile Effluent and Study of Antibacterial Activity
Abstract: ZnO nanoparticles doped with cobalt were synthesized by electrochemical method. The crystal structure and surface morphology were characterized by X-Ray diffraction and Scanning electron microscopy. The optical properties were studied by UV-Vis spectroscopy and from this the band gap energy was found to be 3.17 eV. The XRD data revealed that the crystalline size to be ~21.23 nm. The functional group test was done by FTIR-spectroscopy. SEM results showed the …
Published in Journal of Nanoscience, NanoEngineering & Applications · Vol. 5, Issue 1, 2015 · pp. 1–13 Read article